• 제목/요약/키워드: fracture toughness $K_{IC}$

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사이잘 섬유 강화 복합재료의 기계적 특성에 미치는 표면처리와 흡습의 영향 (Effects of Water Absorption and Surface Treatment on Mechanical Properties of Sisal Textile Reinforced Composites)

  • 김효진;서도원;박한주;전양배;임재규
    • 대한기계학회논문집A
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    • 제30권7호
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    • pp.779-786
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    • 2006
  • Woven sisal textile reinforced composites were manufactured to evaluate fracture toughness, and tensile test. All specimens were immersed in water five times. All specimens are immersed in pure water during 9 days at room temperature, and dried in 1 day at $50^{\circ}C$. Two kinds of polymer matrices such as epoxy and vinyl-ester were used. Fractured surface were investigated to study the failure mechanism and fiber/matrix interfacial adhesion. It is shows that it can be enhanced to improve their mechanical performance to reveal the relationship between fracture toughness and water absorption fatigue according to different polymer matrices. Water uptake of the epoxy composites was found to increase with cycle times. Mechanical properties are dramatically affected by the water absorption cycles. Water-absorbed samples observed poor mechanical properties such as lower values of maximum strength and extreme elongation. The $K_{IC}$ values demonstrate a decrease in inclination with increasing cyclic times of wetting and drying fur the epoxy and vinyl-ester.

국산 원자로용기 재료의 피로 및 파괴특성 연구 (A study on the fatigue and fracture characteristics of localized nuclear reactor vessel material)

  • 정순억
    • 대한기계학회논문집A
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    • 제21권10호
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    • pp.1626-1635
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    • 1997
  • It is important to ensure the reliability of the first localized reactor vessel steel. To satisfy with this purpose, a study on the impact/hardness, low cycle fatigue(LCF), crack growth rate(da/dN) and fracture toughness( ) of base material(BM) and weld metal(WM) were performed under room temperature air and corrosion conditions. A summary of the results is as folows : (1) Charpy impact absorbed energy of BM was the highest value, heat affected zoon(HAZ) and the lowest, WM. The hardness of BM was similar to HAZ. (2) Coefficients of Manson equation using the monotonic tensile test data were obtained for the present material. (3) The effects of stress ratio and ambient (120.deg. C and NaCl) condition on da/dN were investigated, da/dN with NaCl condition expressed the highest value. (4) The results of Charpy V-notch impact test had good correlation with $K_{IC}$ characteristics and the lowest curve of $K_{IC}$ for BM was derived, more researches about WM and HAZ are required hereafter.

고무변성 에폭시 수지의 균열진전과정과 음향방출 특성 (Acoustic Emission during Crack Propagation Process of Rubber-Modified Epoxy Resin)

  • 이덕보;김현수;최낙삼;남기우;문창권
    • Composites Research
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    • 제16권4호
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    • pp.44-50
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    • 2003
  • 균열선단에 발생하는 손상역은 재료의 파괴인성 메카니즘을 알 수 있게 하는 중요한 영역이다. 본 연구에서는 고무변성 에폭시 수지의 균열선단 손상역의 생성 및 성장 과정을 음향방출법을 이용하여 조사하였다. 고무변성 에폭시 수지의 고무함량은 5 wt%와 15 wt%로 하였고, 3점 굽힘시험편을 사용하여 모드 I 파괴시험에 대한 각 시험편의 파괴인성값을 구하였다. 또한, 균열선단의 손상역과 그 내부의 고무입자 변형상태를 편광현미경과 원자력간 현미경을 사용하여 관찰하였다. 고무변성 에폭시 수지의 균열선단부의 손상역은 파괴하중의 약 13 % 하중에서 생성이 되어, 약 57 % 하중까지 균열개시 없이 성장하였다. 57 % 하중 근처에서 개시만 균열은 최대하중부근까지 고착-활강거동을 반복하면서 안정 / 불안정 파괴로 진전하였다 이 과정에서 발생한 음향방출신호의 시간-주파수 분석결과, 고투입자 내부에서의 케비테이션 생성단계에서 주파수대역은 0.15 ∼ 0.20 MHz 이었고, 그 후의 안정 및 불안정시의 주파수 대역은 0.20∼0.30MHz 이었다.

도시가스용 D3507 및 D3631 강관의 파괴특성 (Fracture Characteristics of D 3507 and D 3631 City Gas Steel Pipes)

  • 박재학;김한국;신규인;김만원
    • 한국안전학회지
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    • 제16권4호
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    • pp.39-46
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    • 2001
  • It is noted that KS D 3507 pipe steel has several problems when it is used as a city gas pipe at medium pressure. So new pipe steel, KS D 3631, was developed in order to be used as a pipe for medium and low pressure and now it is being substituted for D 3507. In this study, several mechanical tests, such as tensile test, microhardness test, and Charpy impact test were conducted to get material properties of D 3507 and D 3631 pipe steels. And also microstructures at the weld and heat affected zones were observed for the two materials. From the Charpy test results $K_{IC}/$ was estimated for the upper and lower shelf and the critical crack length is calculated for supposed axial semi-elliptical surface cracks. And the burst pressure is estimated as a function of wear depth for a defective D 3631 pipe by using the finite element method. The burst pressure is also calculated for pipes with an axial crack by using the published equations.

