• Title/Summary/Keyword: gel strength

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Effect of Washing and Additives on Gel Formation of Squid Surimi

  • LEE Nahm-Gull;CHO Young-Je
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.29 no.6
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    • pp.754-760
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    • 1996
  • Effects of washing and additives on the texture of squid surimi gel which has been known to hard to gelation due to high protease activities and many water solubles were studied by SDS-PAGE, compression test, jelly strength and transmission electron microscopy analysis (TEM). Myosin (205 kDa) heavy chain was the major protein in water soluble fractions. It was impossible to make a gel after washing of the minced squid meat. These results suggested that squid (Todarodes pacificus) minced meat does not need a washing for good jelly products. $3.0\%$ of bovine plasma protein (BPP) produced the hardest gel ($16\%$ harder than the control) among the additives including egg white (EW), potato extracts (PE) and transglutaminase-K (TG-K) by compression test (P>0.05). Microstructure of control, $2\%$ EW and $4\%$ TG-K treated gels showed a sponge-like structure with more vacant space. Gels containing $3\%$ BPP formed the most rigid and arranged networks. Those results indicates that poor gel-network formation Was due to the degradation of myofibrillar proteins by proteases contained in the minced meat, which result in non-interlinkage.

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Morphology and Swelling Behaviors of PVA/Gelatin Blend Membranes Prepared Under High Electric Field (고전장하에서 제조된 PVA/Gelatin 블렌드막의 구조와 팽윤거동)

  • Huh, Yang-Il;Yun, Hyung-Ku
    • Polymer(Korea)
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    • v.30 no.6
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    • pp.563-567
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    • 2006
  • Poly(vinyl alcohol) (PVA) and gelatin (GEL) blend membranes were prepared by solution casting method under a high electric field. SEM observation of the membrane showed that gelatin rich domains were elongated and oriented to the direction of the applied electric field in PVA matrix. This can be attributed to the electrostatic emulsifying effects due to a reduction in interfacial tension. In addition, it was observed through WAXD and swelling measurements that the degree of crystallinity of membranes increased with applied electric field strength. This may be interpreted to be caused by the orientation effect of GEL domains in the blend membrane, and the self-annealing effect due to some heat generated from high electric field during casting.

The Effect of Moisture Absorption and Gel-coating Process on the Mechanical Properties of the Basalt Fiber Reinforced Composite

  • Kim, Yun-Hae;Park, Jun-Mu;Yoon, Sung-Won;Lee, Jin-Woo;Jung, Min-Kyo;Murakami, Ri-Ichi
    • International Journal of Ocean System Engineering
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    • v.1 no.3
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    • pp.148-154
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    • 2011
  • Generally, strength degradation is caused by the absorption of moisture in composites. For this reason, a fracture is generated in the composites and traces of glass fiber degrade human health and physical damage is generated. Therefore, in this research, we studied the mechanical properties change of composites by moistureabsorption. The composites were manufactured with and without the Gel-coating process and were immersed in a moisture absorption device at $80^{\circ}C$ for more than 100 days. The mechanical properties of the moistureabsorption composites and the composites which dry after moisture-absorption were compared. The mechanical properties degradation of basalt fiber composites according to the result of the measurement of moistureabsorption was smaller than that of glass fiber composites by about 20%. In addition, the coefficient of moisture absorption was lower for the case of Gel-coating processing than the composites without the Gel-coating process by about 2% and it was deduced that Gel-coating did not have a significant effect on the mechanical properties.

Quality Characteristics of Mackerel Surimi Prepared by Alkaline Washing under Reduced Pressure (감압 알칼리 수세하여 제조한 고등어 Surimi의 품질 특성)

