• 제목/요약/키워드: homogenization pressure

검색결과 87건 처리시간 0.025초

분말가압 성형공정의 멀티스케일 시뮬레이션과 공정변수 최적화 (Multi-scale Simulation of Powder Compaction Process and Optimization of Process Parameters)

  • 심진우;심정길;금영탁
    • 한국소성가공학회:학술대회논문집
    • /
    • 한국소성가공학회 2007년도 추계학술대회 논문집
    • /
    • pp.344-347
    • /
    • 2007
  • For modeling the non-periodic and randomly scattered powder particles, the quasi-random multi-particle array is introduced. The multi-scale process simulation, which enables to formulate a regression model with a response surface method, is performed by employing a homogenization method. The size of ${Al_2}{O_3}$ particle, amplitude of cyclic compaction pressure, and friction coefficient are considered as optimal process parameters. The optimal conditions of process parameters providing the highest relative density are finally found by using the grid search method.

  • PDF

초고압균질 가공에 의해 제조된 초미세 비지 현탁액의 영양성분 및 항산화성 (Antioxidant capacity and nutritive components from biji sub-micron suspension by ultra-high pressure homogenization process)

  • 이선호
    • 한국식품저장유통학회지
    • /
    • 제22권5호
    • /
    • pp.714-720
    • /
    • 2015
  • 본 연구는 산업 폐기물인 비지를 활용하여 부가 가치가 높은 가공식품을 개발하기 위한 일환으로 수행되었다. 즉 대두 가공 부산물인 비지를 활용하여 죽류, 음료류 및 유동식 등의 제품으로 개발하기 위해, 초고압균질 가공 기술을 활용하여 초미세 비지 현탁액을 제조하고 추출수율, 영양성분 및 항산화성을 확인하였다. 비지 분산액을 homogenizer를 이용하여 1,0000 rpm에서 5분 분쇄한 후 1,000bar, 1,500bar 및 2,000bar의 압력을 가해 고압균질 가공 처리하였다. 고압균질 가공처리한 모든 실험구가 대조군에 비하여 추출수율이 유의적으로 증가하였다(p<0.05). 초고압균질 처리 후 총당, 환원당 및 가용성 식이섬유의 함량은 유의적으로 증가하였으며, 불용성 식이섬유는 유의적으로 감소하였다(p<0.05). 단백질 함량과 유리아미노산 함량은 대조군보다 높은 경향을 나타내었다. 총 폴리페놀 함량은 처리 압력이 높아질수록 유의적으로 증가하였으며, ABTS 라디칼 소거능도 유의적으로 증대되었다(p<0.05). 초고압균질 가공 기술은 비지의 영양성분과 항산화성을 증가시키는 매우 효과적인 가공방법이며, 비지의 영양성분을 효율적으로 활용하여 가공식품을 제조할 수 있음을 확인하였다.

Lipid nanodispersion for parenteral drug delivery: in vitro characterization

  • Lee, Jung-Min;Choi, Sung-Up;Lee, Byoung-Moo;Lee, Sung-Jae;Choi, Young-Wook
    • 대한약학회:학술대회논문집
    • /
    • 대한약학회 2003년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.1
    • /
    • pp.295.2-295.2
    • /
    • 2003
  • Lipid nanodispersion (LN) composed of biocompatible lipids and surfactants is an alternative parenteral drug delivery system especially for lipophilic drugs. It has been studied for versatile applications such as oral, parenteral, topical, ocular, vaccine, and peptide drug delivery. The purpose of this study was to produce a novel LN system for intravenous injection using the high pressure homogenization. (omitted)

  • PDF

청일(晴日) 금광산(金鑛山)의 유체포유물연구(有體包有物硏究) (Fluid Inclusion Study of Chungil Gold mine)

  • 장태영;지정만
    • 자원환경지질
    • /
    • 제22권3호
    • /
    • pp.193-205
    • /
    • 1989
  • Regional geology of Chungil mine is composed of Cretaceous biotite granite. Chungil ore deposits are fissure filled quartz veins which developed in Cretaceous biotite granites. Mineralogic and fluid inclusion studies were undertaken to illuminate the origin of the ore deposits. Data gathered from occurrences of ore deposits and mineral paragenesis reveals that there were two major mineralization stage. The first stage is sulfides-quartz stage. The constituents of ore minerals are chalcopyrite, sphalerite, pyrrhotite with minor amount of galena, native Au, Ag, pyrite. The second stage is gangue mineral stage. Gangue minerals are quartz, fluorite and calcite. Homogenization temperature of fluid inclusions in quartz of the first and the second stage ranges from $212^{\circ}C$ to $336^{\circ}C$ and from $154^{\circ}C$ to $355^{\circ}C$ respectively. Homogenization temperature in fluorite and calcite of the second stage ranges from $127^{\circ}C$ to $252^{\circ}C$ and from $129^{\circ}C$ to $158^{\circ}C$ but these data require positive pressure corrections. Fluid inclusions in quartz of the Bongmyeong mine, Jangja the first mine and the second mine show range of homogenization temperature from $178^{\circ}C$ to $330^{\circ}C$, from $185^{\circ}C$ to $354^{\circ}C$ and from $206^{\circ}C$ to 336 respectively. The comparison of the fluid inclusion data, mineralogical component and vein attitude of the three mines with that of Chungil mine indicates that the origin of the deposits above mentioned is elucidated to be formed under similar environment. The compositions of the sphalerite in the first stage range from 16.05 mol.% FeS to 20.36 mol.% FeS.

