• Title/Summary/Keyword: grain

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Determination of Material Parameters for Microstructure Prediction Model of Alloy 718 Based on Recystallization and Grain Growth Theories (재결정 및 결정립 성장이론에 기초한 Alloy 718의 조직예측 모델에 대한 재료상수 결정방법)

  • Yeom, J.T.;Hong, J.K.;Kim, J.H.;Park, N.K.
    • Transactions of Materials Processing
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    • v.20 no.7
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    • pp.491-497
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    • 2011
  • This work describes a method for determining material parameters included in recrystallization and grain growth models of metallic materials. The focus is on the recrystallization and grain growth models of Ni-Fe based superalloy, Alloy 718. High temperature compression test data at different strain, strain rate and temperature conditions were chosen to determine the material parameters of the model. The critical strain and dynamically recrystallized grain size and fraction at various process conditions were generated from the microstructural analysis and strain-stress relationships of the compression tests. Also, isothermal heat treatments were utilized to fit the material constants included in the grain growth model. Verification of the determined material parameters is carried out by comparing the average grain size data obtained from other compression tests of the Alloy 718 specimens with the initial grain size of $59.5{\mu}m$.

Altered Fine Structure of Amylopectin Is Induced by Exogenous Gibberellin During Rice Grain Ripening

  • Kim, Sang-Kuk;Park, Shin-Young;Lee, Sang-Chul;Lee, In-Jung
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.51 no.6
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    • pp.523-526
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    • 2006
  • When $GA_{4}$ was applied to heading stage, it was examined to understand the change of plant hormones and starch during grain filling and ripening. Exogenous gibberellin caused a dramatic decrease in endogenous ABA content. Endogenous $GA_{4}$ content in both superior and inferior part was more promoted in $GA_{4}-treated$ rice grain than in the control. $GA_{1}$ content of an inferior part was not detected in the control and $GA_{4}-treated$ rice otherwise $GA_{4}$ was detected in all grain parts. Ripened grain rate in $GA_{4}-treated$ rice grain was lower than that of the control plant. Amylopectin from $GA_{4}-treated$ grain contained more very short chains with degree of polymerization (DP) between 4 and 8 than amylopectin from the control plant. It suggests strongly that fine structure of rice endosperm may be changed by exogenously applied $GA_{4}$ in rice plants.

Chaff-outlet Grain Loss of Head-feed Combine -Development of a Monitor for Detecting Chaff-outlet Grain Loss of Head-feed Combine- (자탈형(自脱型) 콤바인의 배진손실(排塵損失)에 관(關)한 연구(硏究)(I) -자탈형(自脱型) 콤바인의 배진손실(排塵損失) 모니터 개발-)

  • Chung, C.J.;Choe, J.S.;Choi, Y.S.
    • Journal of Biosystems Engineering
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    • v.14 no.4
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    • pp.251-261
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    • 1989
  • The amount of grain loss incurred during harvesting operation through the chaff-outlet of combine may not be negligible. To minimize this grain loss and optimize condition of combining, it may be necessary that the amount of chaff-outlet loss dependent on varying crop condition is to be estimated as exactly as possible. This study was thus intended to develop the monitor that could indicate the amount of grain loss occurred through the chaff-outlet of combine during harvesting operation. The function of this monitor is to measure at the sounding board the impact sound of paddy kernels which could be distinguished from those of other threshing products through chaff-outlet, and from vibration or noise created by the combine engine and other moving parts. To develop such monitor, the frequency distributions of each sound generated by the impact of grain and chaff, the sound generated by the impact of the mixture of grain and chaff, and vibration or noise created by the combine engine and other moving parts were investigated experimentally. From the results of frequency analyses, the trainsducer adequate for the monitering system was selected and sounding board was constructed. The grain loss monitor thus obtained was tested by attaching the sounding board to the chaff-outlet of combine.

