• Title/Summary/Keyword: grain-size distribution

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Comparison of Microstructure and Hardness of Pure Copper Fabricated by Multi-Axial Forging and Multi-Axial Diagonal Forging (다축단조와 다축대각단조로 제조된 순동의 미세조직 및 경도 비교)

  • Lee, J.K.;Kwon, S.C.;Kim, S.T.;Jeong, H.T.;Kim, Y.G.;Park, S.H.
    • Transactions of Materials Processing
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    • v.28 no.5
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    • pp.257-265
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    • 2019
  • Multi-axial forging (MAF), a severe plastic deformation technique, is known to be difficult to obtain materials with homogeneous microstructures. Recently, multi-axial diagonal forging (MADF) process has been developed to solve this problem. In this study, in order to compare the microstructural and mechanical homogeneities of the MAFed and MADFed samples, oxygen-free copper (OFC) cubes measuring 25 mm in length were deformed through MAF and MADF processes and the average grain size and hardness were measured at the edge, face, and center regions of the samples. In the MAFed samples, ultrafine grains were formed at the center region, but a considerable amount of coarse grains remain at the face region. Therefore, the MAFed samples showed a high inhomogeneity in regards to grain size and hardness. On the contrary, in the case of the MADFed sample, the grain sizes at the edge, face, and center regions were similar and the hardness in all the regions are almost similar. This indicates that the MADFed sample has a homogeneous microstructure and uniform mechanical properties, which can be attributed to the homogeneous distribution of the effective strain throughout the material. The results of this study suggests that the MADF is a suitable process in the fabrication of high-strength copper materials with a homogeneous and ultrafine grain structure.

Distribution of Some Metallic Elements in Surface Sediments of the Southeastern Yellow Sea. (황해 남동해역 표층퇴적물 중 수종 금속원소의 분포 특성에 관한 연구)

  • 이창복;정회수
    • 한국해양학회지
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    • v.27 no.1
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    • pp.55-65
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    • 1992
  • Ninety-seven surface sediment samples, collected from the southeastern part of the Yellow Sea, were analyzed for their contents of five metallic elements, including Fe, Mn, Ni, Cu and Pb as well as their grain-size and calcium carbonate content. The result showed a contrasting behaviour among the five metallic elements. with respect to their relationship with the sediment grain0size. contents of nickel and copper demonstrated a fairly linear relationship with the pediment grain-size whereas those of manganese and lead did not. This different behaviour in these metals was interpreted as being the result of the anthropogenic inputs (for Pb) and modification during the early diagenesis (for Mn). The R0mode factor analysis result also confirmed the different behaviour of manganese and lead from that of copper and nickel. Based on this different behaviour in metals the (Mn+Pb)/(Cu+Ni) ratio was suggested as a possible criterion for distinguishing the fine sediments in the study area, which originated from two different source area. China and Korea.

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Effect of Grain Size Control and Binder Additions on the Soft Magnetic Properties of Fe-based Nanocrystalline Powder Cores (Fe계 나노결정 분말코아의 연자성특성에 미치는 입도제어 및 바인더 첨가의 영향)

  • Cho E.K.;Cho H.J.;Kwon H.T.;Cho E.M.;Ryu H.H.;Sohn K.Y.;Park W.W.
    • Journal of Powder Materials
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    • v.13 no.4 s.57
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    • pp.256-262
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    • 2006
  • The amorphous $Fe_{73}Si_{16}B_7Nb_3Cu_1$ alloy strip was pulverized to get a flake-shaped powder after annealing at $425^{\circ}C$ for 90 min and subsequently ground to obtain finer flake-shaped powder by using a ball mill. The powder was mixed with polyimide-based binder of $0.5{\sim}3wt%$, and then the mixture was cold compacted to make a toroidal powder core. After crystallization treatment for 1 hour at $380{\sim}600^{\circ}C$, the powder was transformed from amorphous to nanocrystalline with the grain size of $10{\sim}15nm$. Soft magnetic characteristics of the powder core was optimized at $550{\sim}600^{\circ}C$ with the insulating binder of 3wt%. As a result, the powder core showed the outstanding magnetic properties in terms of core loss and permeability, which were originated from the optimization of the grain size and distribution of the insulating binder.

Laboratory Test for Permanent Settlement Behavior of Geo-materials used in Railway Considering Grain size distribution and Water content (입도 및 함수비 조건에 따른 철도 노반 재료의 영구침하거동 요소시험평가)

  • Lee, Sung Jin;Lee, Il Wha;Lee, Su Hyung;Eum, Ki Young
    • Journal of the Korean Society for Railway
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    • v.18 no.4
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    • pp.354-362
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    • 2015
  • Since allowable settlement of concrete slab track is about 30mm, a lot of attention must be paid to the settlement of the earthwork (reinforced trackbed, upper subgrade, under subgrade) under the concrete track. To this end, more experimental data should be accumulated through tests for these materials. In this study, we evaluate the long-term settlement of reinforced trackbed and subgrade materials using factors such as repeated loading conditions, water content, and grain size distributions in a large triaxial test and a large oedometer test. In cases in which the performance of the reinforced trackbed layer meets the design criteria, the settlement caused by train load was considerably small. But, when the water content increases in the subgrade, unexpectedly large settlement might occur for certain grain size distributions of the subgrade materials.