  • Park, Hyung-Sun;Park, Sang-Woo;Yang, Seung-Taek
    • Korean Journal of Food Science and Technology
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    • v.30 no.5
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    • pp.1120-1127
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    • 1998
  • An attempt was made in this study to investigate the optimum condition of washing for preparation of mackerel surimi by alkaline washing of 1, 3, 5, and 7 times under atmospheric (760), 660, and 560 mmHg pressure. The qualities of surimis were examined by analyzing the factors such as water content, crude lipid, pH, volatile basic nitrogen (VBN), expressible drip, protein extractability, $Mg^{2+}-$, $Ca^{2+}-$ and EDTA-ATPase activity, transglutaminase (TGase) activity, gel strength and color. The contents of moisture, crude lipid, pH and VBN in surimis prepared by alkaline washing under atmospheric, and reduced pressure went up to $72.0{\sim}72.9%$, $4.8{\sim}5.7%$, $6.9{\sim}7.0$ and $6.7{\sim}7.0\;mg/100\;g$, respectively. Protein extractability, ATPase activity and TGase activity were highest in surimis prepared by alkaline washing under 560 mmHg. Gel strengths of surimi setting gel and cooked gel from five times washing under 560 mmHg were 420 g cm (atmospheric, 330 g cm) and 485 g cm (atmospheric, 412 g cm), respectively. For the preparation of mackerel surimi, optimum washing condition was five times washing under 560 mmHg.

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Thermally Induced Gelation of Alaska pollack Meat Paste -2. The states of water in meat paste by gelation- (가열에 의한 명태 연육의 Gel화에 관한 연구 -2. Gel화에 따른 연육내의 물의 거동-)

  • JUNG Woo-Jin;PARK Seong-Min;LEE Kang-Ho;LEE Keun-Tai
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.26 no.3
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    • pp.230-234
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    • 1993
  • In order to obtain the fundamental factors influencing on gelation of Alaska pollack meat paste during processing, the states of water in gel from meat paste were studied using differential scanning calorimetry(DSC) and thermogravimetry(TG). In the differential scanning calorimetry, the calorimetric curves of gels were characterized by single peak through the evaporation of water. Each curve was divided into two divisions below and above $105^{\circ}C(Q_1\;and\;Q_2)$, and a quotient, $R_{105}[={Q_2/(Q_1+Q_2)}+100]$ was adopted to represent the amount of immobilized water in the total water of gels. There was a good correlationships between gel strength values and those quotients($R_{105}$), the correlation coefficient was 0.93. Three types of water(A, B, C) differentiated by evaporating velocity were regarded as free water and it was abundant among the three types of water. The type C water was regarded as the water in so-called mono-molecular layer region. The ratio of the content C versus total water content showed good correlationships with the gel strength and its correlation coefficient was 0.99.

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Properties of Liquid Chemical Grouting Material for Soil Grouting using Non-cement Binder (무시멘트 결합재를 사용한 지반 그라우팅용 약액주입재의 특성)

  • Lee, Jae-Hyun;Kim, Yong-Ro;Kim, Gyu-Yong;Yoon, Seong-Jin;Mun, Kyoung-Ju
    • Journal of the Korea Institute of Building Construction
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    • v.16 no.1
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    • pp.45-52
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    • 2016
  • In this research, characteristic properties of gel time and homo gel strength of liquid chemical grouting material for soil grouting using non-cement binder(NCB) were measured according to kinds of liquid B's Binders, W/B of liquid B's Binders and the volume ratio between liquid A and liquid B in order to examine on the applicability of soil grouting material using non-cement binder. The test was performed using NCB-1, NCB-2, NCB-3 which are environment-friendly inorganic binders developed by means of collaboration by our research team and which are different from chemical composition ratio each other. In conclusion, it was found that NCB could be applied to liquid soil grouting material using non-cement binder and replace ordinary portland cement, because NCB had the most excellent performance in certain section of gel time and homo gel strength in condition of this experiment.

Preparation and Characterization of Hydrogels of PVA and PVP Containing Chitosan by Radiation (방사선에 의한 키토산을 포함하는 PVA와 PVP 하이드로겔의 제조 및 특성)

  • 박경란;노영창
    • Polymer(Korea)
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    • v.25 no.5
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    • pp.728-735
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    • 2001
  • In this study, hydrogels from mixtures of chitosan/poly(vinyl alcohol) (PVA) and chitosan/poly(N-vinylpyrrolidone) (PVP) were prepared by ${\gamma}$-ray irradiation, and the mechanical properties such as gelation, water absorptivity and gel strength were examined to evaluate the applicability of these for wound dressing. The PVA : chitosan and PVP : chitosan ratio were in the range of 97:3 ~ 90:10, and the solid concentration of PVA/chitosan and PVP/chitosan solution were 15 wt%. Gamma irradiation with doses of 25, 35, 50, 60 and 70 kGy, was exposed to mixtures of PVA/chitosan and PVP/chitosan to evaluate the effect of irradiation dose. Gel content and gel strength increased as chitosan concentrations in PVA/chitosan and PVP/chitosan decreased, and as irradiation dose increased. Swelling degree increased as chitosan concentrations in PVP/chitosan and PVA/chitosan increased, and as irradiation dose decreased.

