• Title/Summary/Keyword: fractographic analysis

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Property differences between GTAW and SMAW duplex stainless steel weld metal (이상계 스테인레스 강 용접부의 인성과 내식성 거동)

  • 백광기;김희진;안상곤
    • Journal of Welding and Joining
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    • v.4 no.3
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    • pp.58-71
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    • 1986
  • Mechanical and corrosion property of duplex stainless steel weldments made by the GTAW and SMAW process were studied. Fracture toughness, general and local corrosion resistance of GTAW and SMAW weldments were evaluated in terms of Charpy V notch impact test, anodic polarization diagram, pitting corrosion rate, respectively. SMA weld metal showed much lower impact toughness and higher ductile-brittle transition temperature than GTA weld metal. Fractographic and EDX analysis on fracture surface of SMA weld metal demonstrated the existence of (Si, Ti), oxide in large amounts. Potentiodynamic anodic polarization diagram of GMA weld metal showed much lower passive current density than SMA weld metal in 4% $H_2/SO_4$ solution. And pitting corrosion rate test showed the same tendency. Relating the microstructure, chemistry and property, it can be concluded that GTA weld metal gives better toughness due to lower oxygen content, i.e. lower inclusion content, and better corrosion resistance due to higher Pitting Index(PI) than SMA weld metal.

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Stable and Unstable Crack Growth in Chromium Pre-alloyed Steel

  • Gerosa, Riccardo;Rivolta, Barbara;Tavasci, Adriano;Silva, Giuseppe;Bergmark, Anders
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.138-139
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    • 2006
  • Sintered steels are materials characterized by residual porosity, whose dimension and morphology strongly affect the fatigue crack growth behaviour of the material. Prismatic specimens were pressed at $7.0\;g/cm^3$ from Astaloy CrM powder and sintered varying the sintering temperature and the cooling rate. Optical observations allowed to evaluate the dimensions and the morphology of the porosity and the microstructural characteristics. Fatigue tests were performed to investigate the threshold zone and to calculate the Paris law. Moreover $K_{Ic}$ tests were performed to complete the investigation. Both on fatigue and $K_{Ic}$ samples a fractographic analysis was carried out to investigate the crack path and the fracture surface features. The results show that the Paris law crack growth exponent is around 6.0 for $1120^{\circ}C$ sintered and around 4.7 for $1250^{\circ}C$ sintered materials. The same dependence to process parameters is not found for $K_{Ith}$.

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The necessary number of profile lines for the analysis of concrete fracture surfaces

  • Konkol, Janusz;Prokopski, Grzegorz
    • Structural Engineering and Mechanics
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    • v.25 no.5
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    • pp.565-576
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    • 2007
  • The article describes a technique for the measurement of the level of complexity of fracture surfaces by the method of vertical sections, and a performed statistical analysis of the effect of profile lines on the fractographic and fractal parameters of fractures, i.e. the profile line development factor, $R_L$, and the fracture surface development factor, $R_S$, (as defined by the cycloid method), as well as the fractal dimension, $D_C$, (as determined by the chord method), and the fractal dimension, $D_{BC}$, (as determined by the box method). The above-mentioned parameters were determined for fracture surfaces of basalt and gravel concretes, respectively, which had previously been subjected to fracture toughness tests. The concretes were made from mixtures of a water/cement ratio ranging from 0.41 to 0.61 and with a variable fraction of coarse aggregate to fine aggregate, $C_{agg.}/F_{agg.}$, in the range from 1.5 to 3.5. Basalt and gravel aggregate of a fraction to maximum 16 mm were used to the tests. Based on the performed analysis it has been established that the necessary number of concrete fracture profile lines, which assures the reliability of obtained testing results, should amount to 12.