Species Composition and Community Structure of Macrobenthos during Fall on the Dokdo Coast, Korea (가을철 독도 연안에 출현하는 대형저서동물의 종 조성 및 군집 구조)

  • Kang, Su Min;Lee, Hyung-Gon;Kim, Sang Lyeol;Choi, Jin-Woo;Park, Chan Hong;Yu, Ok Hwan
    • Ocean and Polar Research
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    • v.41 no.2
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    • pp.47-61
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    • 2019
  • The Dokdo coast is known for its high biodiversity. However, few studies have examined the biodiversity and macrobenthic community on the subtidal soft-bottom. Therefore, we collected macrobenthos (> 1 mm) using a Smith-McIntyre grab ($0.1m^2$) at 15 stations along the Dokdo coast in September 2016. The sediments consisted of badly sorted (1.7) coarse sand with gravel and the mean sediment grain size was $-0.4{\phi}$. In total, 177 macrobenthic species were collected; their mean density was $1,566ind./m^2$. The number of species and density of macrobenthic fauna decreased significantly with the mean grain size. The dominant species were the amphipods Melita denticulata (16.5%) and Melita shimizui (5.5%), polychaete Salvatoria clavata (5.4%), bivalve Glycymeris aspersa (4.4%), and ophiuroid Ophionereis dubia (4.3%). The dominant macrobenthos species on the subtidal soft-bottom differed from the coastal areas of the East Sea, suggesting that the difference in the sediment grain size affected the macrobenthos. Cluster analysis was performed to divide the study area into four groups, and environmental factors which correlated with species composition and distribution in the study area were the combination of the four parameters of salinity, dissolved oxygen, total organic carbon and depth. A future seasonal investigation is needed to understand the species composition and characteristics of the Dokdo macrobenthos.

Analysis of Microstructural Refinement for Inconel 706 during Hot Forging Process through Reheating and Strain (Inconel 706의 열간단조 공정 중 재가열과 변형양에 따른 결정립 미세화에 대한 분석)

  • S. G. Seong;H. J. Kang;Y. S. Lee;S. Y. Lee;U. J. Lee;H. I. Jae;J. H. Shin;E. Y. Yoon
    • Transactions of Materials Processing
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    • v.32 no.5
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    • pp.239-246
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    • 2023
  • To reduce the forming load due to the temperature drop, during the hot forging process, a reheating hot forging process design is required that to repeat heating and forging. However, if the critical strain required for recrystallization is not induced during forging and grain growth becomes dominant due to the reduction in dislocation density due to repeated heating, the mechanical properties may deteriorate. Therefore, in this study, Inconel 706 alloy was applied, and the grain refinement behavior was comparatively analyzed according to the number of reheating times and effective strain during reheating hot forging process. Reheating was carried out with a total compression rate of 40% up to 4 times. The Inconel 706 compression test specimens heated once showed finer grains as the effective strain increased due to the dynamic recrystallization phenomenon. However, as the number of heating increases, grain refinement was observed even in a low effective strain distribution of 0.43 due to static recrystallization during reheating. Moreover, grain growth occurs at a relatively low effective strain of 0.43 when the number of reheating is four or more. Therefore, it was effective to apply an effective strain of 0.43 or more during hot forging to Inconel 706 in order to induce crystallization through grain refinement and improve the properties of forged products. In addition, we could notice that up to three reheating times condition was appropriate to prevent grain growth and maintain fine grain size.

Distribution Pattern, Geochemical Composition, and Provenance of the Huksan Mud Belt Sediments in the Southeastern Yellow Sea (황해 남동부 흑산니질대 퇴적물의 분포, 지화학적 조성 및 퇴적물 기원지)

  • Ha, Hun Jun;Chun, Seung Soo;Chang, Tae Soo
    • Journal of the Korean earth science society
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    • v.34 no.4
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    • pp.289-302
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    • 2013
  • In order to determine the provenance of the Huksan Mud Belt sediments in the southeastern Yellow Sea, the major and rare earth elements of the same sediments were analyzed. The surface sediments were sampled from top of piston-cores and box-cores taken at 51 sites within the Huksan Mud Belt. With the mean grain size of $5-6{\phi}$, the sediments of the study area are mud-dominated. The spatial distribution patterns show that silt content is high in the northern Mud Belt, whereas clay content increases as it moves toward the southern Mud Belt. Interestingly, the geochemical compositions both of major and rare earth elements have resulted in differences of sediment provenance. Among the major elements, plots of Fe/Al vs. Mg/Al ratios, $Al_2O_3$ vs. MgO ratios, and $Al_2O_3$ vs. $K_2O$ reveal that the Huksan Mud Belt sediments are dominated by the Korean river-derived sediments. However, the characteristics of rare earth elements infer sediments originating from the Chinese rivers. This discrepancy between the above provenances is attributed to the different contributory factors in the content of chemical elements. Considering strong correlation between major elements with grain sizes, the contents of the major elements are thought to be influenced by the grain size. However, there is a weak correlation between rare earth elements and grain sizes. The behaviour of rare earth elements may be controlled by heavy minerals, rather than grain sizes. Further study requires to solve the discrepancy arose from the difference in applied chemical tracers.

Thin-Beam Excimer Laser Annealing

  • Ang, Woo Boon;Rothweiler, Dirk;Knowles, David
    • 한국정보디스플레이학회:학술대회논문집
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    • 2007.08b
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    • pp.1061-1064
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    • 2007
  • Thin Beam Excimer Laser Annealing is investigated as one possible process enabled by the variable concept of Thin Beam LTPS processing. The structure of the resulting p-Si material is analyzed in terms of grain size distribution, scaling with energy density and overlap, as well as average surface roughness. This process provides similar control and latitude as conventional excimer laser annealing, but reduced average surface roughness and the potential to be scaled to significant productivity levels.

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