• Title/Summary/Keyword: high speed deposition

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Flow and heat transfer in a thermal CVD for carbon nanotubes according to variation of the inlet and outlet areas (유입.유출구 크기 변화에 따른 CNT용 CVD 장비 내의 열 및 유동해석)

  • Ha, Da-Som;Jang, Young-Woon;Kim, Jong-Seok;Yoon, Suk-Bum;Im, Ik-Tae
    • Journal of the Semiconductor & Display Technology
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    • v.10 no.4
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    • pp.119-124
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    • 2011
  • Flow and temperature field in reactors are important factors for design of thermal chemical vapor deposition system to grow carbon nanotubes. In this study, effects of the variations of the inlet and outlet areas of the CVD reactor to the flow characteristics and temperature field are numerically analyzed. High temperature of the gas in the entrance region is obtained with slow gas speed resulted from the enlarged inlet area. Variation of the exit area has little effects on the flow field and temperature in the reactor. However the largest area among considered cases gives the highest gas temperature though the differences are small.

Mechanical Properties of 316L manufactured by Selective Laser Melting (SLM) 3D printing (Selective Laser Melting (SLM) 방식 3D Printing으로 제조한 스테인레스 316L 기계적 물성 분석)

  • Park, Sun Hong;Jang, Jin Young;Noh, Yong Oh;Bae, Byung Hyun;Rhee, Byong Ho;Eo, Du Rim;Cho, Jung Wook
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2017.05a
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    • pp.872-876
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    • 2017
  • Laser Based 3D Printing is an recently advance manufacturing technology for making complex shape comopnent such as automobile and aerospace. So in this article, stainless steel 316L was manufactured by Selective Laser Melting (SLM) and Laser Melting Deposition (LMD) method. SLM is an additive manufacturing process that allow for the manufacture of small and complex component by laser melting and solidification of powder in bed using a high intensity laser beam. The results showed that the laser scanning speed and laser power affects the defect, microstructure and the hardness of the components.

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Microstructures and Mechanical Properties of Al-B4C Composites Fabricated by DED Process (DED 공정으로 제조된 Al-B4C 복합재의 미세조직 및 기계적 특성)

  • Yu-Jeong An;Ju-Yeon Han;Hyunjoo Choi;Se-Eun Shin
    • Journal of Powder Materials
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    • v.30 no.3
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    • pp.262-267
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    • 2023
  • Boron carbide (B4C) is highly significant in the production of lightweight protective materials when added to aluminum owing to its exceptional mechanical properties. In this study, a method for fabricating Al-B4C composites using high-energy ball milling and directed energy deposition (DED) is presented. Al-4 wt.% B4C composites were fabricated under 21 different laser conditions to analyze the microstructure and mechanical properties at different values of laser power and scan speeds. The composites fabricated at a laser power of 600 W and the same scan speed exhibited the highest hardness and generated the fewest pores. In contrast, the composites fabricated at a laser power of 1000 W exhibited the lowest hardness and generated a significant number of large pores. This can be explained by the influence of the microstructure on the energy density at different values of laser power.

Physical Properties Variation of Grout Materials Based on the Water to Cement Ratio and the Mixing Speed (물시멘트비 및 혼합속도에 따른 주입재의 물성변화 연구)

  • Chun, Byung-Sik;Kim, Jin-Chun;Jang, Bui-Woong;Lee, Jun-Woo
    • Journal of the Korean GEO-environmental Society
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    • v.1 no.1
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    • pp.87-96
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    • 2000
  • Generally, OPC(ordinary portland cement) is used for grouting in Korea, and bentonite has usually been added to prevent the deposition of cement particles. The dispersion of CB(cement bentonite) grout is influenced by variable factors i.e. water to cement ratio, particle size of cement, kind of bentonite, adding volume, method of adding, viscosity of CB grout materials and curdling time. Among variable factors, the viscosity of CB grout materials is influenced by the dispersion, and dispersion is improved as the speed of grout mixer increase. In this paper, the specification of construction was derived by estimating physical characteristics of CB grout materials and confirming the sate of dispersion. The results show that the engineering characteristics of CB grout materials vary with the water to cement ratio and the mixing speed.

