• Title/Summary/Keyword: heating rates

Search Result 461, Processing Time 0.027 seconds

Effect of Microstructure on Conductivity of W-Cu Composite (W-CU 복합재료의 전도도에 미치는 미세조직의 영향)

  • Lee Young Jung;Park Kwang Hyun;Lee Byung Hoon;Kim Deok-Soo;Kim Young Do
    • Korean Journal of Materials Research
    • /
    • v.15 no.2
    • /
    • pp.85-88
    • /
    • 2005
  • [ $W-15wt.\%$ ] Cu nanocomposite powders are fabricated by ball-milling and subsequent hydrogen-reduction. The compacted parts of $W-15wt.\%Cu$ nanocomposite powders were sintered at $1200^{\circ}C$ for 1 h with various heating rates of 5 and $20^{\circ}C/min$. The homogeneity of the sintered microstructures was evaluated through homogeneity index by the standard deviation of Victor's hardness test. The W-W contiguities were calculated by using Voronoi diagrams. The sintered microstructure with the heating rate of $20^{\circ}C/min$ was more homogeneous and had lower W-W contiguity than that of $5^{\circ}C/min$. The microstructural homogeneity was directly related to the W-W contiguity. Thermal conductivity of the sintered parts with the heating rate of $20^{\circ}C/min$ was higher than that with heating rate of $5^{\circ}C/min$. This phenomenon indicates that the thermal conductivity is affected by the W-W contiguity resulting from the homogeneity of the sintered microstructure.

Influence of Heating Rate and Temperature on Carbon Structure and Porosity of Activated Carbon Spheres from Resole-type Phenolic Beads

  • Singh, Arjun;Lal, Darshan
    • Carbon letters
    • /
    • v.10 no.3
    • /
    • pp.181-189
    • /
    • 2009
  • Activated carbon spheres (ACS) were prepared at different heating rates by carbonization of the resole-type phenolic beads (PB) at $950^{\circ}C$ in $N_2$ atmosphere followed by activation of the resultant char at different temperatures for 5 h in $CO_2$ atmosphere. Influence of heating rate on porosity and temperature on carbon structure and porosity of ACS were investigated. Effect of heating rate and temperature on porosity of ACS was also studied from adsorption isotherms of nitrogen at 77 K using BET method. The results revealed that ACS have exhibited a BET surface area and pore volume greater than $2260\;m^2/g$ and $1.63\;cm^3/g$ respectively. The structural characteristics variation of ACS with different temperature was studied using Raman spectroscopy. The results exhibited that amount of disorganized carbon affects both the pore structure and adsorption properties of ACS. ACS were also evaluated for structural information using Fourier Transform Infrared (FTIR) Spectroscopy. ACS were evaluated for chemical composition using CHNS analysis. The ACS prepared different temperatures became more carbonaceous material compared to carbonized material. ACS have possessed well-developed pores structure which were verified by Scanning Electron Microscopy (SEM). SEM micrographs also exhibited that ACS have possessed well-developed micro- and meso-pores structure and the pore size of ACS increased with increasing activation temperature.

Evaluation of Energy Consumption through Field Measurement at the Apartment Housing Unit Using Dynamic Flow Rate Balancing (실물실험을 통한 다이나믹 유량밸런싱 적용 공동주택 세대의 에너지소비량 평가)

  • Ryu, Seong-Ryong;Cheong, Chang-Heon;Cho, Hyun
    • Journal of the Korean Society for Geothermal and Hydrothermal Energy
    • /
    • v.12 no.4
    • /
    • pp.15-20
    • /
    • 2016
  • Even though the control device of the heating system works well, insufficient water flow rates can degrade control performance and thermal comfort. The water flow rate should be adjusted appropriately to cope with the heating load of each zone. In order to solve these problems, a new balancing concept 'dynamic balancing' was proposed where a balancing valve opening can be automatically modulated according to the heating condition of the room. This study analyzed the effects of dynamic balancing upon indoor thermal environment and energy consumption in a radiant floor heating system through field measurement. Under part-load conditions, the use of a dynamic balancing is a more effective method to reduce energy consumption and to prevent a cavitation. Dynamic balancing is able to help boost the temperature of a room in the start-up period.

