• Title/Summary/Keyword: grain growth behavior

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Mechanical Properties of Ultrafine Grained 5052 Al Alloy Produced by Cryogenic Rolling Process (극저온 압연으로 제조된 5052 Al 합금의 기계적 성질)

  • Nam W. J
    • Transactions of Materials Processing
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    • v.13 no.8
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    • pp.704-709
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    • 2004
  • The effect of annealing temperature on microstructures and mechanical properties of the 5052 Al sheets rolled 88% reduction at cryogenic temperature was investigated for the annealing temperature of 150 ~ $300^{\circ}C$, in comparison with those rolled at room temperature. The presence of equiaxed grains, whose size is about 200nm in a diameter, was observed in the alloy deformed 88% and annealed $200^{\circ}C$ for an hour. When compared with the deformation at room temperature, the deformation at cryogenic temperature showed the higher strengths and equivalent elongation after annealing at the annealing temperature below $200^{\circ}C$. However, for annealing above $250^{\circ}C$ materials deformed at cryogenic temperature showed the lower strength than those deformed at room temperature. This behavior might be attributed to the higher rate of recrystallization and growth in materials deformed at cryogenic temperature during annealing, due to the lager density of dislocations accumulated during the deformation.

Expansion Behavior of Iron-copper Compact Made from (Fe-Cu) Prealloyed Powder

  • Kim, Youn-Che;Suk, Myung-Jin
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.812-813
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    • 2006
  • Dimensional change of compact made from (Fe-Cu) prealloyed powder and copper powder compared to that of compact made from iron-copper elemental powder. The compact made from the prealloyed powder with a copper content of 7.18mass% which is nearly equal to its solution limit and copper powder showed only the large contraction in spite of penetration of liquid copper into grain boundary of the prealloyed powder. But the compact made from iron-copper elemental powder showed the large expansion in spite of same chemical composition with former case.

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Behaviors of surface micro-crack of 304 stainless steel at elevated temperature (304스테인리스강의 고온표면미소 균열의 거동에 관한 기초적 연구)

  • 서창민;이정주;김영호
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.12 no.6
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    • pp.1320-1326
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    • 1988
  • This paper deals with the behavior of surface crack growth and the characteristics of surface micro-crack distribution under creep and creep-fatigue with 1 min. and 10 min. of load holding times at 593.deg.C, in air. The test specimen is a plate type with a small artificial defect of type 304 the small defect has been carried out by the surface replica method and optical microphotography. The experimental results have been interpreted from the view-point of fracture mechanics. It can be concluded that the longer the hold time the longer the total life time. Most of surface micro-cracks initiate at grain boundaries before the specimen reaches 20% of its total life time, a few of them lead to fracture by coalescence with the main crack.

Reactive Sintering of SiC (탄화규소의 활성화소결)

  • 김영욱;이준근
    • Journal of the Korean Ceramic Society
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    • v.20 no.2
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    • pp.115-122
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    • 1983
  • There has been many controversies about the effects of additive in sintering of SiC But no prior systematic work has been reported about the difference between the effects of B and $B_4C$ as additive. The sintering behavior of SiC and its strength are studied and the optimum concentrations of additives and sintering conditions for SiC are determined. The effects of B and $B_4C$ have same effects on reactive sintering of SiC except the easiness of transport via vapor phase for uniform distribution in case of B. The strength of sintered SiC without exaggerated grain growth is limited by surface flaws and is nearly independent of temperature up to 140$0^{\circ}C$.

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Low temperature solid phase crystallization of amorphous silicon thin film by crystalline activation

  • Kim, Hyung-Taek;Kim, Young-Kwan
    • Journal of Korean Vacuum Science & Technology
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    • v.2 no.2
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    • pp.97-100
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    • 1998
  • We have investigated the effects of crystalline activation on solid phase crystallization (SPC) of amorphous silicon (a-Si) thin films. Wet blasting and self ion implantation were employed as the activation treatments to induce macro or micro crystalline damages on deposited a-Si films. Low temperature and larger grain crystallization were obtained by the applied two-step activation. High degree of crystallinity was also observed on both furnace and rapid SPC. crystalline activations showed the promotion of nucleation on the activated regions and the retardation of growth in an amorphous matrix in SPC. The observed behavior of two-step SPC was strongly dependent on the applied activation and annealing processes. It was also found that the diversified effects by macro and micro activations on the SPC were virtually diminished as the annealing temperature increased.

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Recent Progress in Dielectric-Based Ultrafast Charging/Discharging Devices (유전체를 활용한 초고속 에너지 충/방전 소자 기술)

  • Choi, Hyunsu;Ryu, Jungho;Yoon, Woon-Ha;Hwang, Geon-Tae
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.35 no.4
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    • pp.322-332
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    • 2022
  • Energy storage capacitors based on dielectric ceramics with superior polarization properties and dielectric constant can provide much higher output power density due to their very fast energy charging/discharging rates, which are particularly suitable for operating pulsed-power devices. For an outstanding energy storage performance of dielectric capacitor, a large recoverable energy density could be derived by introducing a slim polarization-electric field hysteresis loop into dielectric materials by various technical approaches. Many research teams have explored various dielectric capacitor technologies to demonstrate high output power density and ultrafast charging/discharging behavior. This article reviews the recent research progress in high-performance dielectric capacitors for pulsed-power electronic applications.