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Mechanical Properties of HfN/Si$_3$N$_4$and NbN/$Si_3N_4$Multilayer Coatings (HfN/Si$_3$N$_4$와 NbN/$Si_3N_4$다층박막의 기계적 특성)

  • Jeong, Jin-Jung;Hwang, Seon-Geun;Lee, Jong-Mu
    • Korean Journal of Materials Research
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    • v.11 no.3
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    • pp.236-242
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    • 2001
  • HfN/Si$_3$N$_4$and NbN/Si$_3$N$_4$ multilayer coatings were deposited onto a high speed tool steel substrate by reactive sputtering and their mechanical properties were evaluated in terms of the dependence of hardness and adhesion strength on the sputter deposition process parameters. The hardnesses of both HfN/Si$_3$N$_4$and NbN/Si$_3$N$_4$ multiplayer coatings increase up to the flux ratio of 0.4 but nearly do not change after that as the $N_2$/Ar flux ratio in nitride sputter deposition increases. The hardnesses of both multiplayer coatings nearly do not change with annealing at low temperatures but decrease owing to oxidation with annealing at a high temperature like 80$0^{\circ}C$ after depositing the layers by sputtering. Post-annealing at low temperatures increases the adhesion strength of the multilayers. but high temperature annealing is not desirable since it decreases the adhesion strength besides the hardness deterioration.

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An Evaluation of Skiving Cutting Characteristics of TiCN PACVD Coating Caribide Hob (TiCN PACVD코팅 초경호브의 Skiving절삭특성 평가)

  • Cheon, Jong-Pil
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.2
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    • pp.471-477
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    • 2012
  • SCM420 steel tempered after performing gear hove PACVD carbide coating on the surface after the cutting surface hardness was high. Difficult-to-cut, without coating is classified as mild as large, including materials like mild, high strength that improves tool life and productivity have limited availability. Drive to improve it in the TiCN-coated carbide call for war to the finish coating on cutting a hob skiving good workability, tool wear less, 2.5-fold increase in tool life results were obtained. Experiments using CNC Skiving hobbing machine with wet cutting conditions, cutting speed and feed rate to apply a variety of the tool wear and surface roughness data were obtained. Results from condition 2 (V = 200m/min F = 0.7mm/rev) cutting speed feed mark the cutting surface microstructure and surface roughness Rmax $4.7{\mu}m$(Ra $1.19{\mu}m$) of the data was obtained.

Development of Variable Deposition manufacturing for Ethylene Vinyl Acettecopolymer (EVA를 이용한 가변 용착 쾌속 조형 공정의 개발)

  • Lee, Sang-Ho;Sin, Bo-Seong;Jeong, Jun-Ho;An, Dong-Gyu;Yang, Dong-Yeol
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.9
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    • pp.189-195
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    • 2000
  • RP techniques have their unique characteristics according to the working principles : star-stepped surface of parts due to layer-by-layer stacking low build speed caused by line-by-line solidification to fish one layer and post processing to improve surface finish etc The objective of this study is to propose a new RP technique Variable Deposition Mnanufacturing (VDM) which can make up for the disadvantages of the existing RP techniques and to develop an apparatus to implement the technique. The proposed process can greatly reduce the build time and improve the surface finish of parts generated. Experiments are carried out to obtain the range of temperature of molten material to maintain its fluidity and to investigate the effect of gas cooling on the preservation of the slopes. Some simple shapes such as a line-shape an S-shape and a circle-shape are fabricated from Ethylene Vinyl Acetatecopolymer(EVA) In order to examine the applicability of VDM to more general shapes a tensile specimen and a yo-yo shape were manufactured by the proposed RP method using EVA material as a trial approach. The current basic study shows a high potential of practical use of the proposed VDM process to prototyping of a general three-dimensional shape.

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Characteristics of regional scale atmospheric dispersion around Ki-Jang research reactor using the Lagrangian Gaussian puff dispersion model

