• 제목/요약/키워드: grain

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용접 열영향부 미세조직 및 재질예측 모델링: II. Fe-C-Mn 강에서 페라이트 결정립크기의 영향을 고려한 Austenitization kinetics 및 오스테나이트 결정립크기 예측모델 (Prediction Model for the Microstructure and Properties in Weld Heat Affected Zone: II. Prediction Model for the Austenitization Kinetics and Austenite Grain Size Considering the Effect of Ferrite Grain Size in Fe-C-Mn Steel)

  • 유종근;문준오;이창희;엄상호;이종봉;장웅성
    • Journal of Welding and Joining
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    • 제24권1호
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    • pp.77-87
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    • 2006
  • Considering ferrite grain size in the base metal, the prediction model for $A_{c3}$ temperature and prior austenite grain size at just above $A_{c3}$ temperature was proposed. In order to predict $A_{c3}$ temperature, the Avrami equation was modified with the variation of ferrite grain size, and its kinetic parameters were measured from non-isothermal data during continuous heating. From calculation using a proposed model, $A_{c3}$ temperatures increased with increasing ferrite grain size and heating rate. Meanwhile, by converting the phase transformation kinetic model that predicts the ferrite grain size from austenite grain size during cooling, a prediction model for prior austenite grain size at just above the $A_{c3}$ temperature during heating was developed.

Ti$_3$SiC$_2$의 소성 변형 특성에 미치는 결정립 크기의 효과 (Effect if Grain Size on Plasticity of Ti$_3$SiC$_2$)

  • 이승건
    • 한국세라믹학회지
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    • 제35권8호
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    • pp.807-812
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    • 1998
  • Mechanical properties of two types of polycrystlline {{{{ { { Ti}_{3 }SiC }_{2 } }} with different grain size were investigated. A fine grain {{{{ { { Ti}_{3 }SiC }_{2 } }} has a higher fracture strength and hardness. Plot of strength versus Vickers indentation load indicated that {{{{ { { Ti}_{3 }SiC }_{2 } }} has a high flaw tolerance. Hertzian indentation test using a spherical indenter was used to study elastic and plastic behavior in {{{{ { { Ti}_{3 }SiC }_{2 } }}. Indentation stress-strain curves of each material are made to evaluate the plasticity of {{{{ { { Ti}_{3 }SiC }_{2 } }} Both find and coarse grain {{{{ { { Ti}_{3 }SiC }_{2 } }} showed high plasticity. In-dentation stress-strain curve of coarse grain {{{{ { { Ti}_{3 }SiC }_{2 } }} deviated even more from an ideal elastic limit in-dicating exceptional plasticity in this material. Deformation zones were formed below the contact as well as around the contact area in both materials but the size of deformation zone in coarse grain {{{{ { { Ti}_{3 }SiC }_{2 } }} was much larger than that in fine grain {{{{ { { Ti}_{3 }SiC }_{2 } }} Intragrain slip and kink would account for high plasticity. Plastic behavior of {{{{ { { Ti}_{3 }SiC }_{2 } }} was strongly influenced by grain size.

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Radiation induced grain boundary segregation in ferritic/martensitic steels

  • Xia, L.D.;Ji, Y.Z.;Liu, W.B.;Chen, H.;Yang, Z.G.;Zhang, C.;Chen, L.Q.
    • Nuclear Engineering and Technology
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    • 제52권1호
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    • pp.148-154
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    • 2020
  • The radiation induced segregation of Cr at grain boundaries (GBs) in Ferritic/Martensitic steels was modeled assuming vacancy and interstitialcy diffusion mechanisms. In particular, the dependence of segregation on temperature and grain boundary misorientation angle was analyzed. It is found that Cr enriches at grain boundaries at low temperatures primarily through the interstitialcy mechanism while depletes at high temperatures predominantly through the vacancy mechanism. There is a crossover from Cr enrichment to depletion at an intermediate temperature where the Cr:Fe vacancy and interstitialcy diffusion coefficient ratios intersect. The bell-shape Cr enrichment response is attributed to the decreasing void sinks inside the grains as temperature rises. It is also shown that low angle grain boundaries (LAGBs) and special Σ coincidence-site lattice (CSL) grain boundaries exhibit suppressed radiation induced segregation (RIS) response while high angle grain boundaries (HAGBs) have high RIS segregation. This different behavior is attributed to the variations in dislocation density at different grain boundaries.

