• Title/Summary/Keyword: heat treatment processing

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Evaluation of the Oral Acute Toxicity of Black Ginseng in Rats

  • Lee, Mi-Ra;Oh, Chang-Jin;Li, Zheng;Li, Jing-Jie;Wang, Chun-Yan;Wang, Zhen;Gu, Li-Juan;Lee, Sang-Hwa;Lee, Jae-Il;Lim, Beong-Ou;Sung, Chang-Keun
    • Journal of Ginseng Research
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    • v.35 no.1
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    • pp.39-44
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    • 2011
  • We studied the acute oral toxicity of black ginseng (BG) produced by heat process in rats. Single acute BG extract doses of 0, 5, 10, and 15 g/kg dissolved in saline were administered by oral gavage and the animals were kept under observation for 14 days. The single administration of BG extract up to 15 g/kg did not produce mortality, behavioral change or abnormal clinical signs in the rats. These results indicated that the oral $LD_{50}$ of the BG extract in the rats is higher than 15 g/kg. Compared to the control group, no treatment-related biologically significant effects of BG extract were noted in the measurements of the body weight or food intake. At the end of the period, the biochemical parameters and hematological parameters were analyzed in the plasma and blood. A histopathological examination of the liver and kidney was also conducted. Only the blood nitrogen urea and potassium levels in the biochemical indices showed significant differences at 10 and 15 g/kg doses of BG extract compared to the control group. These changes were not considered to be due to the toxicity. None of the other clinical chemistry parameters were affected. Therefore, these results indicate that the BG by heat processing is virtually nontoxic.

Direct Microwave Sintering of Poorly Coupled Ceramics in Electrochemical Devices

  • Amiri, Taghi;Etsell, Thomas H.;Sarkar, Partha
    • Journal of Electrochemical Science and Technology
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    • v.13 no.3
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    • pp.390-397
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    • 2022
  • The use of microwaves as the energy source for synthesis and sintering of ceramics offers substantial advantages compared to conventional gas-fired and electric resistance furnaces. Benefits include much shorter processing times and reaching the sintering temperature more quickly, resulting in superior final product quality. Most oxide ceramics poorly interact with microwave irradiation at low temperatures; thus, a more complex setup including a susceptor is needed, which makes the whole process very complicated. This investigation pursued a new approach, which enabled us to use microwave irradiation directly in poorly coupled oxides. In many solid-state electrochemical devices, the support is either metal or can be reduced to metal. Metal powders in the support can act as an internal susceptor and heat the entire cell. Then sufficient interaction of microwave irradiation and ceramic material can occur as the sample temperature increases. This microwave heating and exothermic reaction of oxidation of the support can sinter the ceramic very efficiently without any external susceptor. In this study, yttria stabilized zirconia (YSZ) and a Ni-YSZ cermet support were used as an example. The cermet was used as the support, and a YSZ electrolyte was coated and sintered directly using microwave irradiation without the use of any susceptor. The results were compared to a similar cell prepared using a conventional electric furnace. The leakage test and full cell power measurement results revealed a fully leak-free electrolyte. Scanning electron microscopy and density measurements show that microwave sintered samples have lower open porosity in the electrode support than conventional heat treatment. This technique offers an efficient way to directly use microwave irradiation to sinter thin film ceramics without a susceptor.

Preliminary Acrylamide Monitoring of Domestic Heat-Treated Food Products (국내 가열식품군의 아크릴아마이드 예비 모니터링)

  • Park, Jae-Young;Kim, Hye-Young;Lee, Jong-Ok;Chung, So-Young;So, Yu-Sub;Kim, Chang-Min;Oh, Sang-Suk
    • Korean Journal of Food Science and Technology
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    • v.35 no.4
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    • pp.748-751
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    • 2003
  • Acrylamide is considered as potential carcinogen and genotoxicant. Swedish National Food Administration reported that acrylamide was detected in heat treated starch rich food products. Acrylamide formation during food processing was confirmed by researchers of other countries including UK, Norway, Japan, Switzerland, and United States. It is noticed that the formation of acrylamide in potato products was greater than other food products. It may be due to high concentration of asparagine and glucose in potato products comparing to those of other food products. Interaction between asparagine and glucose during heat treatment resulted in acrylamide formation via Maillard reaction. Analytical method (LC-MS/MS) adopted by FDA was performed to monitor acrylamide concentrations in domestic food products. Acrylamide quantitation in several food categories, such as raw materials, boiled foods, fried foods, hardtacks, breads, breakfast cereals, potato chips, french fries, biscuits, and others, were carried out.

