• Title/Summary/Keyword: heat cured

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Comparison of bond strength between denture base resin and reline resin (의치상 레진과 이장 레진 간의 결합강도 비교)

  • Geum, Young-Hee;Kim, Busob
    • Journal of Technologic Dentistry
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    • v.39 no.3
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    • pp.161-167
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    • 2017
  • Purpose: We compare the bond strength of heat-cured PMMA of Lucitone 199 and QC-20 and Tokuyama Rebase Resin of self-cured resin, which are widely used and well accepted in clinical practice. In order to test the mechanical bonding and chemical bonding, we will compare the bond strength between EstheShot Bright, Smiletone, Repair and Rebase resins. Methods: The denture base resin used in this study was PMMA heat-cured QC-20 and Lucitone 199, polyamide resin EstheShot Bright, Smiletone. And Two types of self-curing Rapid Repair and Tokuyama Rebase were used as resection resins. To measure the bond strength, the denture specimens were fabricated in the size of $10{\times}64{\times}3.5mm$ as instructed by the manufacturer. A surface treatment agent was applied to the cut surfaces of each denture specimen, and the specimens were placed in a preformed silicone mold, and autoclaved excimer resins were prepared. The bending strength of the fabricated specimens was measured using a universal testing machine (STM-5, United Calibration Co., U.S.A.) to measure the three-point bending strength. Results: In both polycarbonate and polyacetal resin, a special resin surface treatment agent showed higher bonding strength than the resin surface treatment agent(p<0.05). Regardless of the type of surface treatment, polycarbonate showed higher bond strength than polyacetal resin(p<0.05). Conclusion: It is considered desirable to use a special surface treating agent for the thermoplastic denture base resin such as polycarbonate and polyacetal resin.

Bonding of nano-modified concrete with steel under freezing temperatures using different protection methods

  • Yasien, A.M.;Bassuoni, M.T.
    • Computers and Concrete
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    • v.26 no.3
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    • pp.257-273
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    • 2020
  • Concrete bond strength with steel re-bars depends on multiple factors including concrete-steel interface and mechanical properties of concrete. However, the hydration development of cementitious paste, and in turn the mechanical properties of concrete, are negatively affected by cold weather. This study aimed at exploring the concrete-steel bonding behavior in concrete cast and cured under freezing temperatures. Three concrete mixtures were cast and cured at -10 and -20℃. The mixtures were protected using conventional insulation blankets and a hybrid system consisting of insulation blankets and phase change materials. The mixtures comprised General Use cement, fly ash (20%), nano-silica (6%) and calcium nitrate-nitrite as a cold weather admixture system. The mixtures were tested in terms of internal temperature, compressive, tensile strengths, and modulus of elasticity. In addition, the bond strength between concrete and steel re-bars were evaluated by a pull-out test, while the quality of the interface between concrete and steel was assessed by thermal and microscopy studies. In addition, the internal heat evolution and force-slip relationship were modeled based on energy conservation and stress-strain relationships, respectively using three-dimensional (3D) finite-element software. The results showed the reliability of the proposed models to accurately predict concrete heat evolution as well as bond strength relative to experimental data. The hybrid protection system and nano-modified concrete mixtures produced good quality concrete-steel interface with adequate bond strength, without need for heating operations before casting and during curing under freezing temperatures down to -20℃.

Analysis of cure behavior of low temperature curing liquid silicone rubber (LSR) for multi-material injection molding (이중사출 성형을 위한 저온 경화 액상실리콘고무 (LSR)의 경화 거동 분석)

  • Hyeong-min Yoo
    • Design & Manufacturing
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    • v.17 no.1
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    • pp.1-5
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    • 2023
  • In multi-material injection molding, since two or more materials with different process conditions are used, it is essential to maximize process efficiency by operating the cooling or heating system to a minimum. In this study, Liquid silicone rubber (LSR) that can be cured at a low temperature suitable for the multi-material injection molding was selected and the cure behavior according to the process conditions was analyzed through differential scanning calorimetry (DSC). Dynamic measurement results of DSC with different heating rate were obtained, and through this, the total heat of reaction when the LSR was completely cured was calculated. Isothermal measurement results of DSC were derived for 60 minutes at each temperature from 80 ℃ to 110 ℃ at 10 ℃ intervals, and the final degree of cure at each temperature was calculated based on the total heat of reaction identified from the Dynamic DSC measurement results. As the result, it was found that when the temperature is lowered, the curing start time and the time required for the curing reaction increase, but at a temperature of 90 ℃ or higher, LSR can secure a degree of cure of 80% or more. However, at 80 ℃., it was found that not only had a relatively low degree of curing of about 60%, but also significantly increased the curing start time. In addition, in the case of 110 ℃, the parameters were derived from experimental result using the Kamal kinetic model.

