• Title/Summary/Keyword: fracture surfaces

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Preparation and Properties of Glass Fiber-Reinforced Poly(olefin ketone) Composites (유리섬유 강화 폴리올레핀케톤 복합재료의 제조 및 특성에 대한 연구)

  • Cho, Hae-Souk;Chung, Jae-Seung;Baek, Seung-Jo;Choi, Won Jae;Kim, Jin-joo;Yoon, Sung Kyun;Lee, Jong-Chan
    • Applied Chemistry for Engineering
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    • v.23 no.3
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    • pp.339-343
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    • 2012
  • Poly(olefin ketone) terpolymer having excellent mechanical properties was synthesized and composite materials of poly(olefin ketone) containing polyurethane/amino silane functionalized glass fibers were prepared. The compatibilities between the functionalized glass fiber and the polymer were characterized by observing the fracture surfaces of the composites using scanning electron microscopy (SEM). Mechanical properties of composites with different contents, diameters, lengths, and binders of glass fibers were also studied using universal testing machine (UTM). The introduction of suitably functionalized glass fiber into the poly(olefin ketone) produces composite materials having excellent mechanical properties and they are very promising alternative materials for the engineering plastic applications.

Effects of Reinforced Pseudo-Plastic Backfill on the Behavior of Ground around Cavity Developed due to Sewer Leakage (하수관 누수에 의해 발생되는 공동 주변 지반의 거동에 대한 가소성유동화토의 보강효과)

  • Oh, Dongwook;Kong, Sukmin;Lee, Daeyoung;Yoo, Yongseon;Lee, Yongjoo
    • Journal of the Korean GEO-environmental Society
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    • v.16 no.12
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    • pp.13-22
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    • 2015
  • Developed ground cavity due to leakage of decrepit old sewer pipe causes ground surface settlement and brittle fracture of pavement. Recently, for 5 years, frequency of occurrence of ground subsidence phenomenon tends to increase rapidly and/or steadily. It is difficult to investigate ground surface settlement and/or subsidence in urban area because most ground surfaces are covered with asphalt or concrete pavement. In this research, therefore, ground surface settlement, influence zone and settlement of sewer pipe were analyzed using finite element method. Not only reinforced effect of pseudo-plastic backfill that is applied to prevent ground surface settlement or subsidence spot, was compared and analyzed using numerical analysis program, but also direct shear test was carried out to determine strength parameters of pseudo-plastic backfill.

Maxillary cement retained implant supported fixed prosthesis using the millingable Pd-Ag alloy generated by CAD/CAM system: clinical report after two years in service (상악 전부 무치악 환자에서 CAD/CAM 시스템으로 제작되는 Pd-Ag 합금을 이용한 고정성 임플란트 전악 수복 증례)

  • Lee, Jun-Sik;Han, Se-Jin;Choi, Yu-Sung
    • Journal of Dental Rehabilitation and Applied Science
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    • v.30 no.1
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    • pp.71-80
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    • 2014
  • Full-mouth reconstruction of a patient using dental implants is a challenge if there is vertical and horizontal bone resorption. Therefore, it is should be cautious in making the fixed prostheses that restore the function and the esthetics of the gingiva and teeth. In full mouth rehabilitation, CAD/CAM system makes it possible to fabricate restorations with high precision, regardless of span of the restoration. Recently, Palladium-silver (Pd-Ag) alloy which is highly biocompatible and millingable has been developed to compensate for the shortcomings of the titanium or zirconia. This clinical report presents the reconstruction of a maxillary arch with a cement retained implant supported fixed prosthesis using a Pd-Ag alloy generated by CAD/CAM system on eleven osseointegrated implants. The occluding surfaces were made of Pd-Ag alloy, to decrease the risk of chipping or fracture. The prostheses were esthetically pleasing, and no clinical complications have been reported after two years.

Effect of Porosity on the High-Cycle Fatigue Behavior of Al-Si-Mg Casting Alloy (Al-Si-Mg계 주조용 알루미늄 합금의 고주기 피로 거동에 미치는 기공의 영향)

  • Lee, Young-Jae;Kang, Won-Guk;Euh, Kwang-Jun;Cho, Kyu-Sang;Lee, Kee-Ahn
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.350-352
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    • 2009
  • The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore fur its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

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Study on Solid-liquid Mixture Flow in Inclined Annulus (경사 환형관내 고-액 혼합 유동특성에 관한 연구)