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연선균열성장 저항곡선에 대한 2매개변수의 특성 (Two-Parameter Characterization for the Resistance Curves of Ductile Crack Growth)

  • X.K.Zhu
    • Journal of Advanced Marine Engineering and Technology
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    • 제23권4호
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    • pp.488-503
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    • 1999
  • The present paper considers the constraint effect on J-R curves under the two-parameter $J-A_2$ controlled crack growth within a certain amount of crack extension. Since the parameter $A_2$ in $J-A_2$ three-term solution is independent of applied loading under fully plasticity or large-scale defor-mation $A_2$ is a proper constraint parameter uring crack extension. Both J and $A_2$ are used to char-acterize the resistance curves of ductile crack growth using J as the loading level and $A_2$ are used to char-acterize the resistance curves of ductile crack growth using J as the loading level and A2 as a con-straint parameter. Approach of the constraint-corrected J-R curve is proposed and a procedure of transferring the J-R curves determined from standard ASTM procedure to non-standard speci-mens or real cracked structures is outlined. The test data(e.g. initiation toughness JIC and tearing modulus $T_R$) of Joyce and Link(Engineer-ing Fracture Mechanics 1997, 57(4) : 431-446) for single-edge notched bend[SENB] specimen with from shallow to deep cracks is employed to demonstrate the efficiency of the present approach. The variation of $J_{IC}$ and $T_R$ with the constraint parameter $A_2$ is obtained and a con-straint-corrected J-R curves is constructed for the test material of HY80 steel. Comparisons show that the predicted J-R curves can very well match with the experimental data for both deep and shallow cracked specimens over a reasonably large amount of crack extension. Finally the present constraint-corrected J-R curve is used to predict the crack growth resistance curves for different fracture specimens. over a reasonably large amount of crack extension. Finally the present constraint-corrected J-R curve is used to predict the crack growth resistance curves for different fracture specimens. The constraint effects of specimen types and specimen sizes on the J-R curves can be easily obtained from the constrain-corrected J-R curves.

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탄소섬유 복합재료의 모드1 및 모드 2 층간파괴인성치에 관한 연구 (A Study on Mode 1 and Mode 2 Interlaminar Fracture Toughness of Carbon Fiber Reinforced Plastics)

  • 김재동;고성위
    • 수산해양기술연구
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    • 제31권3호
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    • pp.272-278
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    • 1995
  • 강도가 각각 다른 세 종류의 프리프레그를 사용하여 일방향 CFRP를 적층하였으며, 모드 I과 모드 II 실험을 통하여 층간 파괴인성치를 고찰하였고, 또한 적층 섬유방향을 변화시킨 사교적층판의 그것도 함께 고찰하였으며, 이를 요약하면 다음과 같다. 1) 임계에너지 방출률 G 하(IC)의 값을 컴플라이언스 법, 수정 컴플라이언스 법, 그리고 보이론에 의해 계산하여 비교 검토한 결과 본 연구에서 사용한 수정식에 의한 값들이 거의 일치하였다. 2) G 하(IC) 값은 대체로 프리프레그의 C, B, A재의 순으로 높게 나타났으며, G 하(II C)의 값을 세가지 식에 의해 계산하여 비교 검토한 결과 거의 일치하였다. 3) 사교적층판의 경우 G 하(IC) 값은 [0/90] 하(6s), [0/45] 하(6s), [0/45/90] 하(6s)의 순으로 높게 나타났으며, G 하(II C)는 [0/90] 하(6s), [0/45/90] 하(6s), [0/45] 하(6s)의 순으로 높게 나타났다. 4) 사교적층판과 일방향의 임계에너지 방출률을 비교하였을 때, 모드 I의 경우 일방향의 결과가 다소 높았으며, 모드 II의 경우는 [0/45] 하(6s)의 결과는 거의 일치함을 알 수 있었다.

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에폭시/PMR-15 폴리이미드 블렌드계의 경화동력학 및 열안정성에 관한 연구 (Studies on Cure Behavior and Thermal Stability of Epoxy/PMR-15 Polyimide Blend System)

  • Lee, Jae-Rock;Lee, Hwa-Young;Park, Soo-Jin
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2002년도 추계학술발표대회 논문집
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    • pp.265-268
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    • 2002
  • In this work, the blend system of epoxy and PMR-15 polyimide is investigated in terms of the cure behaviors and thermal stabilities. The cure behaviors are studied in DSC measurements and thermal stabilities are also carried out by TGA analysis. DDM (4, 4'-diamino diphenyl methane) is used as curing agent for EP and the content of PMR-15 is varied within 0, 5, 10, 35, and 20 phr to neat EP. As a result, the cure activation energy ($E_a$) is increased at 10 phr of PMR-15, compared with that of neat EP. From the TGA results of EP/PMR-15 blend system, the thermal stabilities based in the initial decomposed temperature (IDT) and integral procedural decomposition temperature (IPDT) are increased with increasing the PMR-15 content. The fracture toughness, measured in the context of critical stress intensity factor ($K_{IC}$) and critical strain energy release rate ($G_{IC}$), shows a similar behavior with $E_a$. This result is probably due to the crosslinking developed by the interactions between intermolecules in the polymer chains.