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Formulation and Pharmaceutical Properties of Mucoadhesive Film Containing Dipotassium Glycyrrhizate (구내염증 치료용 구강점막 필름제의 제제설계와 약제학적 성질)

  • Rhee, Gye-Ju;Lee, Duk-Keun;Sin, Kwang-Hyun;Park, Chong-Bum
    • Journal of Pharmaceutical Investigation
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    • v.29 no.2
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    • pp.127-136
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    • 1999
  • In order to eliminate demerits of conventional dosage forms, dipotassium glycyrrhizate was formulated as a slim mucoadhesive film type dosage form. The mucoadhesive drug layer gel containing dipotassium glycyrrhizate was prepared using $Noveon^{\circledR}$ AA-1, hydroxypropylcellulose-M, ethylcellulose N 100 and citric acid, and the protective layer gel by using ethylcellulose N 100, $Eudragit^{\circledR}$ RS and castor oil. The viscosity of drug layer gel of mucoadhesive film was enhanced as the increased amount of $Noveon^{\circledR}$ AA-1 or hydroxypropyl cellulose-M. The drug content was unifonnly $1160{\pm}14.6\;{\mu}g$, and was varied within 3.5%. The optimum film dosage form showed a good fluidity and malleability of drug layer, with 179 g of thickness, pH 5.7, 411 min of in vitro adhesion time and 172 g in gravity adhesive strength. The release time of drug from the mucoadhesive film was significantly shorter but was delayed when polymers such as ethylcellulose was added. From these results, the new mucoadhesive film may be effective for the treatment of aphthous stomatitis.

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Preparation of the Anti-Reflective(AR) Coating Film by Sol-Gel Method to Improve the Efficiency of Solar Cell (태양전지 효율 향상용 졸-겔 법에 의한 반사방지 코팅막의 제조)

  • Kim, Hyosub;Kim, Youngho;Choi, Jaeyune
    • Transactions of the Korean hydrogen and new energy society
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    • v.25 no.2
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    • pp.145-150
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    • 2014
  • This study investigates the preparation of anti-reflective (AR) coating film to improve the efficiency of solar cell. The AR coating film was successfully obtained by dip-coating with AR coatings prepared by sol-gel method. Fluoroalkylsilane was additionally introduced into the coatings to give the self-cleaning effect of AR coating film. We performed the abrasion test, pencil scratch hardness test and cross-cut test to identify the mechanical strength of AR coating film. As the results, the transmittance of AR coating films with 9.07, 18.13 and 27.20 of IPA/MTMS molar ratios were 93.1, 93.6 and 95.3%, respectively. The water contact angle and transmittance of AR coating film increased by the introduction of hydrophobicity. The prepared AR coating film shows the high level of abrasion, hardness and adhesion. The IPA/MTMS molar ratio of 27.20 and the withdrawing speed range of 0.20 ~ 0.28cm/sec are the optimal coating condition in terms of the transmittance and mechanical strength of AR coating film.

Properties and Preparation of PVA/Silica Hybrid Films by Sol-Gel Method (졸-겔법에 의한 PVA/Silica 하이브리드 필름의 제조 및 특성)

  • Kim, Tae-Hyoung;Lee, Jin-Hwa;Lee, Dong-Kyu
    • Journal of the Korean Applied Science and Technology
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    • v.16 no.4
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    • pp.317-322
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    • 1999
  • Transparent films were prepared using the sol-gel process by mixing TEOS with PVA solution that was solved in EtOH and distilled water homogeneously. HCl, $CH_3COOH$ and $NH_4OH$ were used as catalysts of the sol-gel process, and for improving the flexibility of films glycerol was used as plasticizer. In case of each catalyst, transparency and tensile strength were increased, and glass transition temperature (Tg) was shifted to higher temperature with increasing TEOS ratio. Also, in case of adding the plasticizer, the flexibility of films was increased. On the contrary, transparency, thermal stability and tensile strength were decreased with increasing HCl and $NH_4OH$ ratio. Also, the range of being made of film type was expanded when $CH_3COOH$ was used than HCl and $NH_4OH$.