• Proceedings of the Materials Research Society of Korea Conference
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• 2009.11a
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• pp.31.1-31.1
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• 2009

In an approach to acclimate ourselves torecent ecological consciousness trend, a lead-free piezoelectric material, bismuth sodium titanate (abbreviated as BNT) based bismuth sodium barium titanate (abbreviated as BNT-BT), was considered as an environment-friendly alternative for a lead based piezoelectric system. Ceramic specimens of0.94[(BixNa0.5)TiO3]-0.06[BaTiO3] (x = 0.500~0.515) compositions were prepared by a modified mixed oxide method. To increase the chemical homogeneity andre action activity, high energy mechanical milling machine and pre-milled nanosized powder has been used. In this method (BixNa0.5)TiO3 (x=0.500~0.515) andBaTiO3 were prepared separately from pre-milled constituent materials at low calcination temperature and then separately prepared BNTX (X=1, 2, 3 and 4) and BT were mixed by high energy mechanical milling machine. Without further calcination step the mixed powders were pressed into disk shape and sintered at $1110^{\circ}C$. Microstructures, phase structures and electrical properties of the ceramic specimens were systematically investigated. Highly dense ceramic specimens with homogenous grains were prepared in spite of relatively low sintering temperature. Phase structures were not significantly influenced by the excess amount Bi. Large variation on the piezoelectric and dielectric properties was detected at relative high excess Bi amounts. When $x{\leq}0.505$, the specimens exhibit insignificant variation in piezoelectric and dielectric constant though depolarization temperature is found to be decreased. Considerable amount of decrease in piezoelectric and dielectric properties are observed with higher excess of Bi amounts ($x{\geq}0.505$). This research indicates the advantages of high energy mechanical milling and importance of proper maintenance of Bi stoichiometry.

• Advanced Composite Materials
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• v.18 no.3
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• pp.233-249
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• 2009

Safe installation and operation of high-pressure composite cylinders for hydrogen storage are of primary concern. It is unavoidable for the cylinders to experience temperature variation and significant thermal input during service. The maximum failure pressure that the cylinder can sustain is affected due to the dependence of composite material properties on temperature and complexity of cylinder design. Most of the analysis reported for high-pressure composite cylinders is based on simplifying assumptions and does not account for complexities like thermo-mechanical behavior and temperature dependent material properties. In the present work, a comprehensive finite element simulation tool for the design of hydrogen storage cylinder system is developed. The structural response of the cylinder is analyzed using laminated shell theory accounting for transverse shear deformation and geometric nonlinearity. A composite failure model is used to evaluate the failure pressure under various thermo-mechanical loadings. A back-propagation neural network (NNk) model is developed to predict the maximum failure pressure using the analysis results. The failure pressures predicted from NNk model are compared with those from test cases. The developed NNk model is capable of predicting the failure pressure for any given loading condition.

• Journal of Powder Materials
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• v.6 no.4
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• pp.277-285
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• 1999

Mechanical properties of nanocrystalline Al-5at.%Ti alloy were investigated through high temperature compression test. Al-5at.%Ti nanocrystalline metal powders, which had finer and more equiaxed shape than those produced at room temperature, were produced by mechanical alloying at low temperature. The powders were successfully consolidated to 99fo of theoretical density by vacuum hot pressing. XRD and TEM analysis revealed that $Al_3Ti$ intermetallic compounds formed inside powders and pure Al region with coarse grains formed between powders, especially at triple junction. Mechanical properties in terms of hardness and strength were improved by grain size refinement, but ductility decreased presumably due to the formation of the weak interfaces between Al pool and powders.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1988.05a
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• pp.67-69
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• 1988

In this study, after changing the curing condition of hardner(DDM) and filler($SiO_2$) contents dielectric and dynamic mechanical properties were studied according to the variation of temperature. As the result we obtained a correlative $\alpha$-peak at 125-150[$^{\circ}C$] from dielectric and mechanical properties. With increasing curing condition and filler contents both dielectric and internal friction loss were, decreased, peak temperature shifted to high temperature, but there was no variation on peak temperature with filler contents. As the above result we knew the correspondence between dielectric and mechanical characteristics.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2011.11a
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• pp.211-212
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• 2011

It was very important to evaluate concrete experimentally at elevated temperature because concrete was filled with aggregate of concrete volume about 70 percent. Concrete exposure to high temperatures produces changes in its internal structure, for instance loss of its strength and deformation capacity, in extreme cases risking the service life of the structure. The work of this paper is performed to evaluate the thermal behavior of ultra-high strength concrete having different water to cement ratio (strength), fine aggregate to aggregate ratio and maximum size of coarse aggregate. For exposure to 500℃ during 1 hour, residual mechanical properties of the ultra-high strength concrete decreased as the s/a ratio decreases and the maximum size of coarse aggregate increases.

