• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.03a
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• pp.73-76
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• 1997

Nanocrystalline materials have been modeled as a mixture of the crystallite and the grain boundary phases. The mechanical property has been calculated using the rule of mixtures based on the volume fractions. The critical grain size concept suggested by Nieh and Wadsworth and porous material model suggested by Lee and Kim were applied to the calculation. The theoretical results fit very well with the experimental values

• Journal of the Korean Ceramic Society
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• v.33 no.5
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• pp.602-615
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• 1996

The purpose of the present study is to investigate the microstructural effect on the R-curve behavior in three aluminas with different grain size distributions by analyzing the bridging stress distribution. The crack opening displacement (COD) according to the distance behind the stationary crack tip was measured using an in situ SEM fracture method. The measured COD values in the fine-grained alumina agreed well with Wiederhorn's sollution while they deviated from Wiederhorn's solution in the two coarse-grained aluminas because of the increase of the crack closure due to the grain interface bridging in the crack wake. A numerical fitting procedure was conducted by the introduction of the power-law relation and the current theoretical model together with the measured COD's in order to obtain the bridging stress distribution. The results indicated that the bridging stress function and the R-curve computed by the current model were consistent with those computed by the power-law relation providing a reliable evidence for the bridging stress analysis of the current model. The strain-softening exponent in the power-law relation n, was calculated to be in the range from 2 to 3 and was closely related to the grain size distribution. Thus it was concluded from the current theoretical model that the grain size distribution affected greatly the bridging stress distribution thereby resulting in the quantitative analysis of microfracture of polycrystalline aluminas through correlating the local-fracture-cont-rolling microstructure.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.70-73
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• 2006

In the present study, the flow-softening behavior occurring during high temperature deformation of AZ31 Mg alloy was investigated. Flow softening of AZ31 Mg alloy was attributed to (1) thermal softening by deformation heating and (2) microstructural softening by dynamic recrystallization. Artificial neural networks method was used to derive the accurate amounts of thermal softening by deformation heating. A series of mechanical tests (High temperature compression and load relaxation tests) was conducted at various temperatures ($250^{\circ}C{\sim}500^{\circ}C$) and strain rates ($10^{-4}/s{\sim}100/s$) to formulate the recrystallization kinetics and grain size relation. The effect of DRX kinetics on microstructure evolution (fraction of recrystallization) was evaluated by the unified SRX/DRX (static recrystallization/dynamic recrystallization) approaches

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2000.10a
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• pp.25-28
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• 2000

The flow stress of 304 stainless steel during high during hot forming process were determined by conducting hot compression tests at the range of 1273 K-1423 K and 0.05 /s-2.0 /s as these are typical temperature and strain rate in hot forging operation. Based on the observed phenomena, a constitutive model of flow stress was assumed as a function of strain, strain rate, temperature. Dynamic recrystallization was found to be the major softening mechanism with this conditions as previous studies. A finite element analysis was performed to predict the recrystallized volume fraction and the mean grain size in hot compression of 304 stainless steel.

• Journal of Welding and Joining
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• v.30 no.2
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• pp.76-80
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• 2012

In this study, the effect of the welding current on the hardness characteristics and microstructure in the resistance spot welding of 1GPa grade cold-rolled DP steel was investigated, Also, correlation between the hardness and microstructure was discussed. In spite of the change in the welding current, the hardness distributions near weld was similar. the hardness in the HAZ and the fusion zone was higher than that of the base metal and the hardness in the fusion zone was variated with the location. Especially, the hardness of HAZ adjacent to the base metal showed maximum value, and softening zone in the base metal adjacent to HAZ was found. With the increasing of welding current, there were no difference in maximum hardness and average hardness in the fusion zone were, but the hardness of the softening zone reduced. The difference in the hardness in each location of weld due to grain size of prior austenite. The softening of the base metal occurred by tempering of the martensite.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.57-58
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• 2006