  • Kim, Young-Ju;Kim, Young-Hun;Woo, Nam-Sub
    • Journal of Ocean Engineering and Technology
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    • v.25 no.5
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    • pp.15-20
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    • 2011
  • This study carried out a series of experiments involving impact tests (Drop Weight type & Charpy type with a standard specimen and newly designed I-type specimen), hardness tests, and fracture surface observations of French-made roll shell steel (F), abnormal roll shell steel (M), reheated roll shell steel (R), and S25C steel under heat treatment conditiAn experimental study was carried out to study the solid-liquid mixture upward hydraulic transport of solid particles in vertical and inclined annuli with a rotating inner cylinder. The lift forces acting on a fluidized particle play a central role in many important applications such as the removal of drill cuttings in horizontal drill holes, sand transport in fractured reservoirs, sediment transport, the cleaning of particles from surfaces, etc. In this study a clear acrylic pipe was used to observe the movement of solid particles. Annular velocities varied from 0.4 to 1.2 m/s. The effect of the annulus inclination and drill pipe rotation on the carrying capacity of a drilling fluid, particle rising velocity, and pressure drop in a slim hole annulus were measured for fully-developed flows of water and aqueous solutions of CMC (sodium carboxymethyl cellulose) and bentonite. The rotation of the inner cylinder was efficient at carrying particles to some degree. For a higher particle volume concentration, the hydraulic pressure loss of the mixture flow increased because of the friction between the wall and solids or between solids.

Effects of Rotational Velocity on Weld Character of Inertia-Welded IN713C-SAE8630 (관성용접(慣性熔接)된 이종재질(異種材質) IN713C-SAE8630의 용접성능(熔接性能)에 회전속도(回轉速度)가 미치는 영향(影響))

  • Sae-Kyoo,Oh
    • Bulletin of the Society of Naval Architects of Korea
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    • v.9 no.2
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    • pp.43-48
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    • 1972
  • Inertia friction welding, a relatively recent innovation in the art of joining materials, is a forge-welding process that releases kinetic energy stored in the flywheel as frictional heat when two parts are rubbed together under the right conditions. In a comparatively short time, the process has become a reliable method for joining ferrous, and dissimilar metals. The process is based on thrusting one part, attached to a flywheel and rotating at a relatively high speed, against a stationary part. The contacting surfaces, heated to plastic temperatures, are forged together to produce a reliable, high-strength weld. Welds are made with little or no workpiece preparation and without filler metal or fluxes. However, In order to obtain a good weld, the determination of the optimum weld parameters is an important problem. Especially, because the amount of the flywheel mass will be determined according to the initial rotating velocity values at the constant thrust load, the initial rotating velocity is an important factor to affect a weld character of the inertia-welded IN713C-SAE8630, which is used for the wheel-shafts of turbine rotors or turbochargers, exhausting valves, etc. In this paper, the effects of initial rotational velocity on a weld character of inertia-welded IN713C-SAE8630 was studied through considerations of weld parameters determination, micro-structural observations and tensile tests. The results are as the following: 1) As initial rotating velocity was reduced to 267 FPM, cracks and carbide stringers were completely eliminated in the micro-structure of welded zone. 2) As initial rotating velocity was reduced and flywheel mass was increased correspondingly, the maximum welding temperatures were decreased and the plastic working in the weld zone was increased. 3) As initial rotating velocity was progressively decreased and carbides were decreased, the tensile strengths were increased. 4) And also the fracture location moved out of the weld zone and the tensile tests produced, the failures only in the cast superalloy IN713C which do not extend into the weld area. 5) The proper initial rotating velocity could be determined as about 250 thru 350 FPM for the better weld character.

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Thermal and Mechanical Properties of Short Fiber-Reinforced Epoxy Composites (단섬유 강화 에폭시 복합재료의 열적/기계적 특성)

  • Huang, Guang-Chun;Lee, Chung-Hee;Lee, Jong-Keun
    • Polymer(Korea)
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    • v.33 no.6
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    • pp.530-536
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    • 2009
  • A cycloaliphatic epoxy/acidic anhydride system incorporating short carbon fibers (SCF) and short glass fibers (SGF) was fabricated and thermal/mechanical properties were characterized. At low filler content both SCF- and SGF-reinforced composites showed a similar decrease in coefficient of thermal expansion (CTE), measured by a thermomechanical analyzer, with increasing loadings, above which SCF became more effective than SGF at reducing the CTE. Experimental CTE data for the SCF-reinforced composites is best described by the rule of mixtures at lower SCF contents and by the Craft-Christensen model at higher SCF contents. Storage modulus (E') at $30^{\circ}C$ and $180^{\circ}C$ was greatly enhanced for short fiber-filled composites compared to unfilled specimens, Scanning electron microscopy of the fracture surfaces indicated that the decreased CTE and the increased E' of the short fiber-reinforced composites resulted from good interfacial adhesion between the fibers and epoxy matrix.