Impact of Thermal and Nonthermal Technologies in Milk Processing (우유의 가열 및 비가열 살균 기술에 관한 연구 동향)

  • Park, Jung Geun;Lee, Yeo Jin;Yoon, Joon Yong;Om, Ae Son
    • Journal of Dairy Science and Biotechnology
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    • v.33 no.3
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    • pp.223-229
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    • 2015
  • Milk is a food with high nutritional value as it contains abundant water, proteins, vitamins, lactose, fat, minerals, enzymes, etc. However, in order to make milk suitable for intake, it should be thermally treated to eliminate microbiologically hazardous factors. Heat treatment is an essential sanitation process for milk, but various precautions must be taken in order to process and preserve it. Therefore, various techniques should be developed to minimize the nutrient loss and to ensure that milk is safe for consumption, conservation, and distribution. However, the existing thermal pasteurization methods are harmful and increase the nutrient loss; moreover, no new thermal pasteurization methods are being researched that are safe for the human health and minimize the nutrient loss. Hence, this study aims to review new processes for thermal (low temperatures) and no thermal pasteurization methods that can minimize the nutrient loss during milk pasteurization.

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Effect of the Initial Microstructure of Low Temperature Superconducting Monowire on Critical Current Density (초기 미세조직에 따른 저온 초전도 모노선재의 임계전류밀도 분석)

  • Kim, H.R.;Oh, Y.S.;Kim, S.J.;Lee, H.W.;Kim, J.H.;Kang, S.H.
    • Transactions of Materials Processing
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    • v.29 no.1
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    • pp.37-43
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    • 2020
  • Increasing the critical current density of superconducting wire is one of the difficult challenges in the field of superconductivity. It is well known that the higher volume fraction of uniformly dispersed α-Ti is able to enhance the critical current density of superconducting material NbTi because α-Ti serves as a flux pinning center. The volume fraction of α-Ti highly depends on the grain size of NbTi because α-Ti precipitates at the grain boundaries or triple points. For this purpose, we investigated the effect of initial microstructures of NbTi obtained from hot rolling in various temperature conditions on the critical current density. In addition, subsequent heat treatment was assigned to precipitate α-Ti and groove rolling/cold drawing was adopted to produce a wire with a diameter of about 1.0 mm. It was observed that the band structure was formed after hot rolling at 500~600℃. It was also found that the volume fraction of α-Ti after hot rolling at 500~600℃ was higher and it led to the highest critical current density.

WO3 Fabrication and Thermal Spray Coating of WC-Co using Recycled Ammonium Paratungstate (APT) (재활용 APT를 이용한 WO3 제조와 WC-Co 의 용사코팅)

  • Chung, J. K.;Kim, S. J.;On, J. H.;Moon, H. S.;Pee, J. H.;Ha, T. K.;Park, S. Y.
    • Transactions of Materials Processing
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    • v.24 no.4
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    • pp.287-292
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    • 2015
  • The possibility of chemical precipitation for recycled ammonium paratungstate (APT) was studied. WO3 particles were synthesized by chemical precipitation method using a 1:2 weight ratio of APT:DI-water. At the 500℃ sintering temperature, the X-ray diffraction results showed that APT completely decomposed to WO3. For the granulated powder WC-Co, vacuum heat treatment at proper temperatures increases tap density and flow-ability. Hardness of the WC-Co thermal spray coating layer was measured in the range HV 831~1266. Spray conditions for the best characteristic values were an oxygen flow rate=1500 scfh, a fuel flow rate = 5.25gph and a gun distance = 320mm.

Fabrication of Ultra Small Size Hole Array on Thin Metal Foil (초미세 금속 박판 홀 어레이 가공)

  • Rhim S. H.;Son Y. K.;Oh S. I.
    • Transactions of Materials Processing
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    • v.15 no.1 s.82
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    • pp.9-14
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    • 2006
  • In the present research, the simultaneous punching of ultra small size hole of $2\~10\;{\mu}m$ in diameter on flat rolled thin metal foils was conducted with elastic polymer punch. Workpiece used in the present investigation were the rolled pure copper of $3{\mu}m$ in thickness and CP titanium of 1.5fm in thickness. The metal foils were punched with the dies and arrays of circular and rectangular holes were made. The process set-up is similar to that of the flexible rubber pad farming or Guerin process. Arrays of holes were punched successfully in one step forming. The punched holes were examined in terms of their dimensions. The effects of the wafer die hole dimension and heat treatment of the workpiece on ultra small size hole formation of the thin foil were discussed. The process condition such as proper die shape, pressure, pressure rate and diameter-thickness ratio (d/t) were also discussed. The results in this paper show that the present method can be successfully applied to the fabrication of ultra small size hole away in a one step operation.