Field-Induced Translation of Single Ferromagnetic and Ferrimagnetic Grain as Observed in the Chamber-type μG System

  • Kuwada, Kento;Uyeda, Chiaki;Hisayoshi, Keiji;Nagai, Hideaki;Mamiya, Mikito
    • Journal of Magnetics
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    • 제18권3호
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    • pp.308-310
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    • 2013
  • Translation induced by the field-gradient force is being observed for a single ferromagnetic iron grain and a ferrimagnetic grain of a ferrite sample ($CuFe_2O_4$). From measurements on the translation, precise saturated magnetization of $M_S$ is possible for a single grain. The method is based on the energy conservation rule assumed for the grain during its translation and the grain is translated through a diffuse area under microgravity conditions. The results of the two materials indicate that a field-induced translation of grain bearing spontaneous moment is generally determined by a field-induced potential $-mM_SH(x)$ where m denotes the mass of sample. According to the above translations, the detection of $M_S$ is not interfered by any signals from the sample holder. The $M_S$ measurement does not require m value. By observing translations resulting from fieldinduced volume forces, the magnetization of a single grain is measurable irrespective of its size; the principle is also applicable to measuring susceptibility of diamagnetic and paramagnetic materials.

미립 절대밀도의 품종간 변이 및 몇가지 미립형질과의 관계 (Varietal Variations in Absolute Density of Rice Grain and Its Relations with Other Grain Characters)

  • Hee Jong, Koh;Mun Hue, Heu;Cheng Mo, Jiang
    • 한국작물학회지
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    • 제37권3호
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    • pp.244-249
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    • 1992
  • 벼 품종간 미립 절대밀도의 변이와 그에 영향하는 미립관련형질들을 구명하기 위하여 통일형 30, Japonica형 72 및 Indica형 133 계 235 품종에 대해 미립의 절대밀도와 모양 및 크기, 경도, 심복백, ADV, amylose 함량, 전분구조를 조사하고 그들 간의 관계를 검토한 결과는 다음과 같다. 1. 백미의 절대밀도는 평균적으로 통일형 1.496g/$cm^3$, Japonica형 1.506g/$cm^3$, Indica형 1.500g/$cm^3$이었고, 출수까지의 생육일수 및 현미의 경도와는 정의 상관을 심복백, 현미의 부피 및 1000립중, 입장과는 부의 상관을 보였다. 2. 편회귀분석 결과 미립의 크기가 절대밀도에 가장 크게 영향하는 것으로 나타났다. 3. 절대밀도의 고, 저에 따른 전분결정구조의 차이는 감별할 수 없었으며, 심복백의 경우 정상배유부분에 비해 전분립자가 둥글고 그 결정조직이 느슨하였다. 4. 미립의 크기가 비슷하고 심복백이 없는 경우 절대밀도의 품종간 차이는 미미한 것으로 나타나서 수량성에는 크게 영향하지 못할 것으로 생각되나, 미질의 측면에서는 검토되어져야 할 것이다.

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INTERGRANULAR CORROSION-RESISTANT STAINLESS STEEL BY GRAIN BOUNDARY ENGINEERING