  • PDF

삼광(三光) 금(金) 광상(鑛床)의 광화(鑛化) 온도(溫度) 및 근원(根源)에 관關(한) 연구(硏究) (Study on the Temperature and the Origin of Mineralization at the Samkwang Au Deposits)

  • 문건주
    • 자원환경지질
    • /
    • 제19권1호
    • /
    • pp.19-24
    • /
    • 1986
  • The Samkwang mine is one of gold deposits distributed mainly in the southwestern province (Chungnam) of the Korean peninsula. Golds occur in quartz veins aged of $223{\pm}4MA$ according to K-Ar age dating from muscovite in a pegmatitic quartz vein. Quantz veins intrude Precambrian biotite-granite gneiss and mica schist of unknown age. Fluid inclusions in the quartz show a range of homogenization temperatures from 159 to $274^{\circ}C$. A calculated temperature from the isotopes of the galena-sphalerite pair is $375^{\circ}C$. Two phases-fluid inclusions homogenized either by liquid or vapor phase are frequently observed in specimens over $260^{\circ}C$, which may indicate the boiling of the fluids. Pressure of formation of the quartz veins inferred by the homogenization temperatures of liquid-$CO_2$ bearing fluid is 1kb. Based on these data, it is assumed that the temperature of the formation of the Samkwang mine may lie in between $350^{\circ}-230^{\circ}C$. ${\delta}^{34}S_{{\Sigma}s}$ values of sulphide minerals show narrow range of +2.1 to +4.6, and show a trend of enrichments of $^{34}S$ in the fluid from deep to the surface. ${\delta}^{34}S_{{\Sigma}s}$ in the fluid estimated is less than 3 permil, suggesting sulphur fluid originated from the magma.

  • PDF

금령(金嶺) 및 기구광상(基邱鑛床)의 동광화작용(銅鑛化作用) (The Copper Mineralization of the Keumryeong and Kigu Ore Deposits)

  • 박희인;설용구
    • 자원환경지질
    • /
    • 제25권3호
    • /
    • pp.283-296
    • /
    • 1992
  • The Keumryeong deposits is a low grade copper deposits in which copper minerals form disseminated grains and thin veinlets in felsic volcanics seem to be dacite. Alteration of the volcanics consists mainly pervasive propylitization and silicification. Potassic alteration characterized by biotite developed locally adjacent to southwestern contact of granodiorite body. Principal sulfide minerals in altered zone are mainly pyrite and lesser chalcopyrite. Chalcopyrite content in potassic zone is relatively higher than that of surrounding propylitized zone. Pyrite and chalcopyrite accompanies magnetite, molybdenite, sphalerite, pyrrhotite, arsenopyrite, pentlandite, marcasite, hematite, ilmenite, rutile, bismuthinite and native Bi as disseminations, veinlets and knots. Granodiorite body is propylitized and contains veinlets of pyrite, chalcopyrite and molybdenite. Fluid inclusions in sulfide-bearing quartz veinlets and quartz grains of felsic volcanics and granodiorite in altered zone consist of liquid-rich, vapor-rich, $CO_2-bearing$ and halite-bearing inclusions. These four types of inclusion intimately associated on a microscopic scale and indicate condensing or boiling of ore fluid during mineralization. Homogenization temperature of coexisting fluid inclusions are mostly in the range of 350 to $450^{\circ}C$. High salinity fluid contains 28.6 to 48.4 weight percent NaCI equivalent and moderate salinity fluid cotains 0.5 to 12.5 weight percent NaCl equivalent. Pressure estimated from $CO_2$ mole fraction of $CO_2-bearing$ inclusion range 160 to 375 bars. The Kigu copper deposits is a fissure filling copper vein developed 500 m south from the Keumryong deposits. Mineralogy and fluid inclusion data of the Kigu deposits are similar to that of the Keumryeong deposits. Homogenization temperature of fluid inclusions from the Kigu deposits are reasonable agreement with temperature estimated from sulfidation curve of cubanite-chalcopyrite-pyrite-pyrrhotite and pyrite-pyrrhotite mineral assemblages. Not only mineral occurrence and wall rock alteration in the Keumryeong deposits but also fluid inclusion data such as temperature, salinity, pressure and boiling evidences are similar to those of porphyry copper deposits.

