• Title/Summary/Keyword: granule powder

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Spherical Granule Production from Micronized Saltwort (Salicornia herbacea) Powder as Salt Substitute

  • Shin, Myung-Gon;Lee, Gyu-Hee
    • Preventive Nutrition and Food Science
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    • v.18 no.1
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    • pp.60-66
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    • 2013
  • The whole saltwort plant (Salicornia herbacea) was micronized to develop the table salt substitute. The micronized powder was mixed with distilled water and made into a spherical granule by using the fluid-bed coater (SGMPDW). The SGMPDW had superior flowability to powder; however, it had low dispersibility. To increase the dispersibility of SGMPDW, the micronized powder was mixed with the solution, which contained various soluble solid contents of saltwort aqueous extract (SAE), and made into a spherical granule (SGMPSAE). The SGMPSAE prepared with the higher percentages of solid content of SAE showed improved dispersibility in water and an increase in salty taste. The SGMPSAE prepared with 10% SAE was shown to possess the best physicochemical properties and its relative saltiness compared to NaCl (0.39). In conclusion, SGMPSAEs can be used as a table salt substitute and a functional food material with enhanced absorptivity and convenience.

Effect of Organic Additives on Microstructure and Green Density of Zirconia Granules Using Water Solvent (유기첨가제가 수계에서 제조된 지르코니아 과립의 미세구조 및 성형밀도에 미치는 영향)

  • Jung, Ji-Hwan;Lee, Sang-Jin
    • Journal of Powder Materials
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    • v.24 no.2
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    • pp.147-152
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    • 2017
  • Spherical-type zirconia granules are successfully fabricated by a spray-drying process using a water solvent slurry, and the change in the green density of the granule powder compacts is examined according to the organic polymers used. Two organic binders, polyvinyl alcohol (PVA) and 2-hydroxyethyl methacrylate (HEMA), which are dissolved in a water solvent and have different degrees of polymerization, are applied to the slurry with a plasticizer (polyethylene glycol). The granules employing a binder with a higher degree of polymerization (PVA) are not broken under a uniaxial press; consequently, they exhibit a poor green density of $2.4g/cm^3$. In contrast, the granule powder compacts employing a binder with a lower degree of polymerization (HEMA) show a higher density of $2.6g/cm^3$ with an increase in plasticizer content. The packing behavior of the granule powders for each organic polymer system is studied by examining the microstructure of the fracture surface at different applied pressures.

Preparation of Granule Powders for Thermal Spray Coating by Utilization of Pyrophyllite Minerals

  • Kim, Yong-Hyeon;Shin, Pyung-Woo;Lee, Sang-Jin
    • Journal of the Korean Ceramic Society
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    • v.53 no.5
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    • pp.557-562
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    • 2016
  • Pyrophyllite granule powders for thermal spray coating were successfully prepared through spray drying process. To produce a stable slurry, commercial pyrophyllite powder of $45{\mu}m$ in size was ball-milled for reduction of the size to $2{\sim}3{\mu}m$ and a dispersant was added to control the viscosity. Dense and spherical granules (average granule size : $59{\mu}m$) were prepared under conditions of 12,500 rpm for rotation velocity of the atomizer and 100 cps for slurry viscosity. The granules were then heat treated at $1,200^{\circ}C$ for proper handling strength and flow properties. The final granules had an apparent density of $0.725g/cm^3$ and a flow rate of 2.5 g/sec, which represent excellent properties to be used as the granule powder for thermal spray coatings.

Production of Porous Metallic Glass Granule by Optimizing Chemical Processing

  • Kim, Song-Yi;Guem, Bo-Kyung;Lee, Min-Ha;Kim, Taek-Soo;Eckert, Jurgen;Kim, Bum-Sung
    • Journal of Powder Materials
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    • v.21 no.4
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    • pp.251-255
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    • 2014
  • In this study, we optimized dissolution the dissolution conditions of porous amorphous powder to have high specific surface area. Porous metallic glass(MG) granules were fabricated by selective phase dissolution, in which brass is removed from a composite powder consisting of MG and 40 vol.% brass. Dissolution was achieved through various concentrations of $H_2SO_4$ and $HNO_3$, with $HNO_3$ proving to have the faster reaction kinetics. Porous powders were analyzed by differential scanning calorimetry to observe crystallization behavior. The Microstructure of milled powder and dissolved powder was analyzed by scanning electron microscope. To check for residual in the dissolved powder after dissolution, energy dispersive X-ray spectroscory and elemental mapping was conducted. It was confirmed that the MG/brass composite powder dissolved in 10% $HNO_3$ produced a porous MG granule with a relatively high specific surface area of $19.60m^2/g$. This proved to be the optimum dissolution condition in which both a porous internal granule structure and amorphous phase were maintained. Consequently, porous MG granules were effectively fabricated and applications of such structures can be expanded.

Hybrid Composite Nano-sized WC-Co Cemented Carbide

  • Park, Sun-Yong;Lee, Wan-Jae
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.640-641
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    • 2006
  • To improve the mechanical properties of WC-Co cemented carbides, the dual composite was studied. The compositions of granule and matrix were nano-sized WC-6 wt% Co(granule) and normal sized WC-20 wt% Co(matrix), respectively. The granules were grouped 50, 100 and $150\;{\mu}m$ and mixed with WC and Co powders as the volume fractions of granule to matrix were 50 to 50, 40 to 60 and 30 to 70. These compacts were sintered at $1380^{\circ}C$ for 10 minutes in vacuum. The microstructure, transverse rupture strength and wear resistance were investigated.