Drying Characteristics of Plating Sludge by Microwave (마이크로파 가열에 의한 도금슬러지 건조특성)

  • 문경환;손종렬;김덕찬
    • Journal of environmental and Sanitary engineering
    • /
    • v.13 no.1
    • /
    • pp.9-15
    • /
    • 1998
  • Microwave heating and drying processes have been well established in various industrial applications. Feasibilities of successful application of microwave drying to many material have been shown on the laboratory or pilot-plant scale. The microwave drying behavior of plating sludge are considered in this paper. The plating sludge containing 70%, 80% and 90% water exposed to microwave power at 2,450 MHz, 700W. An experimental microwave drying apparatus was designed and constructed to monitor weight loss during drying. By studying the drying characteristic curve, the moisture in sludge was almost classified into two categories : free moisture and intestinal moisture. And the critical moisture contents at which the drying rate ceases to be constant were from 10.1 to 10.5%. A simple drying model is proposed which may be used to describe drying behavior of plating sludge. The constant rate and the falling rate periods in microwave drying were addressed separately. From the eqation of constant rate period the drying rate constants decreased exponentially with increasing depth. Microwave heating compared with conventional heating offered higher heating rates from 9 to 16 times. Therefore, microwave drying process can be effective in removing moisture from plating sludge.

  • PDF

Variations in Ginsenosides of Raw Ginseng According to Heating Temperature and Time

  • Kim, Chan Joong;Kim, Bo Mi;Kim, Cheon Suk;Baek, Jung Yeon;Jung, In Chan
    • Journal of Pharmacopuncture
    • /
    • v.23 no.2
    • /
    • pp.79-87
    • /
    • 2020
  • Objectives: Ginsenosides found in ginseng, and the hydrolysates derived from their conversion, exhibit diverse pharmacological characteristics [1]. These have been shown to include anti-cancer, anti-angiogenic, and anti-metastatic effects, as well as being able to provide hepatic and neuroprotective effects, immunomodulation, vasodilation, promotion of insulin secretion, and antioxidant activity. Therefore, the purpose of this study was to examine how quickly the ginsenosides decompose and what kinds of degradation products are created under physicochemical processing conditions that don't involve toxic chemicals or other treatments that may be harmful. Methods: The formation of ginsenoside-Rg2 and ginsenoside-Rg3 was examined. These demonstrated diverse pharmacological effects. Results: We also investigated physicochemical factors affecting their conversion. The heating temperatures and times yielding the highest concentration of ginsenosides (-Rb1, -Rb2, -Rc, -Rd, -Rf, -Rg1, and -Re) were examined. Additionally, the heating temperatures and rates of conversion of these ginsenosides into new 'ginseng saponins', were examined. Conclusion: In conclusion, obtained provide us with effective technology to control the concentration of both ginsenosides and the downstream converted saponins (ginsenoside-Rg2, Rg3, Rg5, and Rk1 etc.), as well as identifying the processing conditions which enable an enrichment in concentration of these compounds.

An Investigation on the Crystal Growth Studies and Emission line shape in $Er^{3+}$-doped Sodium Tellurite Glasses

  • Joshi, Purushottam;Jha, Animesh
    • Ceramist
    • /
    • v.10 no.3
    • /
    • pp.67-74
    • /
    • 2007
  • Crystallisation kinetics of the erbium doped soda-tellurite glasses were studied using the differential thermal analysis (DTA) and differential scanning calorimetery (DSC) techniques. The DTA curves in the temperature range of 350 K to 650 K were obtained from isochronal heating rates, chosen in the range of 2 to 20 K/min. DSC isothermal curves were used to calculate the fraction of crystals formed on reheating. The apparent activation energies for devitrification were derived by measuring the shifts in the values of $T_g$ and $T_x$ with heating rates, using the Kissinger method. The derived values of apparent activation energies for isochronal and isothermal methods varied in the range of $190-204\;{\pm}\;5\;kJ\;mol^{-1}$. The X-ray powder diffraction analysis of heat treated and transparent samples showed the presence of nano-scale size sodium-tellurite crystals. These crystallites were found to have a strong influence on the full width of half maxima of the transition in $Er^{3+}:\;^4I_{13/2}{\rightarrow}^4I_{15/2}$, which extended from 70 nm in the vitreous materials to 132 nm in glass-ceramic materials.

  • PDF

Effect of Thawing Methods and Storage Periods on the Quality of Frozen Cooked Rice

  • Oh, Myung-Suk
    • Preventive Nutrition and Food Science
    • /
    • v.3 no.3
    • /
    • pp.234-240
    • /
    • 1998
  • This study attempted to determine the effect of various thawing methods and storage periods on the quality of froen cooked rice. Frozen cooked rice was thawed at four different methods, such as pressure cooking, conventional cooking, microwave heating and thawing at room temperature after 10 days, 30days and 90 days frozen storage. We conducted a physico-chemical analysis (moisture content, dehydration rates, degree of gelatinization, color value and texture) and sensory evalution on the frozen-thawed cooked rice. The study showed that there were no significant differences on the quality characteristics of frozen-thawed cooked rice during the storage period of 90 days. However, the thawing method of pressure cooking caused high moisture content, rapid dehydration rates, and a high degree of gelatinization on the cooked rice. Thus, the desirabililty for the rice diminished becaused of the excess moisture content and the change of appearance and testure in the rice due to the high temperature. There were similiar quality characteristics to the cooked rice after forzen-thawing whether by conventional cooking or by microwave heating and just after cooking. Thawing at room temperature also caused a significant decrease in quality characteristics.

