• Journal of the Korean Ceramic Society
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• v.24 no.2
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• pp.186-192
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• 1987

ZrO2 powders having high purity were prepared from domestic zircon sand using the caustic fusion method and the soda ash sintering process. In the caustic fusion method, ZrO2 recovery was reached to 96% when 100/140 mesh zircon was reacted with NaOH at the NaOH/Zircon mole ratio 6 and at 650$^{\circ}C$ for 2 hours. And in the soda ash sintering process, ZrO2 was recovered to 88.5% when -325 mesh zircon was reacted with Na2CO3 at the Na2CO3/Zircon mole ratio 1.1 and 1050$^{\circ}C$ for 2 hours. In both cases, Zr component was extracted to ZrOCl2, subsequently crystallized to ZrOCl2$.$8H2O to increase the purity, and converted to ZrO2 by precipitation. And to increase the sinter ability of powder, Cl- ion was removed and strong agglomeration was avoided by methanol distribution of Zr(OH)4 precipitates.

• Applied Chemistry for Engineering
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• v.4 no.4
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• pp.798-806
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• 1993

In this study we developed the synthesis of high purity tungsten oxide from tungsten chlorides obtained by the chlorination of scheelite in a fluidized bed reactor. Within a minute of dissolution time, tungsten chlorides were almost dissolved in $H_2O_2$ solution. The proper dissolution conditions for the tungsten chlorides were as follows : $H_2O_2$ concentration 0.5%, dissolution temperature $15^{\circ}C$ and $H_2O_2$ amount to 0.5g tungsten chlorides 30ml. Under above conditions, the tungsten oxide prepared from dissolved product was identified as $WO_3$ and the purity of $WO_3$ was 99.53%.

• Resources Recycling
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• v.22 no.1
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• pp.48-54
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• 2013

A laboratory study was carried out to recover KI crystals with high purity by using fractional crystallization method from a waste solution generated from the production of polarizing film for LCD industry. The waste solution contains 1.3% KI, and other impurities such as B, Na, and PVA etc. With purity higher than 99.5% KI crystals were produced through refining process such as vacuum evaporation, fractional crystallization, filtering, and 24hr aging. Also the concentrated impurities were eliminated about 70% by recrystallization.

• Archives of Pharmacal Research
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• v.29 no.9
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• pp.808-813
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• 2006

Two methods for the chiral purity determination of bevantolol were developed, namely capillary electrophoresis (CE) using carboxymethyl-${\beta}$-cyclodextrin (CM-${\beta}$-CD) as a chiral selector and high-perfomance liquid chromatography (HPLC) using a chiral stationary phase. In the HPLC method, the separation of bevantolol enantiomers was performed on a Chiralpak AD-H column by isocratic elution with n-hexane-ethanol-diethylamine (10:90:0.1, v/v/v) as mobile phase. In the CE method, bevantolol enantiomers were separated on an uncoated fused silica capillary with 50 mM amonium phosphate dibasic adjusted to a pH 6.5 with phosphoric acid containing 15 mM CM-${\beta}$-CD as running buffer. Validation data such as linearity, recovery, detection limit, and precision of the two methods are presented. The detection limits of S-(-)-bevantolol were 0.1% and 0.05% for CE and HPLC method, respectively and R-(+)-bevantolol were 0.15% and 0.05% for CE and HPLC method, respectively. There was generally good agreement between the HPLC and CE results.

• International Journal of Internet, Broadcasting and Communication
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• v.7 no.2
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• pp.9-15
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• 2015

Various studies with regard to increasing the optical efficiency of plasmonic color filters have previously been conducted, such as mixing materials or applying diverse pattern shapes. Fundamentally, it is important to maximize the photonic crystal effect by finding the optimum periods of lattice as well as calculating the most efficient transmission area. In this study, we propose a technical method for optimizing the plasmonic color filters that have a high color gamut and luminance by analyzing the light spectrums based on the 1931 color coordinate system. Moreover, we suggest a calculation method in order to define the individual color purity of red and green and blue filters. Consequently, efficiency values are obtained independently from each color filter by evaluating the color purity and the luminance. The final result obtained from simulation are 27.6% of relative luminance and 25.3% of color gamut. The proposed optimization method is applicable to all plasmonic color filters having photonic crystal arrays.

• Journal of Korea Foundry Society
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• v.15 no.3
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• pp.235-241
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• 1995

In order to improve the production process of low cost and high purity Vanadium, this study was done to reduce $V_2O_5$ into V-Al master alloy by Aluminothermic Reduction, followed by refining of V-Al master alloy electron beam melting. As melting time was increased in electron beam melting of V, the contents of interstitial impurities and Al, Fe were decreased but the contents of Si, Mo and W were increased due to lower vapor pressure of these elements than that of matrix V. Consequently, it was profitable that melting of V was done for 180 seconds. In addition, with number of melting, the purity of V did not significantly vary, because volatile impurities in V were removed mostly during the first step of melting. As a result of V refining by electron beam melting, high purity Vanadium of 3N(99.91wt%) was acquired including interstitial impurities total contents of which were maximum 400ppm.

• Proceedings of the Materials Research Society of Korea Conference
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• 1992.05a
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• pp.75-76
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• 1992

• Proceedings of the Korean Ceranic Society Conference
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• 1986.12a
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• pp.114-139
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• 1986

• Journal of the Korean Ceramic Society
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• v.49 no.4
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• pp.328-332
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• 2012

Etch rates of Si and high purity SiC have been compared for various fluorocarbon plasmas. The relative plasma resistance of SiC, which is defined as the etch rate ratio of Si to SiC, varied between 1.4 and 4.1, showing generally higher plasma resistance of SiC. High resolution X-ray photoelectron analysis revealed that etched SiC has a surface carbon content higher than that of etched Si, resulting in a thicker fluorocarbon polymer layer on the SiC surface. The plasma resistance of SiC was correlated with this thick fluorocarbon polymer layer, which reduced the reaction probability of fluorine-containing species in the plasma with silicon from the SiC substrate. The remnant carbon after the removal of Si as volatile etch products augments the surface carbon, and seems to be the origin of the higher plasma resistance of SiC.

• Clean Technology
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• v.24 no.1
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• pp.15-20
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• 2018

Hexafluoropropyleneoxide ($C_3F_6O$, HFPO) is highly expensive and it may be used as a raw material for the synthesis of various fluorine based compounds. Currently, extractive distillation method has gained considerable attention to collect the HFPO from a mixture of HFPO / hexafluoropropylene ($C_3F_6$, HFP). Optimized operating conditions are studied using a theoretical method for the extraction process. Among available solvents for the purification process, the use of 1,1-dichloro-1-fluoroethane exhibits a high purity of HFPO as a top product and minimize the required heat duty. Since the boiling point of the solvent increases as the pressure in the column increases, the enhanced extractive capability of the solvent led to the high purity of HFPO at the high pressure.