• Journal of Surface Science and Engineering
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• v.45 no.6
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• pp.226-231
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• 2012

Characteristics of carburized surface layers in 0.18C-3.5Ni-1.5Cr-0.2Mo steels for main shaft bearings of wind turbines have been analyzed and evaluated before and after rolling contact fatigue tests. Mixed microstructure consisting of retained austenite and tempered martensite has been formed with compressive residual stresses in the surface hardened layers of the specimens showing uniform hardness distribution with value about Hv700 after vacuum carburizing and tempering. It has been found on the raceway of the layers of the specimens after rolling contact fatigue tests that the amount of retained austenite decreased and compressive residual stresses increased, resulting from cyclic contact stresses applied during the tests. It has been also revealed that higher durability of the bearings can be obtained through controlling the amount of the retained austenite in the surface of the bearing steels to be lower in this study.

• Journal of Surface Science and Engineering
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• v.42 no.3
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• pp.116-121
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• 2009

The 2-step low temperature plasma processes (the combined carburizing and post-nitriding) offer the increase of both surface hardness and thickness of hardened layer and corrosion resistance than the individually processed low temperature nitriding and low temperature carburizing techniques. The 2-step low temperature plasma processes were carried out for improving both the surface hardness and corrosion resistance of AISI 316L stainless steel. The influence of gas compositions on the surface properties during nitriding step were investigated. The expanded austenite (${\gamma}_N$) was formed on all of the treated surface. The thickness of ${\gamma}_N$ and concentration of N on the surface increased with increasing both nitrogen gas and Ar gas levels in the atmosphere. The thickness of ${\gamma}_N$ increased up to about $20{\mu}m$ and the thickness of entire hardened layer was determined to be about $40{\mu}m$. The surface hardness was independent of nitrogen and Ar gas contents and reached up to about 1200 $HV_{0.1}$ which is about 5 times higher than that of untreated sample (250 $HV_{0.1}$). The corrosion resistance in 2-step low temperature plasma processed austenitic stainless steels was also much enhanced than that in the untreated austenitic stainless steels due to a high concentration of N on the surface.

• Journal of the Korean Wood Science and Technology
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• v.46 no.5
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• pp.610-621
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• 2018

In conservation treatment lacquer has been used variously as a restoration material. However, dealing with Lacquer is very difficult as it dried in high humidity that can be harmful to the base materials. Also being natural varnish, dried lacquer layer is very different from the drying condition and the quality of the lacquer. These make difficult to predict the result of drying lacquer. In this study, using the humidity control machine, firstly, the main contents of the two different type of lacquer was experimented. And these lacquers was cured in various conditions. The duration time was checked until totally hardened. After that, obtained lacquer layers was analyzed to understand optical properties. Therefore, this study made a result about the relationship between characteristics of lacquer layer and the hardening condition. As a result, duration time of the Korean lacquer drying which has average 13.4% more urushiol than the Chinese lacquer is recorded a twice or triple decrease over it of the Chinese one. And, in all types of lacquer, the higher humidity makes the faster a pace of lacquer dried. In same lacquer, the shorter the duration time of drying lacquer is much darker and glossier. However, gloss deteriorated in saturated humidity. In humidity lower than RH 70%, lacquer is not hardened in 336 hours. When the layer totally cured through long period more than 30 days, the drying lacquer is appeared high brightness and almost transparent. Thus, in lower than RH 70%, it is hard to obtain durable layer.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.9 no.1
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• pp.96-101
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• 2000

Ceramic, PCD and CBN tools are available for the difficult-to-cut-materials such as hardened carbon tool steel, stainless steel, Inconel 718 and etc.. Ceramic toolsare likely to be chipped and abruptly broken before the appearance of normal wear in turning. Ther2efore ceramic tools are suitable for continuous cut in turning not for intermittent in milling. In this study, TiN/TiCN multi-layer coated ceramic tools were found to restrain the chipping, breaking and early fracture and to increase the critical cutting speed owing to TiN/TiCN multi-layer coating in Arc Ion Plating of PVD method.

• Transactions of Materials Processing
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• v.21 no.6
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• pp.354-359
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• 2012

Effects of a nitriding treatment on the tensile and high cycle fatigue properties were investigated by conducting ion-nitriding and gas nitro-caburizing treatments on the spheroidized SCr430B medium-carbon steel and performing tensile and tension-tension high cycle fatigue tests. The nitrided samples showed much lower strength and ductility compared to those in the initial as-spheroidized state and premature fracture occurred at the hardened layers. The micro-voids in the compound layer caused fatigue crack initiation. Thus, the removal of the compound layer with micro-voids remarkably improved the fatigue resistance to even beyond that of the as-spheroidized sample.