  • PDF

Thermogravimetric and Fourier Transform Infrared Analysis of Switchgrass Pyrolysis (스위치그라스 열분해에 대한 TGA-FTIR 분석)

  • Lee, Seong-Beom;Fasina, Oladiran O.
    • Journal of Biosystems Engineering
    • /
    • v.34 no.1
    • /
    • pp.44-49
    • /
    • 2009
  • This study was conducted to investigate the pyrolysis characteristics of switchgrass using TGA-FTIR instrument. Switchgrass is a high yielding perennial grass that has been designated as a potential energy crop, because of its high energy value. Ground switchgrass were pyrolysed at different heating rates of 10, 20, 30, and $40^{\circ}C/min$ in a TGA-FTIR instrument. The thermal decomposition characteristics of switchgrass were analyzed, and the gases volatilized during the experiment were identified. The thermal decomposition of switchgrass started at approximately $220^{\circ}C$, followed by a major loss of weight, where the main volatilization occurred, and the thermal decomposition was essentially completed by $430^{\circ}C$. The pyrolysis process was found to compose of four stages; moisture evaporation, hemicellulose decomposition, cellulose decomposition, and lignin degradation. The peak temperatures for hemicellulose decomposition ($306^{\circ}C$ to $327^{\circ}C$) and cellulose decomposition ($351^{\circ}C$ to $369^{\circ}C$) were increased with greater heating rates. FTIR analysis showed that the following gases were released during the pyrolysis of switchgrass; $CO_2$, CO, $CH_4$, $NH_3$, COS, $C_{2}H_{4}$, and some acetic acid. The most gas species were released at low temperature from 310 to $380^{\circ}C$, which was corresponding well with the observation of thermal decomposition.

Determination of Thermal Decomposition Parameters for Ablative Composite Materials (삭마용 내열 복합재료의 열분해 반응인자 결정)

  • Kim Yun-Chul
    • Proceedings of the Korean Society of Propulsion Engineers Conference
    • /
    • 2005.11a
    • /
    • pp.22-25
    • /
    • 2005
  • The thermal degradation of carbon/phenolic composite have been studied at high temperature by using thermogravimetric (TGA). A heating .ate of 5, 10, 15, 30 and $50^{\circ}C/min$ was used for the determination of thermal decomposition parameters of composite materials at high-temperature service. It has been shown that as the heating rates is increased, the peak decomposition rates are occur at higher temperature. Based on results of thermogravimetric analysis, the pyrolysis process is analyzed and physical and mathematical models for the process are proposed. The thermal analysis also has been conducted using transient heat conduction and the in-depth temperature distribution and the density profile were evaluated along the solid rocket nozzle. As a future effort the thermal decomposition parameter determined in this investigation will be used as input to thermal and mechanical analysis when subjected to solid rocket propulsion environment.

  • PDF

A Study on the Characteristics of Cylinder Wake Placed in Thermally Stratified Flow (IV) -On the Cylinder Wake with Various Heating Rates- (열성층유동장에 놓인 원주후류의 특성에 대한 연구 (4) -가열량의 변화에 따른 원주후류에 대하여-)

  • 김경천;정양범
    • Transactions of the Korean Society of Mechanical Engineers
    • /
    • v.19 no.5
    • /
    • pp.1340-1350
    • /
    • 1995
  • The effects of thermal stratification on the flow past a heated circular cylinder with various heating rates were examined in a wind tunnel. Turbulent intensities, r.m.s.values of temperature and turbulent convective heat flux distributions in the cylinder wakes with and without thermal stratification were measured by using a hot-wire and cold-wire combination probe. The phase averaging method was also used to estimate coherent contributions to the turbulent flow field in the near wake. The results show that the scalar mixing process is very different according to the mean temperature fields especially in the upper part of the wake. The coherent structure of the temperature field makes a large contribution to the time mean value like velocity components. However, the coherency of the temperature fluctuation is very different with the change of mean temperature fields, though the velocity coherent motions are quite similar in all experimental conditions.