• 제목/요약/키워드: graphite shape

검색결과 102건 처리시간 0.023초

현장 열응답 시험을 통한 수직 밀폐형 지중열교환기의 성능 평가 (Evaluation of performance of closed-loop vertical ground heat exchanger by In-situ thermal response test)

  • 이철호;박문서;곽태훈;최항석
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2010년도 춘계 학술발표회
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    • pp.229-239
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    • 2010
  • Performing a series of in-situ thermal response tests, the effective thermal conductivity of six vertical closed-loop ground heat exchangers was experimentally evaluated and compared each other, which were constructed in a test bed in Wonju. To compare thermal efficiency of the ground heat exchangers in field, the six boreholes were constructed with different construction conditions: grouting materials (cement vs. bentonite), different additives (silica sand vs. graphite) and the shape of pipe-sections (general U-loop type vs. 3 pipe-type). From the test results, it can be concluded that cement grouting has a higher effective thermal conductivity than that of bentonite grouting, and the efficiency of graphite better performs over silica sand as a thermally-enhancing addictive. In addition, a new 3 pipe-type heat exchanger provides less thermal interference between the inlet and outlet pipe than the conventional U-loop type heat exchanger, which results in superior thermal performance.

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구상흑연주철의 Bainite변태과정에서 Bainitic Ferrite의 형상변화 (Morphological Variation of Bainitic Ferrite in Transformation Process of Austempered Ductile Iron)

  • 최답천
    • 한국주조공학회지
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    • 제12권5호
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    • pp.403-411
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    • 1992
  • The growth characteristics of bainite at early stage in the fast quenched spheroidal graphite cast irons containing 0.06%Mn and 0.45%Mn during austempering process, was investigated with optical and scanning electron microscope. The following results regarding the effects of Mn and isothermal heat treatment on the morphological variation of bainitic ferrite were obtained. The morphology of bainite varies from acicular below 350$^{\circ}C$ to feather shape above 350$^{\circ}C$. The period of isothermal treatment also affects the shape of bainite at the fixed temperature. At 350$^{\circ}C$, bainite is bamboo leaf-like up to 200 secs of isothermal holding time and with further increasing time up to 300 secs, changes to a mixed structure consisting of both feather and bamboo leaf and, finally becomes all feather shape at 900 secs. The morphology of bainitic ferrite formed at early stage of 300$^{\circ}C$ isothermal treatment is similar to that of bainitic ferrite formed at 250$^{\circ}C$ or 350$^{\circ}C$ with unbranched, linear ferrite. However, bainitic ferrite divides into branches with increasing isothermal treatment, which occurs more fast at 400$^{\circ}C$ than at 350$^{\circ}C$. The difference in adding amount of Mn influences the morphology of bainitic ferrite in upper bainite. The bainitic ferrite with 0.45%Mn is observed to be more stable than that with 0.06%Mn, remaining unbranched for a longer period at the same temperature.

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Diamond 박막 성장에 미치는 Si 표면 영향의 AES에 의한 연구 (A Study on the Effect of Si Surface on Diamond Film Growth by AES)

  • 이철로;신용현;임재영;정광화;천병선
    • 한국진공학회지
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    • 제2권2호
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    • pp.199-208
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    • 1993
  • Si 기판 표면상태 변화와 관련된 핵생성 자유에너지 증가에 따른 다이아몬드 박막성장 거동을 관찰하였다. 표면 염마조건 변화에 따른 3가지 기판(A-Si, B-Si, C-Si)위에 동일한 성장조건으로 다이아몬드를 성장하였으며, 이때 형상인자와 관련된 자유에너지 관계는 ${\Delta}G_{A-Si}<{\Delta}G_{B-Si}<{\Delta}G_{C-Si}$이다. AES, SEM, XRD, RHEED에 의해 각각의 박막 A, B, C를 조사한 결과, 핵생성 자유에너지가 가장 적은 A 박막은 (100) (110) 면이 지배적인 고품위 다이아몬드 박막이다. 자유에너지가 A에 비해 다소 적은 B 박막은 (111) 면이 지배적인 8면체 다이아몬드 박막이고, 자유에너지가 자장 적은 C 박막은 흑연이 많이 함유된 구상의 다이아몬드이다.