  • PDF

고압 균질기를 통해 합성된 이산화망간 나노입자에 의한 일산화탄소의 촉매적 산화 (Catalytic Oxidation of CO over Manganese Dioxide Nanoparticles Synthesized Using a High Pressure Homogenizer)

  • 지성화;김효진
    • 한국표면공학회지
    • /
    • 제53권1호
    • /
    • pp.22-28
    • /
    • 2020
  • In this study, manganese dioxide (MnO2) nanoparticles were synthesized from KMnO4 and MnCl2·4H2O without any dispersing agents and oxidant via ultra-high pressure homogenization process. We investigated various physicochemical properties and CO oxidation reactions of the MnO2 nanoparticles as a function of the number of passes at 1,500 bar in a high pressure homogenizer nozzle. The observed X-ray diffraction patterns and scanning electron microscopy images revealed that the synthesized MnO2 nanoparticles had a hexagonal structure and a uniform spherical shape. It was found from the Brunauer-Emmett-Teller measurements that the pore size of the MnO2 nanoparticles ranged from 23.6 to 7.2 nm and their specific surface area ranged from 24 to 208 m2g-1. In particular, it was confirmed from the measurements of CO conversion into CO2 that CO oxidation reaction over the MnO2 nanoparticles exhibited excellent catalytic activity at low temperatures below 100℃.

경상분지 남동부의 산내화강암과 산내 W-MO 광상에 관한 유체포유물 연구 (A Fluid inclusion study of the Sannae granite and the associated Sannae W-Mo deposit, Southeastern Kyongsang Basin)

  • 양경희;이준동
    • 암석학회지
    • /
    • 제8권1호
    • /
    • pp.46-55
    • /
    • 1999
  • Fluid inclusions in granite and hydrothermal quartz indicate that three fluids have affected the Sannae granite. The earliest fluid is represented by three-phase aqueous fluid inclusions with high salinity (38 to 46 wt.% NaCl equiv.). It was exsolves from a crystallizing melt and trapped at a relatively high-pressure condition. The secong fluid is represented by two-phase aqueous fluid inclusion with low entectic temperatures (< $-40^{\circ}C$). low- to moderate salinity (3 to 24.0 wt.% NaCl equiv.) and high homogenization temperatures$ ($309^{\circ}C$$473^{\circ}C$)($. This fluid was trapped at higher pressures than 300-500 bars and precipitated molybdenite and wolframite in quartz veins. It was probably generted by fluid-host rock interactions since they show a wide range of salinity within a narrow range of homogenization temperatures. The final fluid is represented by an aquenous fluid boiling that separated into high-salinity (34-38 wt.% NaCl equiv.) and low-salinity fluid (0 to 8.7 wt.%) at $303-376^{\circ}C$ and 50-150 bars. These boiling fluids precipitated euhedral quartz in miarolitic cavities. The compositions of the final fluid was rather complex in the $H_2$O-NaCl-KCI-$FeCl_2$ system. The Sannae granite was a locus for repeated fluid events including magmatic fluids during the final stage of crystallization, the convection of hydrothermal fluids causing a fluid ascending, fluid boiling, and the local W-Mo mineralization and formation of miarolitic cavities due to thermal, tectonic and compositional properties of the felsic granite.

  • PDF

두유(豆乳)의 현탁안정성에 관한 연구 (Studies on Stability of Soymilk Suspension)

  • 김은수;조재선
    • 한국식품과학회지
    • /
    • 제22권3호
    • /
    • pp.312-318
    • /
    • 1990
  • 두유제품을 저장하는 동안 단백질 등의 침전과 지방질의 크림층이 분리되는 현상에 미치는 두유제조 조건의 영향을 검토하기 위해서 분쇄, 균질처리 및 열처리조건이 두유의 현탁안정성에 미치는 영향을 조사하였다. 먼저 $20^{\circ}C$의 물로 마쇄한 것을 blanching시 온도에 반비례하여 질소 용해도지수가 현저히 감소하였으나 $80^{\circ}C$의 물로 마쇄하는 경우 그 감소폭이 $20^{\circ}C$의 경우보다 적었다. 침지 대두를 분쇄하여 단백질 입자가 $53{\mu}$에서 $8{\mu}$으로 작아질수록 침전량이 감소하여 두유의 현탁안정성이 증가하였고 균질처리를 1회한 것보다는 2회 반복처리 한 것이 안정성이 증가하였으며 1회 처리시는 입자의 크기에 따라 차이가 심하였지만 2회 처리시는 그 차이가 감소되었다. 균질처리시 1단계 처리압력이 $200kg/cm^2$까지는 안정성이 증가하였고 팜유를 첨가하여 균질처리를 할 때의 온도가 $80^{\circ}C$까지 온도를 높일수록 안정성이 증가하였다. 두유제품을 살균할 때 열처리온도가 $120{\sim}125^{\circ}C$에서 30분 이상 열처리시에는 안정성이 급격히 감소되었다.

  • PDF