• Title/Summary/Keyword: heat cured

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Study on Heat Resistance Anaerobic Adhesive Which Expands When Post Cured

  • Zhai, Haichao;Li, Yinbai;Lin, Xinsong
    • Journal of Adhesion and Interface
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    • v.3 no.1
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    • pp.9-12
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    • 2002
  • In this paper, N,N-m-phenyenedimaleimide (m-PDM), Polyamide Resin (PI) and Metallic dimethacrylate etc. influencing the heat resistance of anaerobic adhesive has been studied, an anaerobic adhesive composition capable of post-cure expansion and $230^{\circ}C$ temperature resistance comprising a multifunctional methacrylate and m-PDM capable of effectuating expansion upon post-cure has been developed. A homogeneous mixture of a monomer and m-PDM are subjected to a first cure heat stage (Room Temperature) wherein a rigid partially-cured plastic is formed and a post-cure heat stage ($150^{\circ}C$) to effectuate permanent expansion of cured adhesive composition.

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A STUDY ON THE POROSITY OF DENTURE BASE RESINS PROCESSED BY MICROWAVE ENERGY (극초단파에너지에 의해 온성된 의치상용 레진의 다공성에 관한 연구)

  • Jeong, Chang-Mo
    • The Journal of Korean Academy of Prosthodontics
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    • v.34 no.4
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    • pp.816-822
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    • 1996
  • The purpose of this study was to determine whether there was any difference in the mean porosity of denture base resin cured by microwave energy, when the liquid monomers of denture resin(K-33 : methyl methacrylate for conventional water bath curing or Acron MC : special monomer for microwave curing) and/or the thicknesses of denture base($5{\times}10{\times}60mm\;or\;10{\times}10{\times}60mm$) were varied. The mean porosities of k-33 specimens cured in water bath with two different thicknesses were used as control. The results were as follows : 1. Regardless of specimen thickness, Acron MC cured by microwave energy showed the least mean porosity, followed by K-33 cured by water bath heat, and K-33 cured by microwave energy showed the highest level of mean porosity(P<0.05). 2. In both K-33 and Acron MC cured by microwave energy the mean porosities of 5mm thickness groups were lower than those of 10mm thickness groups(P<0.05). But no significant difference was found in mean porosity between 5mm thickness and 10mm thickness of water bath heat cured groups made of K-33(P>0.05).

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Physical Properties Effect of Dry-Heat and Microwave-Cured Acrylic Resins depending on the Irradiation-Induced Changes (유도광선변화에 따른 건식중합과 마이크로파중합 아크릴레진의 물리적 성질영향)

  • Kim, Gyu-Ri
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.7
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    • pp.4388-4397
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    • 2015
  • The purpose of this study was to research the property change of acrylic resins depending on the induced-beam change and research the improved physical property of dry-heat and microwave-cured dental place acrylic resin in order to develop the acrylic resins with the optimum characteristic. As a result of observing flexural rigidity, hardness and color difference, the dry-heat-cured specimens of Vertex RS and Paladent 20 showed ideal property at 5, 15, and 25 kGy irradiation. The microwave-cured specimens of Vertex RS and Paladent 20 showed ideal property at 5 kGy irradiation. The correlation analysis showed a positive correlation among ARD, flexural rigidity (0 418), E coefficient (0.675) and Barcol hardness (0 588). The radiation cure technology is helpful for relieving the contamination caused by the manufacture of polymer composite. It can significantly contribute to the fusion of ultra violet cure technology and nano technology and the improvement of mechanical property without giving effect to the workability of polymer.

Performance Improvement of Cured-In-Place-Pipe(CIPP) Process by Boiler Waste Heat Recovery (보일러 폐열 회수를 통한 현장경화관(CIPP)공정 성능 향상)

  • Kim, Young-Jin;Jung, Chung Woo;Lee, Yoon Jung;Kim, Sung Soo;Kang, Yong Tae
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.25 no.3
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    • pp.164-167
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    • 2013
  • The objectives of this paper are to study the performance improvement of waste heat recovery from a boiler, by the Cured-In-Place-Pipe(CIPP) process. The conventional apparatus does not utilize the waste heat from the boiler during the process. However, the present apparatus recovers the waste heat from the boiler. When the new apparatus is used, the bending strength and modulus of the CIPP becomes double, and is over 45% stronger, than the required conditions, respectively. It is found that the energy consumption reduces to 50%, by recovering the waste heat from the boiler, and the oil consumption amount reduces to 1/3, compared to the conventional apparatus.