  • Hiroyuki Kokawa;Masayuki Shimada;Wang, Zhan-Jie;Yutaka S. Sato
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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    • pp.250-254
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    • 2002
  • Intergranular corrosion of austenitic stainless steels is a conventional and momentous problem during welding and high temperature use. One of the major reasons for such intergranular corrosion is so-called sensitization, i.e., chromium depletion due to chromium carbide precipitation at grain boundaries. Conventional methods for preventing sensitization of austenitic stainless steels include reduction of carbon content in the material, stabilization of carbon atoms as non-chromium carbides by the addition of titanium, niobium or zirconium, local solution-heat-treatment by laser beam, etc. These methods, however, are not without drawbacks. Recent grain boundary structure studies have demonstrated that grain boundary phenomena strongly depend on the crystallographic nature and atomic structure of the grain boundary, and that grain boundaries with coincidence site lattices are immune to intergranular corrosion. The concept of "grain boundary design and control", which involves a desirable grain boundary character distribution, has been developed as grain boundary engineering. The feasibility of grain boundary engineering has been demonstrated mainly by thermomechanical treatments. In the present study, a thermomechanical treatment was tried to improve the resistance to the sensitization by grain boundary engineering. A type 304 austenitic stainless steel was pre-strained and heat-treated, and then sensitized, varying the parameters (pre-strain, temperature, time, etc.) during the thermomechanical treatment. The grain boundary character distribution was examined by orientation imaging microscopy. The intergranular corrosion resistance was evaluated by electrochemical potentiokinetic reactivation and ferric sulfate-sulfuric acid tests. The sensitivity to intergranular corrosion was reduced by the thermomechanical treatment and indicated a minimum at a small roll-reduction. The frequency of coincidence-site-lattice boundaries indicated a maximum at a small strain. The ferric sulfate-sulfuric acid test showed much smaller corrosion rate in the thermomechanically-treated specimen than in the base material. An excellent intergranular corrosion resistance was obtained by a small strain annealing at a relatively low temperature for long time. The optimum parameters created a uniform distribution of a high frequency of coincidence site lattice boundaries in the specimen where corrosive random boundaries were isolated. The results suggest that the thermomechanical treatment can introduce low energy segments in the grain boundary network by annealing twins and can arrest the percolation of intergranular corrosion from the surface.

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국내산 낙엽송집성재의 지압특성 (Bearing Properties of Domestic Larix Glulam)

  • 김건호;홍순일
    • Journal of the Korean Wood Science and Technology
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    • 제36권4호
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    • pp.93-101
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    • 2008
  • 하중방향(섬유평행방향, 섬유직각방향)과 접합구(볼트, 드리프트 핀) 적층면방향(평행, 수직)에 따른 국내산 낙엽송집성재의 지압강도시험을 실시하였다. 지압시편은 5 ply의 집성재를 사용하였고, 접합구의 직경은 12, 16, 20 mm를 사용하였다. 시험결과는 다음과 같다. 1) 볼트와 드리프트 핀의 각 직경에 따른 평균최대지압강도는 섬유평행하중방향의 경우 비슷한 경향을 보였으며, 섬유평행하중방향의 평균최대지압강도가 섬유직교방향보다 1.50~2.31배 높게 나타났다. 평균지압강도의 경우 섬유평행하중방향시편은 직경 16 mm에서 20 mm로 증가할 때 20% 감소하였으며, 섬유직교방향은 뚜렷한 경향이 없었다. 2) 평균지압초기강성의 경우 섬유평행하중방향은 직경 16 mm일 때 가장 크게 나타났다. 드리프트 핀 접합부의 전단강도실험 시 초기강성과 평균지압초기강성은 직경이 증가할수록 비슷한 경향을 보였다. 3) 지압강도시험 시 섬유평행방향시편의 파괴형상은 직경이 작을수록 할렬파단을 보였다. 섬유직교방향의 시편은 대부분이 섬유평행방향으로 할렬파단이 일어났으며 볼트가 드리프트 핀 시편보다 더 많이 나타났다. 4) 지압강도예측식을 통해 구한 예측지압강도와 실제 5% 유사항복지압강도를 비교하였을 경우 섬유평행방향은 KBCS, NDS의 예측지압강도와 비슷하게 나타났으나, 섬유직교방향은 NDS에서 제안한 예측식이 잘 적용되는 것을 알 수 있었다.