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Study on Test Method for Strength of Ceramic Spray Dried Powder (분무 건조된 세라믹 과립의 강도 측정방법에 대한연구)

  • 엄우식;이희수;이세훈;김덕희;이인식
    • Journal of the Korean Ceramic Society
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    • v.33 no.6
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    • pp.660-664
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    • 1996
  • We have studied the test method for strength of spray dried ceramic powder using manual press and UTM. which is one of the important to influence forming process. We could observe the compaction behavior using manual press. However the measurement of granule strength was only possible with UTM capable of providing the condition of a constant pressing rate. The strength of granule can be measured from the slope change of compaction curve and agrees with the value which is obtained from the combination of saturated tap density and compaction curve. So we proposed the accurate method to measure the strength of granule from the results of this study.

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The Effect of Phosphate Desorption Solution on LDH (Layered Double Hydroxide) Desorption (탈착 용액의 조성변화가 층상이중수산화물에 흡착된 인 탈착에 미치는 영향)

  • Jung, Yong-Jun
    • Journal of Korean Society on Water Environment
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    • v.24 no.6
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    • pp.670-675
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    • 2008
  • Batch type adsorption and desorption tests were performed with different types (Powder, Granule) of Layered double hydroxides (LDHs) saturated with phosphate. The adsorption isotherm was approximated as a modified Langmuir type equation. The maximum adsorption capacity was 55 mg-P/g-LDH for powder type LDH, and 46 mg-P/g-LDH for granule type LDH. The highest phosphate desorption (79.6%) was obtained with 20% NaOH solution, whereas the desorption degrees were 4.8, 22.2% and 46.7% in the solutions of acidic condition (pH 4), 30% NaCl, and 3% NaOH, respectively. It was suggested that the optimal condition for the phosphate desorption from LDH was 30% NaCl + 3~6% NaOH solutions. The desorption characteristics of LDH was little influenced by adsorbent type.

Identification of Irradiated Granule-Type Ramen Soup Powder by Pulsed Photostimulated Luminescence and Thermoluminescence during Storage

  • Yi, Sang-Duk;Yang, Jae-Seung;Kim, Dong-Woo;Shin, Doo-Ho;Jo, Gab-Yeon;Chang, Kyu-Seob;Oh, Man-Jin
    • Preventive Nutrition and Food Science
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    • v.8 no.1
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    • pp.79-84
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    • 2003
  • This study was carried out to establish a method for determining if granule-type Ramen soup powder has been irradiated. Thermoluminescence (TL) and pulled photostimulated luminescence (PPSL) were used as the detection methods through observed changes of TL and PPSL intensities after storage under differing conditions. PPSL intensities increased with increases in irradiation doses. The threshold level of PPSL was below 412$\pm$58 photon counts regardless of storage conditions (room and darkroom) after 10 months. TL intensities also increased with increasing irradiation doses. The coefficients ($R^2$) of PPSL (0.74~0.94) and TL intensities (0.92~0.58) were very highly correlated with irradiation dose. The PPSL and TL intensities were decreased after 10 months of storage. These results indicate that discrimination of irradiated from non-irradiated granule-type Ramen soup powder is possible using TL and PPSL methods despite the decrease in intensities of TL and PPSL with increasing storage times.

A Study on Preparation and the Standard Recipe of Premixed Gam-Injulmi Rice Cake (Premix 감인절미 제조 및 표준 Recipe에 관한 연구)

  • 김경자;오옥자
    • Journal of the East Asian Society of Dietary Life
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    • v.7 no.1
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    • pp.47-55
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    • 1997
  • This study aims to know what the physicochemical properties and physical properties of the Korean traditional rice cake injulmi made from persimmon powder and glutinous rice(powder), and to come up with a standard recipe of it with the premixed powder of persimmon and glutinous rice. Cooked rice powder with 9 different levels of persimmon in cooling dough(75, 100 and 150${\mu}{\textrm}{m}$ power with each 20, 40, and 60%) was tested for rheological parameters, the rate of swelling, degree of gelatinization, sensory evaluation, and the observation of cross section used to electronmicroscope. 1. sensory evaluation conducted by 20 university students as panelists showed that mixed glutinous rice powder and persimmon powder lost their regular forms. increase in persimmon powder content increased a thin layer of starch granule, presumably due to sugar and fiber in the mixed persimmon powder granule. 3. In cooking the rice cake with 20~60% of persimmon, it showed 6.3 to 5.5 pH. 4. Quantitative description analysis conducted by 20 university student s panelists showed that sample that sample C was preferred among 9 samples. From these results, it was concluded that glutinous rice cake cooked with 20% of persimmon powder was quiet acceptable. Optimum cooking condition for the glutinous rice with persimmon powder rice cake was 30min of cooking time and 25$0^{\circ}C$ of cooking temperature with gas oven.

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Effect of Suspension Property on Granule Characteristics and Compaction Behavior of Fine Si3Na4 Powder (분산계 특성이 질화규소 미분의 과립특성 및 충진거동에 미치는 영향)

  • 이해원;오성록
    • Journal of the Korean Ceramic Society
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    • v.32 no.4
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    • pp.462-470
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    • 1995
  • The characteristics of spray-dried granules are important for dry pressing operation since they have great influences on die-filling, compaction ratio, and resulting green microstructure. An attempt was made to control granule morphology and the packing structure of fine Si3N4 particles in granules by adjusting suspension property. Mercury porosimetry was used to characterize the pore structures of both granules and green compacts. Finally, the effects of particle packing structure in granules and green microstructure on sintering behavior were investigated.

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