• Title/Summary/Keyword: grain size

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Effects of Grain Size on High Temperature Deformation Behavior of Sc added Al-Mg Alloy (Sc첨가한 Al-Mg 합금의 고온변형 거동에 미치는 결정립 크기의 영향)

  • Woo, K.D.;Kim, S.W.;Kim, H.S.;Yang, C.H.;Park, H.C.;MIURA, Y.;Park, K.T.
    • Korean Journal of Materials Research
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    • v.12 no.9
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    • pp.701-705
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    • 2002
  • High temperature tensile test has been performed at $450^{\circ}C$ at different strain rate with various grain size due to different reduction rate of Al-4wt%Mg-0.4wt%Sc alloy which is known to be one of useful superplastic alloys. The grain size of Al-4wt%Mg-0.4wt%Sc alloy is $67~100\mu\textrm{m}$ which is courser than that of the alloy which is commonly used as the superplastic material. The total elongation of the Al-4wt%Mg-0.4wt%Sc alloy is strongly dependent on the average grain size, and is a linear function of the inverse average grain size for the present alloy.

Thermal Process Effects on Grain Size and Orientation in (Bi1La1)4Ti3O12 Thin Film Deposited by Spin-on Method (스핀 코팅법으로 증착한 (Bi1La1)4Ti3O12 박막의 후속 열공정에 따른 입자 크기 및 결정 방향성 변화)

  • Kim, Young-Min;Kim, Nam-Kyeong;Yeom, Seung-Jin;Jang, Gun-Eik;Ryu, Sung-Lim;Sun, Ho-Jung;Kweon, Soon-Yong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.7
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    • pp.575-580
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    • 2007
  • A 16 Mb 1T1C FeRAM device was integrated with BLT capacitors. But a lot of cells were failed randomly during the measuring the bit-line signal distribution of each cell. The reason was revealed that the grain size and orientation of the BLT thin film were severely non-uniform. And the grain size and orientation were severely affected by the process conditions of post heat treatment, especially nucleation step. The optimized annealing temperature at the nucleation step was $560^{\circ}C$. The microstructure of the BLT thin film was also varied by the annealing time at the step. The longer process time showed the finer grain size. Therefore, the uniformity of the grain size and orientation could be improved by changing the process conditions of the nucleation step. The FeRAM device without random bit-fail cell was successfully fabricated with the optimized BLT capacitor and the sensing margin in bit-line signal distribution of it was about 340 mV.

Discrimination of Volcanic Ash and Asian Dust (Hwangsa) in Core Sediments from the South Korea Plateau (East Sea) Using Characteristics of Grain-size Distributions (입도 분포 특성을 이용한 동해 남한국대지 시추 퇴적물 중 화산재와 황사의 구분)

  • LEE, HONG-WON;JANG, JUN-HO;BAHK, JANG-JUN
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.26 no.2
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    • pp.135-144
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    • 2021
  • End-member (EM) analysis of grain-size distribution data for detrital fractions of IODP Site U1430 core sediments from the South Korea Plateau (East Sea) identified 4 EMs grain-size populations (EM) which represent either Asian dusts (Hwangsa) or volcanic ashes. The two EMs representing volcanic ashes consist of fine and coarse glass shards with various morphologies and constitute 0-82% of the total grain-size distributions. The 33% mixing percentage of volcanic ash EMs seems appropriate for a cut-off value for discrimination of grain-size data influenced by volcanic ash input from those dominated by Hwangsa.