Effects of $B_2O_3$ Addition on the Sintering Behavior and the Microwave Dielectric Properties of $(Mg_{0.93}Ca_{0.07})TiO_3$ Ceramics ($(Mg_{0.93}Ca_{0.07})TiO_3$ 세라믹스의 소결 및 마이크로파 유전특성에 미치는 $B_2O_3$의 영향)

  • 이득우;박재환;김인태;박재관;김윤호;최덕균
    • Journal of the Korean Ceramic Society
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    • v.35 no.3
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    • pp.287-293
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    • 1998
  • The effects of B2O3 addition on the sintering behavior and th microwave dielectric properties of $(Mg_{0.93}Ca_{0.07})TiO_3$ ceramics were investigated. By addition of $B_2O_3$, increases the density of the ceramics increases and grain growth enhances, It was densified to over 94% of $(Mg_{0.93}Ca_{0.07})TiO_3$ theoretical density by the addition of 0.15-1.0wt% B2O3 and stable microwave dielectric properties observed by the addition of 0.2-0.4wt% $B_2O_3.\;(Mg_{0.93}Ca_{0.07})TiO_3$ ceramics sintered at $1200^{\circ}C$ exhibits maximum dielectric constants of 24-25 quality factor($Q{\times}f$) of more than 70000 and temperature coefficient of resonant frequency of $0\;ppm/^{\circ}C$ by adding of 0.15-0.4wt% $B_2O_3$.

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Dissolution Behavior of Complex Carbonitrides in a Microalloyed Steel (Microalloyed 강에서 복합 탄질화물의 재용해 거동)

  • Jung, Jae-Gil;Park, June-Soo;Ha, Yang-Soo;Lee, Young-Kook;Bae, Jin-Ho;Kim, Kisoo
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.6
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    • pp.287-292
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    • 2008
  • Dissolution behavior of complex carbonitrides in a Nb-Ti-V microalloyed steel was quantitatively examined by electrical resistivity, transmission electron microscopy (TEM), and optical microscopy. The electrical resistivity increased with solution treatment temperature up to $1250^{\circ}C$ for a holding time of 15 min. But, an increasing rate of electrical resistivity with temperature was obviously decreased above $1150^{\circ}C$. As the solution treatment temperature increases, irregular shaped Nb-rich carbonitrides disappear and cuboidal Ti-rich carbonitrides are observed. Abnormal grain growth occurs above $1250^{\circ}C$ for a holding time of 15 min. The optimal solution treatment temperature of a Nb-Ti-V microalloyed steel was determined as $1200^{\circ}C$ for a holding time of 15 min.

Sliding Wear of Alumina-silicon Carbide Nanocomposites

  • Kim, Seung-Ho;Lee, Soo-Wohn;Kim, Yun-Ho;Riu, Doh-Hyung;Tohru Sekino;Koichi Niihara
    • Journal of the Korean Ceramic Society
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    • v.38 no.12
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    • pp.1080-1084
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    • 2001
  • Alumina-based nanocomposites have improved mechanical properties such as hardness, fracture toughness and fracture strength compared to monolithic ceramics. In this study, alumina with 5 vol% of nanosized SiC was sintered by a hot pressing technique at 1600$\^{C}$, 30 MPa for 1h in an argon gas atmosphere. Microstructures and mechanical properties in alumina-SiC nanocomposite were investigated. Moreover, tribological properties in air and water were compared each other. Relationships of wear properties with mechanical properties such as hardness, strength, and fracture toughness as well as microstructure were studied. Based on experimental results it was found that nanosized SiC retarded grain growth of matrix alumina. Mechanical properties such as hardness, fracture toughness and strength were improved by the addition of nanosized SiC in alumina. Improved mechanical properties resulted in increased sliding wear resistance. Tribological behavior of nanocomposites in water seemed to be governed by abrasive wear.

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A Study on Elevated Temperature Fracture Behavior of Cracks in 1Cr-0.5Mo Steel Weld (1Cr-0.5Mo강 용접부 균열의 고온파괴거동 연구)

  • 신규인;윤기봉;최현창;박재학;이해무
    • Journal of the Korean Society of Safety
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    • v.12 no.2
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    • pp.45-56
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    • 1997
  • Fracture behavior of ex-serviced 1Cr-0.5Mo steel was measured at room($24^{\circ}C$) and elevated($538^{\circ}C$) temperature and compared with that measured with virgin 1Cr-0.5Mo steel. Compact C(T) specimens were machined from the base and welded test materials. In case of the C(T) specimens of the weld, fatigue precrack was introduced along the fusion line so that following crack growth should occurs along the region of heat affected zone. It was observed that the J-R curve of the serviced material was significantly lower than that of the virgin material at room temperature. Brittle fracture was observed in the serviced material. On the other hand, at elevated temperature no noticeable difference was found between the J-R curves of the virgin and the serviced material. The measured J-R curves were also compared with those of the 1.25Cr-0.5Mo steel obtained from the other literatures. Optical microscopy and SEM examination of the serviced material reveal the carbide in/along the grain boundary which shows material degradation due to long-term usage. An example of application of the measured J-R curves is shown.

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