이방성 결정립 계면에너지의 2차원 결정립 성장에 미치는 효과에 대한 컴퓨터 모사 (Computer simulation of the effects of anisotropic grain boundary energy on grain growth in 2-D)

  • 김신우
    • 한국결정성장학회지
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    • 제22권4호
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    • pp.178-182
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    • 2012
  • 결정립 성장은 여러 가지 재료의 성질에 미치는 큰 영향으로 재료공학에서 매우 중요하다. 그래서 본 연구에서는 PC에서 대규모 상장 모델을 사용하여 이방성 결정립 계면에너지의 2차원 결정립 성장에 미치는 효과를 조사하였다. 컴퓨터 모사에서는 $2000{\times}2000$의 그리드 시스템과 약 7300개의 초기 결정립 개수가 사용되었다. 결정립계 에너지의 이방성의 비, ${\sigma}_{max}/{\sigma}_{min}$는 1부터 3까지 변경되었다. 이방성이 증가함에 따라 결정립 성장 지수, n은 2.05에서 2.37로 증가하였다. 결정립 크기의 분포는 등방성인 경우에는 중앙에 평탄한 영역을 보였으나 이방성의 경우에는 중앙의 평탄한 영역이 사라지고 매우 느리게 사라지는 작은 결정립에 기인하여 작은 결정립 크기의 분포가 약간 증가하였다. 마지막으로 모사된 결정립 미세구조가 이방성에 따라 비교, 분석되었다.

Influence of Ripening Stages on the Quality of Whole Crop Silage and Grain Silage of Fodder Rice

  • Maruyama, S.;Yokoyama, I.;Asai, H.;Sakaguchi, S.;Ohtani, T.;Yokota, H.;Kita, K.
    • Asian-Australasian Journal of Animal Sciences
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    • 제18권3호
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    • pp.340-344
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    • 2005
  • In high-income Asian countries like Korea and Japan, per capita rice consumption has declined because of the change in consumer' favorite foods from rice to high-cost quality foods. This has forced farmers to reduce rice production. Although fodder rice could be another option to be cultured by farmers, available information concerning rice grain silage has been limited. In the present study, therefore, the difference in the quality of fodder rice silage prepared from either whole crop or grain at different ripening stages was compared. Various supplements were also added into whole crop and grain silages of fodder rice before ensiling, and thereafter, the palatability of prepared silages was determined by beef cattle. At ear emergence stage, the pH values for both grain and whole crop silages were approximately 4.5. In both grain and whole crop silages, the pH values were significantly increased by progressing ripening stages from milk-ripe stage to yellow-ripe stages, and the increase in pH value for grain silage was faster than that for whole crop silage. In the grain silage, the higher lactic acid (LA) content in grain silage seemed to be, the lower pH value was. Both in grain and whole crop silages, pH was significantly decreased by supplementation with LA bacteria. There were no significant differences in feed intake among any treatment groups.

투입식 탈곡기의 탈곡 및 선별 성능에 관한 연구 (Study on the Threshing and Separating Performanee of the Newly Developed Throw-in Type Thresher)

  • 이승규;정창규김성래
    • 한국농공학회지
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    • 제17권3호
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    • pp.3878-3884
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    • 1975
  • This study was carried out to develop the throw-in type thresher with its size as small as possible. Developing the smallest possible size of the throw-in type thresher has been very important to increase mobility and to reduce the machine price. The thresher that developed for this purpose was tested as to threshing and separation performance for the samples collected in eight catch boxes under the concave while threshing. The amount of grain collected in each compartments was measured and the threshing and separating pattern along the total span of the threshing drum was determined. The performance of separating and threshing units of the test thresher and threshing loss was evaluated by use of the developed grain separating apparatus and the method for measuring the grain separating performance of threshers. The results are summarized as follows; 1. The unthreshed grain (drum losses) and semi-threshed grain did not appeared at all throughout the treatments. 2. When threshed by making use of the developed throw-in type thresher, the threshing grain loss at about 25 per cent grain moisture was about one-half when threshed at about 18 per cent grain moisture. 3. And its grain separating loss in higher feed rate was decreased in comparison with that of lower feed rate. These results suggests that the throw-in type thresher may be suitable for wet threshing and for higher feed rate of threshing. 4. Above 60 per cent of total grain passing through concave fell through the screen within a scant 30 cm from the feeding inlet. This threshing pattern may suggest that major threshing action may be finished before about one third of cylinder length. The required separating load extended over the whole drum span is so defferent that separating elements should be redesigned so as to accomodate this variable pattern of separation load. 5. It was apparent from the experiment that the length of the threshing drum of the throw-in type thresher could be reduced from 1285mm to about 1050mm without increasing grain separation loss greatly.

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