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The Development of Electro-Conductive Threads Coated with Silver Nanowires for Use in Wearable Devices (웨어러블 디바이스를 위한 은 나노와이어 코팅 전도사 개발)

  • Kim, Jimin;Yun, Changsang
    • Journal of the Korean Society of Clothing and Textiles
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    • v.45 no.4
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    • pp.674-684
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    • 2021
  • Recent advances in electronic technology have engendered a need for research on the use of smart materials in clothing. Electro-conductive fibers are expected to be a crucial element of wearable devices. Therefore, in this study, we have attempted to develop electro-conductive threads and cables using silver nanowires. Based on the characteristics of silver nanowire, in which electro-conductivity can be imparted via heat treatment, we prepared conductive threads by coating nylon yarn with silver nanowires and curing at temperatures of 140℃, 150℃, and 160℃. Conductive threads cured at 140℃ had the highest conductivity, followed by threads cured at 160℃ and 150℃ respectively. The order of the electrical conductivity of the threads after tensile testing was consistent with the original order of the conductivity of the threads. When we evaluated the sensing performance of electro-conductive cables fabricated from these threads, the cables manufactured from threads cured at 140℃ and 160℃ were found to function normally within temperature and humidity sensors. All the cables operated normally in illuminance and electrocardiogram sensors. Thus, we believe that threads made of silver nanowire have sufficient electrical conductivity to be utilized as wearable sensors.

Study to evaluate the correlation between structural core strength and strength development of standard cured specimens in a summer environment (하절기 환경에서 구조체 코어 강도와 표준양생 공시체 강도의 압축강도 발현 상관성 평가 연구)

  • Jeong, Min-Gu;Kim, Han-Sol;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2023.11a
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    • pp.143-144
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    • 2023
  • The compressive strength of concrete varies depending on various factors. Among them, based on the curing temperature, the KCS 14 20 10 Standard Specification for General Concrete calculates the nominal strength by applying the temperature correction value (Tn) based on the compressive strength of the standard cured concrete at 20±2℃ when designing the formulation strength. However, Tn is a correction value that considers only the temperature, and the correction of strength difference due to heat of hydration is not applied. Therefore, in this study, one-component and two-component concrete are mixed in the summer, structural concrete are manufactured, standard concrete specimen are manufactured, and coring is performed on the central and boundary parts of the structural concrete to calculate the correction value applied to the nominal strength by comparing the compressive strength of standard cured concrete on the 28th day of curing and the compressive strength of structural concrete on the 91st day of curing.

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Field Application of Mass Concrete Using Setting Time Difference of Super Retarding Agent for Reduction of Hydration Heat (초지연제의 응결시간차를 이용한 매스 콘크리트의 수화열 저감을 위한 현장 적용)

  • 전충근;심보길;손성운;신동안;오선교;한천구
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2004.05a
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    • pp.11-14
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    • 2004
  • In this paper, field application of mass concrete using setting time difference of super retarding agent is reported to reduce hydration heat of concrete placed at newly constructed apartment house in Busan. Horizontal placing lift is applied. According to test results. slump and air content meets the requirement of target values. For compressive strength, it exceeds the nominal strength ordered by the costumer. Compressive strength of concrete cured in place is achieved more than the values of nominal strength at l4days. For temperature history, maximum temperature of center at top section shows 58.5$^{\circ}C$, and at bottom section, 62.6$^{\circ}C$. According to naked eye's investigation, no hydration heat crack is observed at the surface of concrete.

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THE RELATIVE DEGREE OF CONVERSION OF THE COMPOSITE RESIN SURFACE (복합레진 표면의 중합률)

  • Park, Seong-Ho
    • Restorative Dentistry and Endodontics
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    • v.21 no.1
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    • pp.360-365
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    • 1996
  • The purpose of this study was to evaluate the changes in the degree of conversion on a composite resin surface following heat treatment and mylar strip finishing. The effects of the time interval between the light-curing and heat-curing process were also evaluated. The composite resin surface which had been covered with a coverglass showed a lower conversion rate than the surface from which a layer of $500{\mu}m$ was ground away. The composite resin surface was definitely affected by oxygen during the heat curing process when it had not been insulated. When the composite resins were heat cured after 3 days of storage following the light curing process, the increased in the degree of conversion through heatcuring was limited.