The effects of lowering ECAP temperature during ECAP process and Post-ECAP annealing on microstructure, texture and mechanical properties of the AZ31 alloys have been investigated in the present study. The as-extruded materials were ECAP processed to 2 passes at 553K prior to subsequent pressing up to 6 passes at 523K or 493K. When this method of lowering ECAP temperature during ECAP was used, the rods could be successfully deformed up to 6 passes without any surface cracking. Grain refinement during ECAP process at 553K might have helped the material to endure further straining at lower deformation temperatures probably by increasing the strain accommodation effect by grain boundary sliding, causing stress relaxation. Texture modification during ECAP has a great influence on the strength of Mg alloys because HCP metals have limited number of slip systems. As slip is most prone to take place on basal planes in Mg at room temperature, the rotation of high fraction of basal planes to the directions favorable for slip as in ECAP decreases the yield stress appreciably. The strength of AZ31 Mg alloys increases with decrease of grain size if the texture is constant though ECAP deformation history is different. A standard positive strength dependence on the grain size for Mg alloys with the similar texture (Fig. 1) supports that the softening of ECAPed Mg alloys (a negative slope) typically observed despite the significant grain refinement is due to the texture modification where the rotation of basal planes occurs towards the orientation for easier slip. It could be predicted that if the original fiber texture is restored after ECAP treatment yielding marked grain refinement, yield stress as high as 500 MPa will be obtained at the grain size of ${\sim}1{\mu}m$. Differential speed rolling (DSR) with a high speed ratio between the upper and lower rolls was applied to alter the microstructure and texture of the AZ31 sheets. Significant grain refinement took place during the rolling owing to introduction of large shear deformation. Grain size as small as $1.4{\mu}m$ could be obtained at 423K after DSR. There was a good correlation between the (0002) pole intensity and tensile elongation. This result indicates that tensile ductility improvement in the asymmetrically rolled AZ31 Mg alloys is closely related to the weakening of basal texture during DSR. Further basal texture weakening occurred during annealing after DSR. According to Hall-Petch relation shown in Fig. 1, the strength of the asymmetrically rolled AZ31 is lower than that of the symmetrically rolled one when compared at the same grain size. This result was attributed to weakening of fiber texture during DSR. The DSRed AZ31, however, shows higher strength than the ECAPed AZ31 where texture has been completely replaced by a new texture associated with high Schmid factors.

• Transactions of Materials Processing
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• v.10 no.7
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• pp.573-578
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• 2001

The flow stress of 304 stainless steel during hot forming process were determined by conducting hot compression tests at the range of 1273 K∼1423 K and 0.05 /s∼2.0 /s as these are typical temperature and strain rate in hot forging operation. In this material, Dynamic recrystallization was found to be the major softening mechanism with this conditions as Previous studies. Based on the observed phenomena, a constitutive model of flow stress was assumed as a function of strain, strain rate, temperature. In the constitutive model, the effects of strain hardening and dynamic recrystallization were taken into consideration. A finite element method connected to constitutive model was performed to predict the dynamic recrystallization behaviors and also stress-strain curves in hot compression of 304 stainless steel.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.03b
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• pp.171-175
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• 1999

the high temperature deformation behavior of 304 stainless steel was characterized by the hot torsion test. Continuous deformation was carried out at the temperature ranges 900-110$0^{\circ}C$ and the strain rate ranges 5x10-2~5/sec. The formulation of the flow stress curves was developed as subtraction form which was based on dynamic softening mechanisms The volume fraction of dynamic recrystallization and the mean grain size could be expressed as a function of deformation variables temperature (T) strain ($\varepsilon$) strain rate ($\varepsilon$) The calculated values of flow stress and mean grain size could be well matched with experimental values.

• Transactions of Materials Processing
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• v.10 no.4
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• pp.338-346
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• 2001

Evaluation of microstructural changes is important for process control during open die forging of heavy ingots. The control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects and to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent Precesses of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

• Transactions of Materials Processing
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• v.27 no.6
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• pp.347-355
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• 2018

This study investigated the effects of the processing number of multi-axial diagonal forging (MADF) on the microstructural changes of OFC fabricated by MADF processes. The as-extruded OFC was cut to $25mm^3$ cube for the MADF processes. The MADF process consists of plane forging with a thickness reduction of 30% and diagonal forging with a diagonal forging angle of $135^{\circ}$. In order to analyze the microstructural evolutions according to the number of repetitions, 1, 2, 3 and 4 cycles of the MADF process were performed. OFC specimens were successfully deformed without surface cracking for up to 4 cycles of MADF. The grain size, average misorientation and average grain orientation spread (GOS) of MADF processed materials were analyzed using EBSD technique and their Vicker's hardness were also measured. The results showed that MADF process effectively refined the microstructure of OFC with initial average grain size of $84.2{\mu}m$. The average grain sizes of specimens MADF processed for 1, 2, 3, 4 cycles were refined to be $8.5{\mu}m$, $2.2{\mu}m$, $1.5{\mu}m$, $1.1{\mu}m$, respectively. The grain refinement seemed to be saturated when OFC was MADF processed over 2 cycles. In the case of specimens subjected to two or more cycles of MADF, the degree of decrease in average grain size was drastically reduced as the number of cycles increased due to softening phenomena such as dynamic recovery or dynamic recrystallization during processing. The degree of increase in average Vicker's hardness was also dramatically reduced as the number of cycles increased due to the same reason.