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Preparation of Yttria-stabilized Zirconia with Irregular Grain Shapes by Ceria Doping (CeO$_2$ 도핑에 의한 불규칙 입자형상의 이트리아 안정화 지르코니아 제조)

  • Lee, Jong-Kook;Kang, Hyun-Hee;Kim, Young-J.;Kim, Hwan
    • Journal of the Korean Ceramic Society
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    • v.35 no.12
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    • pp.1294-1300
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    • 1998
  • Yttria-stabilized zirconia ceramics with irregular grain shapes and curved grain boundaries was prepared by ceria doping. The amount of ceria doped into zirconia compacts by a dipping method were at range of 2 to 20 mol% Irregular grain shapes and curved grain boundaries were formed only inspecimens doped with more than 8mol% cerial. Ceria-doped specimens showed large grain size and low sintered density compared with pure yttria-stabilized zirconia which was due to the increase in the contents of stabilizer and cubic phase. The amount of doped ceria was larger on the surface than the inside regions and therefore mi-crostructure and phase on the surface were different from those in the inside regions. Transgranular frac-ture mode was observed ion ceria doped specimens due to irregular large grain sizes.

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Austenite Grain Growth Prediction Modeling of C-Mn-Mo-Ni Steel HAZ Considering Precipitates (C-Mn-Mo-Ni강 용접열영향부의 석출물을 고려한 오스테나이트 결정립 성장 거동 예측)

  • 서영대;엄상호;이창희;김주학;홍준화
    • Journal of Welding and Joining
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    • v.20 no.5
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    • pp.78-86
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    • 2002
  • A metallurgical model for the prediction of prior austenite grain size considering the dissolution kinetics of M$_3$C precipitates at the heat affected zone of SA508-cl.3 was proposed. The isothermal kinetics of grain growth and dissolution were respectively described by well-known equation, $dD/dT=M({\Delta}F_{eff})^M$ and Whelan's analytical model. The isothermal grain growth experiments were carried out for measure the kinetic parameters of grain growth. The precipitates of the base metal and the specimens exposed to thermal cycle were examined by TEM-carbon extraction replica method. The model was assessed by the comparison of BUE simulation experiments and showed good consistencies. However, there was no difference between the model considering and ignoring $M_3C$ precipitates. It seems considered that pinning force exerted by $M_3C$ Precipitates was lower than driving force for grain growth due to large size and small fraction of precipitates, and mobility of grain boundary was low in the lower temperature range.

PCR-based Identification of Microorganisms in a Kefir Grain

  • Koo, Won Hoe;Seo, Min-Gook;Ahn, Jung Hoon
    • Journal of Marine Bioscience and Biotechnology
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    • v.2 no.4
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    • pp.238-244
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    • 2007
  • Nowadays many people are concerned about being healthy, and many dairy products are taken as health supplementary foods. Among dairy products, kefir, also called as Tibet mushroom, is a yogurt fermented by kefir grain, which is a mixture of lactic acid bacteria and yeasts. Although there are many empirical evidences that kefir is very influential for human body, the exact reason is not definitively discovered. Therefore, it would be useful to understand characteristics of a kefir grain and to categorize bacteria in a kefir grain. In this paper, molecular biological apparatus such as PCR, electrophoresis, PCR purification, DNA sequencing were used to identify and classify the species of lactic acid bacteria and yeast in a kefir grain. We used PCR-based identification method using 16S rRNA primer and Internal Transcribed Spacer (ITS) primer. We identified 6 different species which were selected on different medium. In addition, observation with scanning electron microscope (SEM) enabled us to grasp an external shape of the kefir grain. Although we found a limited number of microbial species, more intensive research are needed for extensive identification of microorganism species in Korean kefir grain.

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Experimental Investigation on Particle Size of Soils Erodible by Wind using Portable Wind Erosion Tunnel (소형 풍동을 이용한 토양의 풍식 가능 입경 분석)

  • Kim, Tae-Wan;Son, Young-Hwan;Min, Seul-Gi;Lee, In-Bok;Hong, Se-Woon;Kim, Min Young
    • Journal of The Korean Society of Agricultural Engineers
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    • v.55 no.6
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    • pp.127-133
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    • 2013
  • The purpose of this study was to investigate maximum and minimum grain size which eroded by wind according to soil and wind conditions, such as top soil water content, roughness, land slope, wind velocity and proportion of grain size under 0.84mm. For performing this study, portable wind erosion tunnel was designed and utilized during field test, which facilitated measuring actual wind erosions under artificially controlled wind conditions. In the result, maximum, minimum grain size had strong negative correlation with roughness while weak positive correlation with wind velocity. Also, Slope which means the effect of gravity also influence grain size erodible by winds. Based on these results, regression equations were suggested for predicting maximum and minimum grain sizes by using multiple linear regression analysis from SPSS 20.0. The equation for maximum grain size erodible by winds showed a good agreement with the observed data with $R^2$=0.896. Other equation for minimum grain size had $R^2$=0.777.