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Epoxidized soybean oil(ESO)의 합성 및 4 관능성 에폭시 수지/ESO 블렌드 시스템의 물성 (Synthesis of Epoxidized Soybean Oil (ESO) and its Blends with Tetrafunctional Epoxy Resins)

  • Lee, Jae-Rock;Jin, Fan-Long;Park, Soo-Jin
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2003년도 춘계학술발표대회 논문집
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    • pp.180-183
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    • 2003
  • In this work. a potential inexpensive epoxy resin. epoxidized soybean oil (ESO) was synthesized and applied as a toughening agent for 4.4'-tetradiglycidyl diaminodiphenyl methane (TGDDM). The chemical structure of ESO was characterized by FT-IR, $^1H NMR, and ^{13}C NMR$ spectroscopy. The curing behaviors. thermal stabilities. fracture toughness. and flexural strength of TGDDM/ESO blend systems were investigated by using the dynamic DSC. thermogravimetric analysis (TGA). and flexural tests. The thermal stabilities of TGDDM/ESO blend systems were decreased with increasing ESO contents. whereas the critical stress intensity factor ($K_{IC}$) and flexural strength ($\sigma_f$) were increased with ESO contents up to 10 wt% ESO.

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전기방사한 폴리에틸렌옥사이드 나노섬유/에폭시 복합재료의 기계적 계면특성 (Mechanical Interfacial Properties of Electrospun-based Poly(ethyleneoxide) Nanofibers/Epoxy Composites)

  • 정효진;이재락;박수진
    • Composites Research
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    • 제18권3호
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    • pp.31-37
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    • 2005
  • 본 연구에서는 나노섬유로 강인화된 복합재료를 만들기 위해 전기방사방법을 이용해서 폴리에틸렌옥사이드 (PEO) 나노섬유를 제조하였고, 제조된 복합재료와의 기계적 계면특성을 비교하기 위해 PEO 입자로 강인화된 복합재료를 제조하였다. PEO 나노섬유의 파이버 직경과 모폴로지는 주사전자현미경을 통해 관찰하였고, 복합재료의 기계적 계면특성은 파괴인성 $(K_{IC})$과 층간 전단 강도실험 (ILSS)을 통하여 알아보았다. 실험결과, 인가전압이 증가될수록 파이버의 직경은 감소하였고. 고전압에서 제트 불안정성의 증가로 인해서 최적의 섬유구조는 15 kV에서 얻을 수 있었다. PEO 나노섬유로 강인화된 에폭시 복합재료는 파괴인성인자 값인 $K_{IC}$와 ILSS가 PEO 입자로 강인화된 복합재료보다 향상된 값을 나타내었다. 이는 나노섬유가 입자에 비해 높은 비표면적과 aspect ratio를 가짐에 따라 복합재료의 기계적 계면특성을 향상시키는데 중요한 역할을 하는 것으로 판단된다.

다이아몬드 마이크로블레이드의 내구성과 절삭성능에 미치는 흑연과 MoS2의 첨가효과 (The Effect of Graphite and MoS2 on Endurance and Cutting Performance of Diamond Micro Blades)

  • 문종철;김송희
    • 한국표면공학회지
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    • 제41권6호
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    • pp.335-340
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    • 2008
  • Cutting performance and wear behavior were studied with the diamond micro-blade of Cu/Sn bond materials containing various amount of lubricant materials such as graphite and $MoS_2$. Measurement of instantaneous electric power consumption for cutting glass workpiece at the constant velocity was conducted and proposed as a method to assess cutting efficiency. The energy consumption of micro-blade for glass cutting decreased with the content of graphite and $MoS_2$ while wear amount of blade in volume increased with the amount of lubricant addition during the dicing test. It is because that hardness, flexural strength, and fracture toughness ($K_{IC}$) reduced with the amount of lubricant addition. Blades with $MoS_2$ additive showed higher mechanical properties than those with graphite additives when the same amount of the lubricant additive in wt.% was added. Due to the lower density of graphite than $MoS_2$, higher volume fraction of graphite could result in stronger effect on lowering electric power consumption by reducing the friction between blade and work piece however increasing wear rate due to the reduction in strength and fracture toughness. Adhesive wearing mode of micro blade could be remarkably improved by the addition of graphite as well as $MoS_2$.