Effect of Surface Treatment on Transverse Strength of Denture Repair When Heat Cured Resin Denture Base is Repaired (열중합(熱重合) 레진의치상(義齒床) 수리시(修理時) 파절면(破折面)에 대한 처리방법(處理方法)이 수리 후 Transverse strength에 미치는 영향(影響))

  • Jung, Jong-Hyun
    • Journal of Technologic Dentistry
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    • v.12 no.1
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    • pp.113-119
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    • 1990
  • The purpose of this study was to investigate the effect of surface tretment on strength of denture repair as influenced by repair resin. Specimens were fabricated from VERTEX heat cured resin. Rectangular specimens($60\times10\times3mm$) were prepared according to the manufacturer's instruction for mixing and packing the resin into molds. Two methods of surface treatment were used and two methods of repair were also tested. The transverse strength of the resin was measured before repair and after repair by AUTOGRAPH testing machine. Six specimens of each category were prepared for testing for a total of 24 specimens. The mean value of the percent of recovery was calculated from the percent of recovery for six specimens. The results were as follows : 1. The mean value of the percent of recovery of each category makes a significant difference statistically one another(p<0.01), and "C" category, chloroform solvent-heat cured resin, has a better effect on repair srength than any other. 2. When no chloroform is used to treat the fractured surface there is no significant difference between the mean values of the percent of recovery influenced by the self curing resin and heat cured resin. But, when chloroform is used there is a significant difference between the two repair resins(p<0.01). 3. When self curing resin repair is used there is no significant difference between repair with and without the surface treatment of chloroform. But, when heat cured resin repair is used the use of chloroform treatment become significant statistically (p<0.01).

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Adhesion of biofilm, surface characteristics, and mechanical properties of antimicrobial denture base resin

  • Ana Beatriz Vilela Teixeira;Mariana Lima da Costa Valente;Joao Pedro Nunes Sessa;Bruna Gubitoso;Marco Antonio Schiavon;Andrea Candido dos Reis
    • The Journal of Advanced Prosthodontics
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    • v.15 no.2
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    • pp.80-92
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    • 2023
  • PURPOSE. This study incorporated the nanomaterial, nanostructured silver vanadate decorated with silver nanoparticles (AgVO3), into heat-cured resin (HT) at concentrations of 2.5%, 5%, and 10% and compared the adhesion of multispecies biofilms, surface characteristics, and mechanical properties with conventional heat-cured (HT 0%) and printed resins. MATERIALS AND METHODS. AgVO3 was incorporated in mass into HT powder. A denture base resin was used to obtain printed samples. Adhesion of a multispecies biofilm of Candida albicans, Candida glabrata, and Streptococcus mutans was evaluated by colony-forming units per milliliter (CFU/mL) and metabolic activity. Wettability, roughness, and scanning electron microscopy (SEM) were used to assess the physical characteristics of the surface. The mechanical properties of flexural strength and elastic modulus were tested. RESULTS. HT 10%-AgVO3 showed efficacy against S. mutans; however, it favored C. albicans CFU/mL (P < .05). The printed resin showed a higher metabolically active biofilm than HT 0% (P < .05). There was no difference in wettability or roughness between groups (P > .05). Irregularities on the printed resin surface and pores in HT 5%-AgVO3 were observed by SEM. HT 0% showed the highest flexural strength, and the resins incorporated with AgVO3 had the highest elastic modulus (P < .05). CONCLUSION. The incorporation of 10% AgVO3 into heat-cured resin provided antimicrobial activity against S. mutans in a multispecies biofilm did not affect the roughness or wettability but reduced flexural strength and increased elastic modulus. Printed resin showed higher irregularity, an active biofilm, and lower flexural strength and elastic modulus than heat-cured resin.

Hardening Properties of Hardener-Free Epoxy-Modified Mortars by Curing Conditions (양생조건에 따른 경화제 무첨가 에폭시수지 혼입 PMM의 경화특성)

  • Lee, Jae-Hwa;Kim, Joo-Young;Kim, Wan-Ki
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2012.11a
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    • pp.255-257
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    • 2012
  • Epoxy resin without any hardener can harden in the presence of hydroxide ions in cement mortars and concretes at ambient temperature. The purpose of present study is to examine the hardening properties of hardener-free epoxy-modified mortars by curing conditions. The hardener-free epoxy-modified mortars using diglycidyl ether of A epoxy resin are prepared with various polymer-cement ratios, and subjected to initial moist/dry curing, initial steam(90℃) curing, initial steam/heat(80℃, 100℃) curing.As a result, degree of hardening of epoxy resin in initial moist/dry cured, initial steam cured and initial steam/heat(80℃) cured hardener-free epoxy-modified mortars is decreased with increasing polymer-cement ratio. However, it is markedly improved with additional dry-curing periods. On the other hand, regardless of the polymer-cement ratio and dry curing periods, degree of hardening of hardener-free epoxy-modified mortars with initial steam/heat(100℃) cure is over 95%.