Microstructure and Electrical Properties of $SiO_2$-Doped Zinc Oxide Varistors ($SiO_2$가 첨가된 산화아연 바리스터의 미세구조 및 전기적 특성)

  • 남춘우;정순철
    • Electrical & Electronic Materials
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    • v.10 no.7
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    • pp.659-667
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    • 1997
  • The influence of SiO$_2$on the microstructure and electrical properties of zinc oxide varistor was investigated. Zn$_2$SiO$_4$third phase in the sintered body was found at grain boundaries, multiple grain junctions, and occasionally within ZnO grains. This phase acted as a grain growth inhibitor, which retard the grain growth of the ZnO matrix by impeding migration on the grain boundaries. As SiO$_2$ addition increases, average grain size decreased from 40.6${\mu}{\textrm}{m}$ to 26.9${\mu}{\textrm}{m}$ due to the pinning effect by Zn$_2$SiO$_4$ and drag effect by Si segregation at grain boundaries, the breakdown voltage consequently increased. When SiO$_2$ addition is increased, interface state density decreased, however, the barrier height increased by decrease of donor concentration, as a result, the nonlinear exponent increased and leakage current decreased. While, as SiO$_2$ addition increase, it was found that the apparent dielectric loss factor shows a tendency of decrease. Wholly, electrical properties of zinc oxide varistor can be said to be improved by SiO$_2$addition.

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Preparation and Crystalline Growth Properties of Diamond Thin Film by Microwave Plasma CVD (MWPCVD법에 의한 다이아몬드 박막의 제조 및 결정성장 특성)

  • ;;A. Fujishima
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.905-908
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    • 2000
  • The growth properties of diamond grain were examined by Raman spectroscopy and microscope images. Diamond thin films were prepared on single crystal Si wafers by microwave Plasma chemical vapor deposition. Preparation conditions, substrate temperature, boron concentration and deposition time were controlled differently. Prepared diamond thin films have different surface morphology and grain size respectively Diamond grain size was gradually changed by substrate temperature. The biggest diamond grain size was observed in the substrate, which has highest temperature. The diamond grain size by boron concentration was slightly changed but morphology of diamond grain became amorphous according to increasing of boron concentration. Time was also needed to be a big diamond grain. However, time was not a main factor for being a big diamond grain. Raman spectra of diamond film, which was deposited at high substrate temperature, showed sharp peaks at 1334$cm^{-1}$ / and these were characteristics of crystalline diamond. A broad peak centered at 1550$cm^{-1}$ /, corresponding to non-diamond component (sp$^2$carbon), could be observed in the substrate, which has low temperature.

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Development of a Mechanistic Fission Gas Release Model for LWR $UO_2$ Fuel Under Steady-State Conditions

  • Koo, Yang-Hyun;Sohn, Dong-Seong
    • Nuclear Engineering and Technology
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    • v.28 no.3
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    • pp.229-246
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    • 1996
  • A mechanistic model has been developed to predict the release behavior of fission gas during steady-state irradiation of LWR UO$_2$ fuel. Under the assumption that UO$_2$ grain surface is composed of fourteen identical circular faces and grain edge bubble can be represented by a triangulated tube around the circumference of three circular grain faces, it introduces the concept of continuous formation of open grain edges tunnels that is proportional to grain edge swelling. In addition, it takes into account the interaction between the gas release from matrix to grain boundary and the reintroduction of gas atoms into the matrix by the irradiation-induced re-solution of grain face bubbles. It also treats analytically the behavior of intragranular, intergranular, and grain edge bubbles under the assumption that both intragranular and intergranular bubbles are uniform in both radius and number density. Comparison of the present model with experimental data shows that the model's prediction produces reasonable agreement for fuel with centerline temperatures of 1000 to 140$0^{\circ}C$, wide scatter band for fuel with centerline temperatures lower than 100$0^{\circ}C$, and underprediction for fuel with centerline temperatures higher than 140$0^{\circ}C$.

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