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A literatual study on the Ecthyma (렴瘡에 對한 文獻的 考察)

  • Kim, Hee-Taek;Oh, Young-Seon;Rho, Sek-Seon
    • The Journal of Korean Medicine Ophthalmology and Otolaryngology and Dermatology
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    • v.10 no.1
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    • pp.209-246
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    • 1997
  • In the literatual study on the Ecthyma, the results were as follows. 1. The pathogenic factors of Ecthyma is divided three parts. One is exogenous pathogenic factors which including the wind evil, wind heat and toxic material produced by wetness evil. Another is endogenous pathogenic factors which including the declination of kidney-yang, impairment of the liver and kidney, the lower classes of yin-fire, accumulation of wetness-heat in the spleen asthenia, impairment of the liver and kidney, wetness-heat of three yang, asthenic heat-syndrome of three yin. The other is pathogenic factors neither endogenous nor exogenous which including the food and living, uncontrol sexual excess, anxiety and angry, injury of skin, injury of insects and animals. 2. Five viscera which was concerned with Ecthyma are liver, spleen and kidney. 3. Frequent region of Ecthyma are S-36(足三里) and C-7(陰交). External Ecthyma was rose to wetness-heat of three yang channel that cured easily. Internal Ecthyma was rose to asthenic heat-syndrome of three yin channel that cured hardly. 4. In the frequency of prescription, the most numerous prescription is Bojungikgitang(補中益氣湯) and the next are Kyukgigo(隔紙膏) and Yukmijihwanghwan(六味地滉丸). 5. In the frequency of medicine, the most medicine is Calomelas(輕粉) which included Hydrargyrum(水銀) and the next are Olibanum(乳香) and Resina Commiphorae Myrrhae(沒藥) which regulating vital energy and pain control medicine used that in order to destroy insects and remove polson. 6. In classification of the medical action, medicine of clearing away summer-heat and heat evil and activating blood circulation to dissipate blood stasis used to be very busy which in order to remove the disorder of vital energy for virulent heat-evil. 7. In classification of four characters, the most part is warm medicine, the next are cold and cool medicine and there is a few that is hot medicine. 8. In classification of five tastes, the most numerous tastes are bitter and acrid, the next are sweet, salty and sour tastes. 9. In classification of virulence of medicine, the most part is non-toxic, the next are weakly and deadly poison. 10. In classification of channel distribution, the most is the medicine that belongs to liver channel, the next are the lung, spleen, stomach and kidney channel.

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Bond strength of denture base resin repaired according to contamination (의치상 수리면 오염원에 따른 수지의 결합강도)

  • Jung, Kyung-Pung
    • Journal of Technologic Dentistry
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    • v.25 no.1
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    • pp.71-79
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    • 2003
  • The purpose of this study was to investigate bond strength of denture base resin repaired according to contamination. One commercial denture base resin and two different kinds of relines resin were tested; Lusiton 199(denture base resin), Vertex(reline resin) and TokusoRebase(repair resin). The specimens were processed according to the manufacturer's instructions to cured denture base resin(polymethylmethacrylate; PMMA) and reline resin. Bond strengths were examined by use of a three-point transverse flexural strength test. Data were analyzed with two-factor analysis of variance and Duncan's post-hoc test at $\alpha$=0.05. Generally, the bondstrength of heat-cured resin(Lusiton 199) was higher than the other resins. The contaminations produced an decrease in bond strength. Therefore the contamination, such as saliva or water must be avoided during the laboratory repair procedures.

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Electrical Properties of Silicone Gels due to the Curing Condition (경화조건에 따른 실리콘 젤의 전기적 특성)

  • 홍능표;이수원;홍진웅
    • Journal of the Korean Society of Safety
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    • v.15 no.1
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    • pp.86-92
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    • 2000
  • Recently, more advanced electronic elements become, they consume powerful and radiate more heat in devices. So the most suitable packaging technique is keenly needed. The most important purpose of packaging is to protect devices within a system for a long time and to prevent life of devices from external environments; floating ions such as humidity or sodium, and exposure from ultraviolet rays. In order to study the electrical properties of silicone gels often used as packing material due to the curing condition, volume resistivity and AC breakdown experiment are performed. Specimens are made up at several cured times and temperatures condition ; 0.5[H], 1[H] and 2[H] at 100[$^{\circ}C$], 125[$^{\circ}C$], 150[$^{\circ}C$], 160[$^{\circ}C$], 170[$^{\circ}C$] and 180[$^{\circ}C$]. It is confirmed that from volume resistivity experiment liquid silicone become get state at 90~100 [$^{\circ}C$] and cured specimen for 1~2[H] at 170[$^{\circ}C$] are superior in electrical properties.

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