  • Choi, Geun-Sik;Lim, Jong-Myoung;Lim, Kyo-Sun Sunny;Kim, Ki-Hyun;Lee, Jin-Hong
    • Nuclear Engineering and Technology
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    • v.50 no.1
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    • pp.68-79
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    • 2018
  • The Ki-Jang research reactor (KJRR), a new research reactor in Korea, is being planned to fulfill multiple purposes. In this study, as an assessment of the environmental radiological impact, we characterized the atmospheric dispersion and deposition of radioactive materials released by an unexpected incident at KJRR using the weather research and forecasting-mesoscale model interface program-California Puff (WRF-MMIF-CALPUFF) model system. Based on the reproduced three-dimensional gridded meteorological data obtained during a 1-year period using WRF, the overall meteorological data predicted by WRF were in agreement with the observed data, while the predicted wind speed data were slightly overestimated at all stations. Based on the CALPUFF simulation of atmospheric dispersion (${\chi}/Q$) and deposition (D/Q) factors, relatively heavier contamination in the vicinity of KJRR was observed, and the prevailing land breeze wind in the study area resulted in relatively higher concentration and deposition in the off-shore area sectors. We also compared the dispersion characteristics between the PAVAN (atmospheric dispersion of radioactive release from nuclear power plants) and CALPUFF models. Finally, the meteorological conditions and possibility of high doses of radiation for relatively higher hourly ${\chi}/Q$ cases were examined at specific discrete receptors.

Research on Acceleration Mechanism of Inflight Particle and Gas Flow Effect for the Velocity Control in Vacuum Kinetic Spray Process (진공상온분사(VKS) 공정에서의 비행입자 가속 기구 및 속도제어를 위한 가스 유량 효과에 관한 연구)

  • Park, Hyungkwon;Kwon, Juhyuk;Lee, Illjoo;Lee, Changhee
    • Korean Journal of Materials Research
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    • v.24 no.2
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    • pp.98-104
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    • 2014
  • Vacuum kinetic spray(VKS) is a relatively advanced process for fabricating thin/thick and dense ceramic coatings via submicron-sized particle impact at room temperature. However, unfortunately, the particle velocity, which is an important value for investigating the deposition mechanism, has not been clarified yet. Thus, in this research, VKS average particle velocities were derived by numerical analysis method(CFD: computational fluid dynamics) connected with an experimental approach(SCM: slit cell method). When the process gas or powder particles are accelerated by a compressive force generated by gas pressure in kinetic spraying, a tensile force generated by the vacuum in the VKS system accelerates the process gas. As a result, the gas is able to reach supersonic speed even though only 0.6MPa gas pressure is used in VKS. In addition, small size powders can be accelerated up to supersonic velocity by means of the drag-force of the low pressure process gas flow. Furthermore, in this process, the increase of gas flow makes the drag-force stronger and gas distribution more homogenized in the pipe, by which the total particle average velocity becomes higher and the difference between max. and min. particle velocity decreases. Consequently, the control of particle size and gas flow rate are important factors in making the velocity of particles high enough for successful deposition in the VKS system.

The Fabrication of Porous Nickel Oxide Thin Film using Anodization Process for an Electrochromic Device

  • Lee, Won-Chang;Choe, Eun-Chang;Hong, Byeong-Yu
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.407.1-407.1
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    • 2016
  • Electrochromism is defined as a phenomenon which involves persistently repeated change of optical properties between bleached state and colored state by simultaneous injection of electrons and ions, sufficient to induce an electrochemical redox process. Due to this feature, considerable progress has been made in the synthesis of electrochromic (EC) materials, improvements of EC properties in EC devices such as light shutter, smart window and variable reflectance mirrors etc. Among the variable EC materials, solid-state inorganics in particular, metal oxide semiconducting materials such as nickel oxide (NiO) have been investigated extensively. The NiO that is an anodic EC material is of special interest because of high color contrast ratio, large dynamic range and low material cost. The high performance EC devices should present the use of standard industrial production techniques to produce films with high coloration efficiency, rapid switching speed and robust reversibility. Generally, the color contrast and the optical switching speed increase drastically if high surface area is used. The structure of porous thin film provides a specific surface area and can facilitate a very short response time of the reaction between the surface and ions. The large variety of methods has been used to prepare the porous NiO thin films such as sol-gel process, chemical bath deposition and sputtering. Few studies have been reported on NiO thin films made by using sol-gel method. However, compared with dry process, wet processes that have the questions of the durability and the vestige of bleached state color limit the thin films practical use, especially when prepared by sol-gel method. In this study, we synthesis the porous NiO thin films on the fluorine doped tin oxide (FTO) glass by using sputtering and anodizing method. Also we compared electrical and optical properties of NiO thin films prepared by sol gel. The porous structure is promised to be helpful to the properties enhancement of the EC devices.

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