• Journal of Powder Materials
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• v.18 no.5
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• pp.401-405
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• 2011

Half-heusler phase ZrNiSn is one of the potential thermoelectric materials for high temperature application. In an attempt to investigate the effect of Sb doping on thermoelectric properties, half-heusler phase $ZrNiSn_{1-x}Sb_x$ ($0{\leq}x{\leq}0.08$) was synthesized by mechanical alloying of stoichiometric elemental powder compositions, and consolidated by vacuum hot pressing. Phase transformations during mechanical alloying and hot consolidation were investigated using XRD. Sb doped ZrNiSn was successfully produced in all doping ranges by vacuum hot pressing using as-milled powders without subsequent annealing. Thermoelectric properties as functions of temperature and Sb contents were evaluated for the hot pressed specimens. Sb doping up to x=0.04 in $ZrNiSn_{1-x}Sb_x$ was shown to be effective on thermoelectric properties and the figure of merit (ZT) was shown to reach to the maximum at x=0.02 in this study.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2008.11a
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• pp.403-403
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• 2008

This article reports changes in the mechanical properties of chromium steel after nitrogen implantation at high temperature. The samples are implanted with 120keV N-ion at doses ranging from $1\times1080$ to $4\times1080ions/cm^2$ and at substrate temperature ranging from 25 to $400^{\circ}C$. Nano-hardness and AES(Auger electrons spectroscopy) were measured from nitrogen ion implanted layer. The sliding wear and impact wear properties of the implanted samples were also measured. The results revealed that the hardness and mechanical properties of ion implanted samples depend strongly on the ion doses and implantation temperature. The hardness of the nitrogen implanted sample with 120keV, $4\times10^{18}ions/cm^2$, $335^{\circ}C$ was measured to be approximately 20 GPa, which is approximately 5 times higher than that of un-implanted sample (H=3.8 GPa). Also, the sliding wear and impact wear properties of nitrogen implanted samples were greatly improved. Detailed experiment results will be presented.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2007.04a
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• pp.9-12
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• 2007

Recently, research and development related to high strength concrete for the high rise and large scale reinforced concrete building has been actively promoted in worldwide by national and private research project. But, it is reported that violent explosive explosion would be happened when it was exposed in fire. In the existed study, a explosion in a reinforced concrete structure looses the organism by the different contraction and expansion of hardened cement paste and aggregate, and causes crack by thermal stress. In case of the Europe, Japan and America, they have studied the explosion for a long time. However it would hardly study the explosion in domestic, So it is needed base on mechanical properties of fire deterioration in high strength concrete. Therefore, this study is intend as an mechanical properties of specimen to high heating by heating and load test machine and $700^{\circ}C$. As a result, it is willing to propose fundamental data for quick and accurate diagnosis of deteriorated concrete structure by fire damage with experiment according to the design high strength concrete.

• Journal of Welding and Joining
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• v.22 no.4
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• pp.50-58
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• 2004

In this study, high temperature tensile properties of high strength steels(POSTEN60, POSTEN80) were investigated. The three-dimensional thermal elastic-plastic analyses were conducted to investigate the characteristics of welding residual stresses in welds of high strength steels on the basis of thermal and mechanical properites at high temperature obtained from the experiment. According to the results, high temperature tensile strength of POSTEN60 steel deteriorated slowly to 10$0^{\circ}C$. As the temperature went up, the tensile strength became better because of blue shortness, and it deteriorated radically after reaching to the maximum value around 30$0^{\circ}C$. For the POSTEN80 steel, high temperature tensile strength deteriorated slowly to 20$0^{\circ}C$. As the temperature went up the tensile strength became better and it deteriorated slowly to $600^{\circ}C$ after reached to the maximum value around 30$0^{\circ}C$. Strain of high strength steels at the elevated temperature increased radically after the mercury rose to $600^{\circ}C$. The strain hardening ratio of POSTEN60 steel was larger then that of POSTEN80 steel at the elevated temperature as in the case at the room temperature and it became smaller radically after the mercury rose to 40$0^{\circ}C$. And, in the welding of high strength steels, increasing tensile strength of the steel (POSTEN60

• Transactions of Materials Processing
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• v.18 no.3
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• pp.236-244
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• 2009

In response to growing environmental and collision-safety concerns, the automotive industry has gradually used high-strength and ultla-high-strength steels to reduce the weight of automobiles. In order to overcome inherent process disadvantages of these materials such as poor formability and high springback at room temperature, hot forming has recently been developed and adopted to produce some important structural parts in automobiles. This method enables manufacturing of components with complex geometric shapes with minimal springback. In addition, a quenching process may enhance the material strength by more than two times. This paper investigates mechanical and forming characteristics of high-strength boron-alloyed steel with hot forming, in terms of hardness, microstructure, residual stress, and springback. In order to compare with experimental results, a finite element analysis of hot forming process coupled with phase transformation and heat transfer was carried out using DEFORM-3D V6.1 and also, to predict high temperature mechanical properties and flow curves for different phases, a material properties modeler, JMatPro was used.