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CuFe2O4을 이용한 메탄부분산화 특성 연구 (A Study of Methane Partial Oxidation Characteristics on CuFe2O4)

  • 우성웅;강용;강경수;김창희;김철성;박주식
    • Korean Chemical Engineering Research
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    • 제46권6호
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    • pp.1113-1118
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    • 2008
  • $CuFe_2O_4$$Fe_3O_4$의 탄소 침적 및 환원 특성을 $900^{\circ}C$에서 TGA, XRD, SEM, TEM 등의 분석 및 반응 후 가스조성분석을 통하여 연구하였다. XRD 분석결과 환원된 $Fe_3O_4$는 Fe(iron)와 graphite(C) 그리고 $Fe_3C$으로 구성되어 있는 것으로 나타났다. 반면에, 환원된 $CuFe_2O_4$에서는 graphite나 $Fe_3C$가 나타나지 않았다. SEM을 이용하여 표면 구조를 관찰한 결과 환원된 $Fe_3O_4$의 표면이 탄소로 뒤덮여 있는 것을 확인할 수 있었다. 이와 달리 $CuFe_2O_4$에서는 $CH_4$ 전환율 및 환원속도가 높았고, 환원반응 후 탄소량 추정결과 $Fe_3O_4$에서보다 훨씬 낮게 나타났다. TEM 분석결과 $Fe_3O_4$ 입자로부터 탄소가 판상구조의 형태로 성장한 것을 확인할 수 있었다.

불활성 가스의 O2와 CO 불순물 제거를 위한 Ni 촉매의 물성 평가 (Assessment of Ni Catalyst Properties for Removal of O2 and CO Impurity in Inert Gas)

  • 김광배;진새라;김은석;임예솔;이현준;김성훈;노윤영;송오성
    • 한국산학기술학회논문지
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    • 제21권4호
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    • pp.588-595
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    • 2020
  • 반도체 산업용 9N 이상의 초고순도 N2, Ar 등 불활성 가스 제조를 위해 가스 정제공정에 사용되고 있는 Ni 촉매의 물성 평가 및 촉매적 특성을 확인하였다. 조성이 다른 원기둥 형태의 C1, 츄러스 형태의 C2의 두 가지 Ni 촉매에 대해 비교 평가를 진행하였다. Ni 촉매의 형상과 미세구조를 분석하기 위해 광학현미경과 FE-SEM을 이용하였으며, 조성 확인 및 물성을 분석하기 위해 EDS, XRD, 그리고 micro-Raman 분석을 이용하였다. 또한 Ni 촉매의 비표면적 및 촉매적 특성을 확인하기 위해 BET, Pulse Titration 분석을 진행하였다. 조성 분석결과, C1의 경우, 상대적으로 graphite가 불순물로 다량 포함되어 있는 것을 확인하였으며, C2는 C1에 비해 Ni의 함량이 높은 것을 확인하였다. 비표면적 분석 결과, C2의 비표면적이 C1보다 약 1.69배 정도 큰 것을 확인할 수 있었다. 촉매적 특성분석 결과, 상온에서 O2와 CO 불순물 제거 정도가 C2가 우수함을 확인하였다. 따라서 반도체 산업용 초고순도 불활성 기체 제조를 위한 Ni 촉매로는 불순물이 적고, 비표면적이 크며, 상온에서 O2와 CO 제거 성능이 우수한 C2가 적합함을 확인하였다.

절연체위의 다결정실리콘 재결정화 공정최적화와 그 전기적 특성 연구 (Optical process of polysilicaon on insulator and its electrical characteristics)

  • 윤석범;오환술
    • E2M - 전기 전자와 첨단 소재
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    • 제7권4호
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    • pp.331-340
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    • 1994
  • Polysilicon on insulator has been recrystallized by zone melting recrystallization method with graphite strip heaters. Experiments are performed with non-seed SOI structures. When the capping layer thickness of Si$\_$3/N$\_$4//SiO$\_$2/ is 2.0.mu.m, grain boundaries are about 120.mu.m spacing and protrusions reduced. After the seed SOI films are annealed at 1100.deg. C in NH$\_$3/ ambient for 3 hours, the recrystallized silicon surface has convex shape. After ZMR process, the tensile stress is 2.49*10$\^$9/dyn/cm$\^$2/ and 3.74*10$\^$9/dyn/cm$\^$2/ in the seed edge and seed center regions. The phenomenon of convex shape and tensile stress difference are completely eliminated by using the PSG/SiO$\_$2/ capping layer. The characterization of SOI films are showed that the SOI films are improved in wetting properties. N channel SOI MOSFET has been fabricated to investigate the electrical characteristics of the recrystallized SOI films. In the 0.7.mu.m thickness SOI MOSFET, kink effects due to the floating substrate occur and the electron mobility was calculated from the measured g$\_$m/ characteristics, which is about 589cm$\^$2//V.s. The recrystallized SOI films are shown to be a good single crystal silicon.