Fabrication and Mechanical Properties of $MoSi_2$ Based Composites ($MoSi_2$ 복합재료의 제조 및 기계적 특성)

  • Park, Yi-Hyun;Lee, Sang-Pill;Lee, Sung-Eun;Jin, Joon-Ok;Kim, Sa-Woong;Lee, Jin-Kyung;Yoon, Han-Ki
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2003.05a
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    • pp.289-293
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    • 2003
  • This study dealt with the characterization of $MoSi_2$ based composites containing three types of additive materials such as SiC, $NbSi_2\;and\;ZrO_2$ particles have been investigated, based on the detailed examination of their microstructures and fracture surfaces. The effects of reinforcing materials on the high temperature strength of $MoSi_2$ based composites have been also examined. $MoSi_2$ based composites were fabricated by the hot press process under the vacuum atmosphere. The volume fraction of reinforcing materials in the composite system was fixed as 20 %. The microstructures and the mechanical properties of $MoSi_2$ based composites were investigated by means of SEM, EDS, XRD and three point bending test.

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Marco and Microscopic Observations of Fatigue Crack Growth Behavior in API 2W Gr. 50 Steel Joints (API 2W Gr. 50 강재 용접부의 피로균열전파거동의 거시적 및 미시적 관찰)

  • Sohn, Hye-Jeong;Kim, Seon-Jin
    • Journal of Ocean Engineering and Technology
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    • v.26 no.5
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    • pp.73-80
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    • 2012
  • It is well known that a considerable amount of scatter is shown in experimental results relating to fatigue crack growth even under identical and constant amplitude cyclic loading conditions. Moreover, flux cored arc welding (FCAW) is a common method used to join thick plates such as the structural members of large scale offshore structures and very large container ships. The objective of this study was to investigate the macro- and microscopic observations of the fatigue crack growth (FCG) behavior of the FCAWed API 2W Gr. 50 steel joints typically applied for offshore structures. In order to clearly understand the randomness of the fatigue crack growth behavior in the materials of three different zones, the weld metal (WM), heat affected zone (HAZ), and base metal (BM), experimental fatigue crack growth tests for each of five specimens were performed on ASTM standard compact tension (CT) specimens under constant amplitude cyclic loading. Special focus was placed on the fatigued fracture surfaces. As a result, a different behavior was observed at the macro-level, depending on the type of material property: BM, HAZ, or WM. The variability in the fatigue crack growth rate for WM was higher than that of BM and HAZ.

INFLUENCES OF SILANE CONCENTRATION FOR FILLER SILANIZATION ON THE PROPERTIES OF COMPOSITES (필러의 실란처리농도가 복합레진의 특성에 미치는 영향)

  • 조태희;박상진
    • Restorative Dentistry and Endodontics
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    • v.26 no.1
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    • pp.23-31
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    • 2001
  • The purpose of this study was to search the optimal silane concentrations for filler- silanization of seven experimental composites. Silica filer was a 25micron crushed type. 0.0%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5%, and 3.0% silane($\gamma$-methacrylooxypropyltrimethoxysilane)were added into silica-filler with weight percentage (wt%). Mixtures(silica filler/silane)were reacted at 6$0^{\circ}C$ for 72hours, and crushed into fine particles those were used as fillers for 7 experimental composites. Monomer was a 3 : 1 mixture of Bis-GMA and TEGDMA containing 0.2% tertiary amine and 0.4% camphoroquinone for light curability. A ratio for mixing the monomer and filler was 75% and 25% respectively. Seven experimental composites was classified with the concentration of silane treated, and the specimen number for each test was 10. Specimens with 6mm diameter and 3mm height dimension for measuring the diametral tensile strength were destroyed with 1mm/min cross-head speed on Instron universal testing machine (No. 4467, USA). Shear bond strength was measured on the specimens bonded to bovine enamel etched with 37% phosphoric acid solution for 1 minute Fractured surfaces were observed by SEM (Hitachi S-3200, Japan) among that of the highest values measured from each groups. Following results were obtained: 1. Experimental composites containing silanized filter showed the significantly higher diametral tensile strength and shear bond strength than the composites containing un-silanized fillers(Group1) (p<0.05). 2. In silanized filler composite resins(Group 2~7), Diametral tensile strength of Group 3 showed the significantly higher than that of Group 2 and Group 6(p<0.05). 3. Shear bond strength was higher in Group 3 than that of Group 7 (p<0.05)in silanized fillers composite resins. 4. Fracture surface was formed in resin matrixes on the specimens from composites containing the fillers treated with 0.5% 1.0%, and 1.5% silane. These results mean that the optimal silane concentrations are exist for each fillet with its size and surface area, and that 1.0% is a optimal value for concentration to coat the 25$\mu\textrm{m}$ filler with silane.

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