• Korean Chemical Engineering Research
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• v.46 no.1
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• pp.200-204
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• 2008

The curing kinetics of diglycidyl ether of bisphenol F (DGEBF) with an asymmetric cycloaliphatic amine curing agent were examined by thermal analysis in both isothermal and dynamic curing conditions. From the residual curing of the samples partially cured in isothermal condition and from the dynamic curing with various heating rates, it was found that there exist two kinds of reactions such as at low temperature and at high temperature regions. It was thus also found that the cure parameters obtained from the isothermal curing kinetic model hardly estimate experimental results for a degree of cure larger than 0.6. The activation energies and frequency factors of these two kinds of reactions were obtained from the dynamic curing experiments with various heating rates. From the curing analysis, it was verified that the total cure kinetics for low degrees of cure is dominated by the cure reaction in the low temperature region.

• Journal of the Korea Institute of Building Construction
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• v.12 no.3
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• pp.291-298
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• 2012

For cold weather concreting, frost damage at early age is generated in the concrete, and problems such as delaying of setting and hardening and lowering of strength manifestation emerge due to the low outside air temperature at the early stage of pouring, making the selection of an effective curing method critically important. Unfortunately, the tent sheet currently used as the curing film for heating insulation at work sites, not only has the problems of inferior permeability and extremely deteriorated airtightness, but a phenomenon of continuous fracturing is also generated along the direction of fabric of the material itself, presenting difficult circumstances for maintaining adequate curing temperature. The aim of this study was to develop an improved bubble sheet type curing film for heating insulation of cold weather concrete by combining mesh-tarpaulin, which has excellent tension properties, with bubble sheet, which offers superior insulation performance. The analysis showed that the improved curing film in which BBS1 is stacked to MT was a suitable replacement for curing films currently in use, as it has better permeability, tension property, and insulation performance than the T type film used at work sites today.

• Proceedings of the Korea Concrete Institute Conference
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• 2001.05a
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• pp.807-812
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• 2001

This study is peformed for checking the limitation and application of each curing/heating methods on cold-weathering mat foundation construction, considering temperature control, early strength security and temperature declination range limit, by means of concrete material properties and thermal analysis technique that were published previously. In the result of this analysis, we checked the open air temperature and mat depth that are possible to apply each curing/heating methods on cold-weathering construction and found curing/heating time of each methods that is able to prevent early aged freezing damage and thermal crack

• Journal of the Korea Institute of Building Construction
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• v.3 no.4
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• pp.87-94
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• 2003

This study is to investigate the temperature hysteresis and development of compressive strength due to the curing conditions and to evaluate the optimum curing condition of test specimens showing the same development of strength to that of real structures in cold weather. The results of temperature curve with curing conditions in mock-up tests showed the trend of decrease plain concrete with insulation form, plain concrete with heating, concrete with accelerator for freeze protection, and control concrete in turn. The strength development of plain concrete of inside and outside of shelter showed the very slow strength gains due to early freezing, but that of concrete with accelerator for freeze protection showed the gradual increase of strength with time. From this, it is clear that accelerator for freeze protection has the effects of refusing the freezing temperature and accelerating the hardening under low temperature. Strength test results of small specimens embedded in members and located in insulation boxes at the site are similar to that of cores drilled from the members at the same ages, thus it is clear that these curing methods are effective for evaluating in-place concrete strength

• Journal of the Korean Recycled Construction Resources Institute
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• v.7 no.3
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• pp.85-90
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• 2012

In this study, temperature profile of the fly ash concrete were studied in accordance with the change of heating curing method combination for the slab concrete in order to develop efficient protection method of the concrete subjected to $-20^{\circ}C$. The slab concretes with the size of $1200mm{\times}600mm{\times}200mm$ were fabricated with W/B of 50% and exposed to $-20^{\circ}C$ for 7 days. Five different combinations of heat curing methods were applied to the slab concrete specimen; two combinations of heat supplying by electrical heater and surface heat insulation material such as polyethylene film and quadrupled layer bubble sheet based on heat enclosure installment; three combinations of heating coil embedment and surface heat insulation materials such as polyethylene film, sawdust and quadrupled layer bubble sheet based on heat enclosure installment. Test results showed that by applying both heating coil and bubble sheet and heat enclosure, the concrete exposed to $-20^{\circ}C$ can be effectively protected from early-age frost damage.

• Proceedings of the Korean Geotechical Society Conference
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• 2002.03a
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• pp.305-312
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• 2002

To estimate the effects of lime and cement on the surplus soil, the engineering properties of the marine deposited clay and the fresh water clay were analyzed. The specimen were prepared under several curing conditions, namely, underwater curing, wet condition curing and underwater curing after heating. Unconfined compression strength were estimated after 7, 14, 28 and 60 days, respectively. The strength were steeply increased with time until first 14 days. Specially the increase of the strength of the heated soil were large.

• Proceedings of the Korean Society of Crop Science Conference
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• 1989.02a
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• pp.108-109
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• 1989

• Proceedings of the KIEE Conference
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• 2002.04a
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• pp.71-73
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• 2002

The Induction heating is used in various industry and ever-increasing number of applications. The heating roll, which is a kind of induction heating, widely used in curing of coatings and fiber industry. In this papaer, we analized thermal characteristic of induction heating roll by three dimensional eddy-current analysis. Using this analytic results, We could predict the thermal distribution of induction heating roll.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1989.06a
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• pp.43-46
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• 1989

Epoxy, noticed as a new insulation material for electrical equipments, may become an excellent cured material from the crosslink reaction with some curing agents and accelerators. The characteristics of cured epoxy is determined by the method of lattice formation according to curing method. The purpose of this paper, varing the process of lattice formation by various surrounding temperatures and heating time during the curing process, is to obtain the optimum cured condition for electrical insulation from the results of investigation on the physical and dielectric properties of cured epoxy. In this investigation, it is found that the excessive temperature and heating time brings on the growth of metamorphic methyl and the insulating properties of cured epoxy is decreased by this phenomenon. As a result, it is concluded that the optimum dielectric characteristics can be obtained when cured at a curing temperature at 14$0^{\circ}C$ for one hour.

• Design & Manufacturing
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• v.17 no.1
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• pp.1-5
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• 2023

In multi-material injection molding, since two or more materials with different process conditions are used, it is essential to maximize process efficiency by operating the cooling or heating system to a minimum. In this study, Liquid silicone rubber (LSR) that can be cured at a low temperature suitable for the multi-material injection molding was selected and the cure behavior according to the process conditions was analyzed through differential scanning calorimetry (DSC). Dynamic measurement results of DSC with different heating rate were obtained, and through this, the total heat of reaction when the LSR was completely cured was calculated. Isothermal measurement results of DSC were derived for 60 minutes at each temperature from 80 ℃ to 110 ℃ at 10 ℃ intervals, and the final degree of cure at each temperature was calculated based on the total heat of reaction identified from the Dynamic DSC measurement results. As the result, it was found that when the temperature is lowered, the curing start time and the time required for the curing reaction increase, but at a temperature of 90 ℃ or higher, LSR can secure a degree of cure of 80% or more. However, at 80 ℃., it was found that not only had a relatively low degree of curing of about 60%, but also significantly increased the curing start time. In addition, in the case of 110 ℃, the parameters were derived from experimental result using the Kamal kinetic model.