Grain size, crystalline phase and fracture toughness of the monolithic zirconia

  • Bocam, Kodchakorn;Anunmana, Chuchai;Eiampongpaiboon, Trinuch
    • The Journal of Advanced Prosthodontics
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    • v.14 no.5
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    • pp.285-293
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    • 2022
  • PURPOSE. This study evaluated the relationship among translucency, crystalline phase, grain size, and fracture toughness of zirconia. MATERIALS AND METHODS. Four commercial zirconia - Prettau®Anterior® (PA), Prettau® (P), InCorisZI (ZI), and InCorisTZI (TZI)- were selected for this study. The bar specimens were prepared to determine fracture toughness by using chevron notched beam method with four-point bending test. The grain size was evaluated by a mean linear intercept method using a scanning electron microscope. X-ray diffraction and Rietveld refinement were performed to evaluate the amount of tetragonal and cubic phases of zirconia. Contrast ratio (CR) was measured to investigate the level of translucency. RESULTS. PA had the lowest fracture toughness among other groups (P < .05). In addition, the mean fracture toughness of P was significantly less than that of ZI, but there was no difference compared with TZI. Regarding grain size measurement, PA had the largest average grain size among the groups. P obtained larger grain size than ZI and TZI (P < .05). However, there was no significant difference between ZI and TZI. Moreover, PA had the lowest CR value compared with the other groups (P < .05). This means PA was the most translucent material in this study. Rietveld refinement found that PA presented the greatest percentage of cubic phase, followed by TZI, ZI, and P, respectively. CONCLUSION. The different approaches are used by manufacturers to fabricate various types of translucent zirconia with different levels of translucency and mechanical properties, which should be concerned for material selection for successful clinical outcome.

Grain Size Characteristics of the Asian Dust in Seoul and Relationship to Loess Sediments in the West Coast of Korea during the Spring (봄철 서울 지역에 발생한 황사의 입도 특성과 뢰스와의 관련성)

  • YOON, Soon-Ock;PARK, Chung-Sun;HWANG, Sangill
    • Journal of The Geomorphological Association of Korea
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    • v.17 no.3
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    • pp.77-88
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    • 2010
  • The grain size characteristics of the Asian Dust(AD) in Seoul during the spring 2010 are analyzed by the different pretreatment procedures. The mean values of the AD samples by the minimal dispersion are 19~56㎛ and the NAD(Non-Asian Dust) samples are 37~92㎛. Contrastively, the mean values of AD and NAD samples by the ultimate dispersion are 13~20㎛ and 14~30㎛, respectively. It is revealed that the particles less than approximately 20㎛ and 40㎛ by the minimal and ultimate dispersion, respectively, are introduced into the atmosphere in the Korean Peninsular by the AD events with the peaks of approximately 0.5㎛, 1.5㎛ and 8.5㎛ by the minimal dispersion, and 0.5㎛ and 7.5㎛ by the ultimate dispersion. Also, the charateristics of AD samples showing similar grain size characteristics to the loess samples rather than the NAD samples indicates long distance origin from China so on. The differences of grain size characteristics between the AD and loess samples may result in duration and intensity of weathering processes.

Characteristics of Grain Size Distribution of River Flooding Sediments in Ibang-myeon, Changnyeong and their Meaning (창녕 이방면 하천범람 퇴적물 입도분포 특성 및 그 의미)

  • Han, Min;Yang, Dong-Yoon;Lim, Jaesoo;Nahm, Wook-Hyun
    • Journal of The Geomorphological Association of Korea
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    • v.27 no.3
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    • pp.13-24
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    • 2020
  • This study analyzed the characteristics of the grain size distribution of the sediments obtained from the flooding in Ibang-myeon, Changnyeong-gun, which was caused by the collapse of a embarkment on the Nakdong River on August 9, 2020. As a results, it was found that the mean grain size decreases and the sorting becomes poorer as the distance from the embarkment collapse point increases. This is attributed to the fact that the transport energy of the river decreases when flooding occurs, ensuring that coarse-grained sediments are deposited first. Further, as the transport energy further reduces and becomes dispersed, the sorting for the fine-grained sediments becomes poor. Considering the characteristics of spatial distribution, sediments along the farm road showed the properties of floodplain deposits that transport to natural levee and back swamp due to river flooding. On the other hand, sediments along the irrigation ditch exhibited the properties of the deposits that are carried by the flow backward of ditch from the river after the collapse of the embarkment. The results of this study are significant because characteristics of flood sediments were elucidated for major rivers where flooding rarely occurs due to the recently built artificial structures. In addition, by applying the grain size distribution characteristics of present river flood sediments, it will be able to contribute to clarifying the sedimentary environments of the paleo river flood deposits.