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분말 압출 공정에서 온도 유지시간 제어를 통한 미세기어의 내피로성 향상 연구 (Improvement of fatigue resistance of the miniature gear by controlling holding time of temperature in the hot powder extrusion process)

  • 김진우;이경훈;황대원;김병민
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2009년도 추계학술대회 논문집
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    • pp.449-452
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    • 2009
  • This paper was designed to fabricate the miniature spur gear with pitch circle of 1.8 by hot extrusion process of mechanically alloyed Zn-22wt%Al powder at various temperature. The mechanical alloying was preformed for ball milled times of 8h, 16h and 32h by the planetary ball milling. Mechanically alloyed powders were compacted cylindrical performs. Extrusions of the miniature spur gear using the alloyed powder were carried out at different extrusion temperatures. The extruded spur gear was sintered for 2h at $350^{\circ}C$ in argon atmosphere. The friction between the die and the powdered billet and the internally different density due to complex product shape cause the internal crack. To overcome the mentioned problems, high dimensional accuracy at cross section of the spur gear and uniform Vickers hardness could be obtained by graphite lubricant and controlling holding time.

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비대칭 복합적층판 의 Warping 해석 (Warping Analysis of Unsymmetric Laminated Composites)

  • 전완주;홍창선
    • 대한기계학회논문집
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    • 제7권4호
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    • pp.404-409
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    • 1983
  • The warping of unsymmetric laminated composites is induced by residual curing stress at the room temperature. Classical lamination theory (C.L.T.) predicts the room temperature shapes of all unsymmetric laminates to be a saddle. Experimental observations, however, indicate some unsymmetric laminated composites have cylindrical room temperature shapes. This anomalous behavior is explained by the extention of C.L.T. which involves Von Karman's large deflection theory. It is shown that, depending on the thickness, width, length, curing temperature and room temperature of the laminate, critical boundaries of the shape change are determined. Theoretical predictions are compared with experimental results of Toray Graphite/Epoxy {O$_{n}$/90$_{n}$}$_{T}$./....

DUST SHELL MODELS FOR THE YOUNG STELLAR OBJECTS IN GIANT MOLECULAR CLOUDS

  • Song, In-Ok;Suh, Kyung-Won
    • Journal of Astronomy and Space Sciences
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    • 제17권1호
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    • pp.11-18
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    • 2000
  • We have modeled the observed spectral energy distributions(SEDs) of young stellar objects (YSOs) in giant molecular clouds (GMCs). We propose the theoretical modles for the dust envelopes around YSOs. The YSOs in a GMC may share the same initial chemical composition. In this paper, we compare the model SEDs with the observations of the YSOs. Dust shells of the YSOs are composed of a mixture of astronomical silicate and graphite grains. We propose the models for the evolution of the GMCs comparing the shape of the SEDs on the IRAS 2-color diagram with the age.

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구상흑연주철의 강인화에 미치는 3상 혼합조직의 영향 (The Effect of the Multi-phase (ferrite-bainite-martensite) on the Strengthening and Toughening in the Ductile Cast Iron)

  • 김석원;이방식
    • 한국주조공학회지
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    • 제8권3호
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    • pp.310-321
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    • 1988
  • This study is aimed to investigate the effects of the multi-phase(ferrite-bainite-martensite) on the strengthening and toughening in ductile cast iron. All the specimen were austenitized at eutectoid transformation temperature range(${\alpha}+{\gamma}$) for 1hr and austempered at $300^{\circ}C$ and $400^{\circ}C$ for various holding time, and then quenched in iced water for multi - phase (${\alpha}-B-M$). When the volume fraction of martensite is below 15%, excellent maximum fracture load can be obtained due to strengthening by the fine martensite, but, with increasing of volume fraction over 15%, it was decreased drastically. The martensite size became finer and the shape of it changed from bar to spherical type with increasing of austempering holding time. The higher the austenitizing temperature is, the more preferential is the formation of austenite phase around the graphite nodules improving strength and toughness of austempered ductile cast iron.

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