• Korean Journal of Metals and Materials
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• v.47 no.11
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• pp.716-721
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• 2009

The major drive for the application of low-temperature plasma treatment in nitrocarburizing of austenitic stainless steels lies in improved surface hardness without degraded corrosion resistance. The low-temperature plasma nitrocarburizing was performed in a gas mixture of $N_{2}$, $H_{2}$, and carbon-containing gas such as $CH_{4}$ at $450^{\circ}C$. The influence of the processing time (5~30 h) and $N_{2}$ gas composition (15~35%) on the surface properties of the nitrocarburized layer was investigated. The resultant nitrocarburized layer was a dual-layer structure, which was comprised of a N-enriched layer (${\gamma}_N$) with a high nitrogen content on top of a C-enriched layer (${\gamma}_C$) with a high carbon content, leading to a significant increase in surface hardness. The surface hardness reached up to about $1050HV_{0.01}$, which is about 4 times higher than that of the untreated sample ($250HV_{0.01}$). The thickness of the hardened layer increased with increasing treatment time and $N_{2}$ gas level in the atmosphere and reached up to about $25{\mu}m$. In addition, the corrosion resistance of the treated samples without containing $Cr_{2}N$ precipitates was enhanced than that of the untreated samples due to a high concentration of N on the surface. However, longer treatment time (25% $N_{2}$, 30 h) and higher $N_{2}$ gas composition (35% $N_{2}$, 20 h) resulted in the formation of $Cr_{2}N$ precipitates in the N-enriched layer, which caused the degradation of corrosion resistance.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.10a
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• pp.245-251
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• 2004

This paper is studied on the effect of TiAlN coated Ball End Mill and MQL(Minimum Quantity Lubrication) cutting condition on cutting characteristic of high hardness steels. KP4 steels[HRC32] and STD11[HRC60] heat treated steels were used as the workpiece and WC-Co ball end mill and single and multi layer TiAlN coated ball end mill were utilized in the cutting tests. MQL device was used to spray botanical oil coolant. Result showed that TiAlN coated ball end mill were increased the cutting length than WC-Co ball end mill in the cutting speed[$245{\sim}320m/min$] about $2.3{\sim}5.7$ times for KP4 steels and about $2.5{\sim}4.3$ times far STD11 heat treated steels. The multi layer TiAlN coated ball end mill is good for KP4 steels than single layer coated.

• Transactions of the Korean Society of Mechanical Engineers
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• v.13 no.3
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• pp.451-460
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• 1989

This paper dealt with the effect of the ratios N2 to H2 gas on the corrosion fatigue failure behavior of ion-nitrided SM45C steel specimens. The specimens were water cooled after ion-nitriding at 500.deg. C for 3hrs in 5 Torr, 0.8N$_{2}$ and 0.5N$_{2}$ atmospheres. As the nitrogen concentration increases, the higher compressive residual stresses developed in the surface layer and the depth of nitrided layer increased, which in turn gave rise to increases in fatigue strength and corrosion fatigue life. In the region less than 1.5 * 10$^{5}$ cycles, fatigue failure initiated at the brittle nitrided case, whereas in the region higher than 1.5 * 10$^{5}$ cycles crack initiated from the non-metallic inclusions in the subsurface. The initiation of corrosion fatigue failure was mainly attributed to pitting of case hardened surface layer.

• Transactions of the Korean Society of Mechanical Engineers
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• v.11 no.1
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• pp.53-62
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• 1987

High power lasers provide a controllable and precise energy source in surface transformation hardening. A careful control of the process is needed in order that the surface layer of the material reaches the austenizing temperature, but that it does not melt. In order to achieve this the results of theoretical and experimental studies on the laser surface hardening of a medium carbon steel are described. A two-dimensional computer program, which can be used generally for the determination of transient temperature distributions in welding and heat treatment, was established on the basis of the finite element method. For the confirmation of the accuracy of the numerical analysis, a medium carbon steel (SM 45C) of 5mm thickness was heat-treated with a 1kW CW CO$_{2}$ laser machine, while the traverse speed and the distance from the focal point (defocused distance) were varied. Experimental and numerical results showed a similar tendency in correlations between the hardened zone shape and the process parameters. With increasing beam spot diameter the width and depth of the hardened zone increased for relatively small beam spot diameters, but decreased rapidly after reaching the maximum value, while with increasing traverse speed the width and depth of the hardened zone decreased monotonously. Too small beam spot diameters are to be avoided, since the surface melting would lower the surface hardness and produce an uneven surface which may be unacceptable because of the possible requirement for subsequent machining. It could be observed that for a given traverse speed and laser power input there exists a optimal range of the beam spot diameter, which produce a large width of the hardened zone but no melting on the surface.

• Journal of the Korean Society for Heat Treatment
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• v.9 no.1
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• pp.69-77
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• 1996

The fatigue crack initiation behavior of plasma ion nitrided SACM645 steel was investigated through the rotary bending fatigue test and residual stress measurement by XRD. It was shown by XRD and EPMA that the plasma ion nitrided surface was composed of ${\gamma}^{\prime}(Fe_4N)$phase and ${\varepsilon}(Fe_{2-3}N)$phase, and that the nitrogen atoms existed in Fe matrix in diffusion layer. The OM, SEM and Auger spectroscopy showed that the depth of compound layer, mixed compound and diffusion layer, and diffusion layer was $8{\mu}m$, $30{\mu}m$ and $300{\mu}m$, respectively. However, the microhardness test showed that the depth of hardened layer was $500{\mu}m$. The tensile strength of the ion nitrided SACM645 was lower than that of the unnitrided SACM645, and the ion nitrided specimen was fractured without plastic deformation. The nitrided SACM645 showed much poorer low cycle fatigue properties than the unnitrided one. In rotary bending fatigue, the fatigue strength of the ion nitrided SACM645 was higher than that of the unnitrided specimen, and the fatigue crack initiation sites changed by applied fatigue stress levels. The XRD result showed that the ion nitrided SACM645 has the compressive residual stress from surface to $600{\mu}m$ deep and the tensile residual stress from $600{\mu}m$ to deeper site. It is thought that crack initiation takes place at the point where the total stress of residual stress and applied stress is maximum.