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A STUDY ON FLEXURAL STRENGTH OF COMPOSITE RESIN INLAY ACCORDING TO HEAT TREATMENT (열처리에 따른 복합레진 인레이의 굴곡강도에 관한 연구)

  • Kim, Yong-Seong;Min, Byung-Soon;Choi, Ho-Young;Park, Sang-Jin;Choi, Gi-Woon
    • Restorative Dentistry and Endodontics
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    • v.18 no.1
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    • pp.84-94
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    • 1993
  • The purpose of this study was to evaluate flexure strength of composite resin inlay according to heat treatment and duration in comparasion with visible light-cured resin. In this study, materials were used 1 visible light-cured resin and 3 kinds of composite resin inlays. Control group was visible light cured resin (Photo Clearfil Posterior) and experimental groups were composite resin inlays (Brilliant Dentin, Brilliant Enamel and Clearfil CR Inlay). Experimental groups were divided 3 groups: First group was Brilliant Dentin and second group was Brilliant Enamel and -third group was Clearfil CR Inlay. Used experimental groups were calculated flexural strength according to heat treatment and duration. The following results were obtained: 1. Experimental groups were higher flexural strength than control group. 2. At $100^{\circ}C$ when heat treatment carried out 7 minutes flexural strength elevated third group, second group, first group in turn and when heat treatment carried out 15 minutes flexural strength elevated third group, second group, first group in turn but no difference was showed between first and second group. 3. At $125^{\circ}C$ when heat treatment was carried out 7 minutes flexural strength elevated third group, second group, first group in turn and when heat treatment was carried out 15 minutes flexural strength elevated third group, first group, second group in turn but no difference was showed between first and second group. 4. In spite of heat treatment and duration the third group was highest flexural strength in the others groups.

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Temperature History of the Wall Concrete Subjected to -10℃ depending on Heat Curing Method (-10℃ 조건에서의 보온양생방법 변화에 따른 벽체 콘크리트의 온도이력)

  • Han, Sang-Yoon;Son, Ho-Jung;Cheong, Sang-Hyun;Ahn, Sang-Ku;Han, Cheon-Goo;Han, Min-Cheol
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2011.11a
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    • pp.255-256
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    • 2011
  • This study investigates the effect of a curing condition on the temperature history and strength development of concrete under -10℃. Combination of various curing methods was applied, i.e. a conventional form was combined with compressed insulation, heat panel and heat cable. Results showed that the concrete cured by a single use of a conventional form resulted in serious deterioration of early strength development. However, other concretes cured by the proposed curing methods maintained the temperature of the concretes between 5 and 20℃, and thus resulted in no frost damage.

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ADHERENCE OF ORAL BACTERIA ON CHITOSAN-ADDED DENTURE BASE MATERIALS IN VITRO (키토산을 첨가한 의치상 재료의 세균 부착에 관한 연구)

  • Chung Sung-Hwan;Vang Mong-Sook;Park Ha-Ok
    • The Journal of Korean Academy of Prosthodontics
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    • v.40 no.5
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    • pp.525-535
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    • 2002
  • The purposes of this study were to evaluate the adherence of bacteria on various denture base resin materials and effects of chitosan, added to denture base materials on bacterial adherence. PMMA denture base resin such as heat-cured Vertex-RS, self-cured Vertex-SC and 4-META denture base resin such as heat-cured Meta-Dent, self-cured Meta-Fast were used in this study Samples were divided into two groups the denture base resin with chitosan, without chitosan Streptococcus mutans and Lactobacillus casei were used in this study. The surface of samples was observed by SEM. When chitosan was added to M17 and MRS broth, viable cell count of bacteria was reduced. Viable cell count of Streptococcus mutans on the samples decreased as follows : Meta-Dent, Vertex-SC, Meta-Fast, Vertex-RS. Viable cell count of Lactobacillus casei on the samples decreased as follows: Vertex-RS, Meta-Dent, Meta-Fast, Vertex-SC. The resin with chitosan showed lower adherence of bacteria than without chitosan. The images of SEM showed that the surface of the resin with chitosan was rougher than that of without chitosan. These results showed that the denture base resin materials with chitosan have rougher surface than without chitosan, but less bacteria adhered on them.