Manufacturing System of Centrifugal Cast Metal Bearing by Dehydrogenation (탈수소 열처리 공정에 의한 원심주조 메탈베어링의 제조 시스템)

  • Kim, Jeung-Hun;Kim, Chung-Gu;Byen, Jea-Young;Lee, Eun-Suk;Yang, Ji-Yung;Choi, Won-Sik
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.5
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    • pp.111-117
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    • 2020
  • Centrifugal casting is suitable for producing hollow-products using centrifugal force. Bush type metal bearings are the key parts that facilitate the rotational movement of various machinery. Metal bearings produced by conventional centrifugal casting machines show rotational imbalance. Therefore, after injecting a large amount of material, the product's precision is secured in the secondary processing. Rotational imbalance is caused by the force acting on the rotary disc plate. In order to minimize rotational imbalance, NASTRAN was used for the optimal design and structural analysis. It was concluded that the rotating plate of the conventional centrifugal casting machine should be prevented from tilting. For this purpose, the location & thickness of the stiffeners were obtained through the optimum design. In the conventional centrifugal casting machine, both ends of the product are lower in temperature than the center part, so internal stress occurs. This solves this problem by inserting a heating coil into the rotating plate.

Study of Material Properties of High Strength Microalloyed Steel for Cold Forming by Controlled Rolling and Cooling Technology (제어압연.제어냉각기술로 제조된 냉간성형용 비조질강의 소재특성)

  • Kim, N.G.;Park, S.D.;Kim, B.O.;An, J.Y.;Choi, H.J.
    • Transactions of Materials Processing
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    • v.15 no.8 s.89
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    • pp.603-608
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    • 2006
  • The main purpose of the present study has been placed on investigating the mechanical properties and microstructures of C-Si-Mn-V steels for cold forming manufactured by controlled rolling and cooling technology. The steels were manufactured in electric arc furnace (EAF) and casted to $160{\times}160mm$ billet. The billets were reheated in walking beam furnace and rolled to coil, the stocks were rolled by Controlled Rolling and Cooling Technology (CRCT), so rolled at low temperature by water spraying applied in rolling stage and acceleratly cooled before coiling. Rolled coils were cold drawed to the degree of 16%, 27% of area reduction respectively without heat treatment. Microstructual observation, tensile test, compression test and charpy impact tests were conducted. The mechanical properties of the steels were changed by area reduction of cold drawing and it is founded that there are optimum level of cold drawing to minimize compression stress for these steels. From the result of this study, it is conformed that $80kg_{f}/mm^{2},\;90kg_{f}/mm^{2}$ grade high strength microalloyed steel for cold forming are developed by accelerated cooling and optimum cold drawing.

Hot Forging of an Engine Piston using Control Cooling (제어냉각 장치를 이용한 엔진피스톤 열간단조 공정에 관한 연구)

  • Lee, S. I.;Choi, D. H.;Lee, J. H.
    • Transactions of Materials Processing
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    • v.24 no.6
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    • pp.411-417
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    • 2015
  • The piston engine is an essential component in automobiles. Since the piston is used in a high temperature and high pressure environment, the piston needs to be manufactured to achieve high strength and high durability. In addition, cost reduction is also an important consideration. In conventional forging, an additional heat treatment after hot forging is necessary to ensure proper mechanical properties for heavy-duty engine pistons. The newly developed manufacturing method lowers production costs by saving manufacturing time and reduces energy consumption. The current paper describes the hot forging of an engine piston made from 38MnSiVS5 micro-alloyed steel using controlled cooling. The finite element analysis was used to check for possible problems and suitable press capacity. Hot forging experiments were then conducted on a 2500tons crank press to evaluate feasibility of the proposed material and process. To check the mechanical properties after hot forging, the forged specimens were tensile tested, and the microstructures were examined in order to compare the results with the conventionally forged material. The skirt region of the as-forged 38MnSiVS5 piston showed better material properties compared to the conventional material. In addition, the total production time was reduced by about 80% as compared to conventional forging.