Effects of Microstructure on the Fatigue Crack Propagation Resistance in Dual Phase Steel (複合組織鋼 의 피勞균열進展抵抗 에 미치는 微視組織 의 영향)

  • 김정규;황돈영;박승락
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.8 no.1
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    • pp.34-40
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    • 1984
  • In this study, martensite-ferrite dual phase steel composed of martensite in hard phase and ferrite in soft phase is made as model material, and the difference of fatigue crack propagation behavior resulted from the structural size is investigated by fracture mechanics and microstructural method. The main results obtained are as follows; 1)Fatigue crack propagation rate is influenced by ferrite grain size. In other words, in the low .DELTA. K region fatigue crack propagation rate is decreased with decreasing of grain size but the difference of propagation rate resulted from the structural size is decreased as .DELTA.K is increased. 2)The above result is explained by the degree of crack arrest effect of second phase for fatigue crack propagation depending on the ratio of reversed plastic zone size to ferrite grain size.

Computer Simulation for Microstructure Development in Porous Sintered Compacts (다공질 소결체의 조직형성에 관한 컴퓨터 시뮬레이션)

  • Shin, Soon-Ki;Matsubara, Hideaki
    • Journal of the Korean Ceramic Society
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    • v.43 no.4 s.287
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    • pp.213-219
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    • 2006
  • A Monte Carlo simulation based on Potts model in a three dimensional lattice was studied to analyze and design microstructures in porous sintered compacts such as porosity, pore size, grain (particle) size and contiguity of grains. The effect of surface energy of particles and the content of additional fine particles to coarse particles on microstructure development were examined to obtain fundamentals for material design in porous materials. It has been found that the larger surface energy enhances sintering (necking) of particles and increases contiguity and surface energy does not change pore size and grain size. The addition of fine particles also enhances sintering of particles and increases contiguity, but it has an effect on increment of pore size and grain size. Such a simulation technique can give us important information or wisdom for design of porous materials, e.g., material system with high surface energy and fine particle audition are available for higher strength and larger porosity in porous sintered compacts with applications in an automobile.

Microstructural Characterization of Gas Atomized Copper-Iron Alloys with Composition and Powder Size

  • Abbas, Sardar Farhat;Kim, Taek-Soo
    • Journal of Powder Materials
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    • v.25 no.1
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    • pp.19-24
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    • 2018
  • Cu-Fe alloys (CFAs) are much anticipated for use in electrical contacts, magnetic recorders, and sensors. The low cost of Fe has inspired the investigation of these alloys as possible replacements for high-cost Cu-Nb and Cu-Ag alloys. Here, alloys of Cu and Fe having compositions of $Cu_{100-x}Fe_x$ (x = 10, 30, and 50 wt.%) are prepared by gas atomization and characterized microstructurally and structurally based on composition and powder size with scanning electron microscopy (SEM) and X-ray diffraction (XRD). Grain sizes and Fe-rich particle sizes are measured and relationships among composition, powder size, and grain size are established. Same-sized powders of different compositions yield different microstructures, as do differently sized powders of equal composition. No atomic-level alloying is observed in the CFAs under the experimental conditions.

Analysis on the Grain Growth of PLZT Ceramics (PLZT세라믹스에서의 입성장 분석)

  • 송병무;김도연
    • Journal of the Korean Ceramic Society
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    • v.25 no.4
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    • pp.329-334
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    • 1988
  • Kinetics of grain growth in PLZT ceramics during isothermal heat treatment and hot-pressing were investigated and the published data on grain growth were reanalyzed. It was found, in many cases, that the errors were introduced by ignoring the initial grain size. The grain growth of PLZT ceramics was confirmed to follow the parabolic normal growth : D2-Do2=Kt.

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