A Study on Fatigue Strength in the Friction Welded Joints of HSS-Co to SM55C Carbon Steel(II) (HSS-Co와 SM55C 이종 마찰용접재의 피로강도에 관한 연구(2))

  • 서창민;서덕영;이동재
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.19 no.4
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    • pp.929-940
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    • 1995
  • The fatigue strength and fracture topography in the friction welded interface of high speed steel (HSS-Co) to SM55C carbon steel have been investigated through the fatigue test, SEM fractograph and EDS (energy dispersive spectrometer) analysis. Three kinds of specimens used in this research are the friction welded joints, HSS-Co and SM55C carbon steel with circumferential notch, saw notch and smooth, respectively. The notch sensitivity factor, .eta. of the friction welded joints is lower than that of the base materials, and that represents a superiority of the joint performance of FRW. Fracture topography of the FRW specimens with a notch showed a cleavage or brittle appearance, while that of the FRW smooth specimen appeared to be ductile. Furthermore, although fatigue crack likely initiated near the weld interface of the FRW smooth specimen, crack propagation continued into the HAZ of SM55C steel. Finally, fatigue fractures of the base materials were associated primarily with the inclusions located at the outer periphery of the specimen.

An Experimental Study on the Inner Crack Growth of Welded Connections of Steel Structures (강구조용접연결부(鋼構造鎔接連結部)의 내부구열성장(內部龜裂成長)에 관한 실험적(實驗的) 연구(硏究))

  • Min, Chang Dong;Kim, Ki Du;Chang, Dong Il
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.5 no.2
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    • pp.121-131
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    • 1985
  • The characteristic of fatigue crack growth in the homogeneous or the soft welded connections used SWS-53 steel and HT-80 steel as base metals is examined by fractographic analysis. As a result of this analysis, the fact that the characteristic of fatigue crack growth which is observed and measured at the surface has wide application to engineering practice is verified. Also, the fact that the welded parts of HT-80 steel have much danger of brittle fracture is prooved. Considering that the striations are observed at the welded parts of SWS-58 steel and the spacing of striations has higher numerical value than da/dN, we can prove that inner fatigue crack growth may develop in zig-zag directions.

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Investigation and Analysis of Cracks in Multi-layer Ceramic Capacitor (다층세라믹 콘덴서에서 생성된 크랙의 관찰과 분석)

  • Lee, Chul-Seung;Kang, Byung-Sung;Hur, Kang-Heon;Park, Jin-Woo
    • Journal of the Korean Ceramic Society
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    • v.46 no.2
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    • pp.211-218
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    • 2009
  • For the Y5V characteristic MLCC which is very prone to crack, it is important to to find out the basic cause of the crack. After finding out the crack origin, the materials and processes should be developed to remove the crack. The microstructures of the cracks were investigated using the fractographic method for the various types of cracks such as an exterior crack, a cyclic thermal shock crack, and an piezo-electric crack. It was found out that the crack origin was the pore at the end of the Ni inner electrode after bake-out. Even though the three dimensional crack shapes were different, the crack origins were seemed to be similar. The exterior crack could grow from the origin with the aids of residual and applied stress. FEM (finite element method) analysis was used to calculate the stress distribution of residual and applied stress. And the concept of fracture mechanics was applied for the explanation of the crack initiation and propagation from the stresses concentration.

Interfacial Shear Strength and Thermal Properties of Electron Beam-Treated Henequen Fibers Reinforced Unsaturated Polyester Composites

  • Pang Yansong;Cho Donghwan;Han Seong Ok;Park Won Ho
    • Macromolecular Research
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    • v.13 no.5
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    • pp.453-459
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    • 2005
  • Natural fiber henequen/unsaturated polyester (UPE) composites were fabricated by means of a compression molding technique using chopped henequen fibers treated at various electron beam (EB) dosages. The interfacial shear strength (IFSS), dynamic mechanical properties, and thermal expansion behavior were investigated through a single fiber microbonding test, fractographic observation, dynamic mechanical analysis, and thermomechanical analysis, respectively. The results indicated that the interfacial and dynamic mechanical properties significantly depended on the level of the EB treatment irradiated onto the henequen fiber surfaces. The effect of EB treatment on the IFSS, storage modulus and fracture surface of the henequen/UPE composites agreed with each other. The results of this study also suggested that the modification of henequen fiber surfaces at 10 kGy EB is the most effective for improving the interfacial properties of the henequen/UPE composites.

Statistical Analysis for Creep Crack Growth Behavior of Modified 9Cr-1Mo Steel (Modified 9Cr-1Mo 강의 크리프 균열성장 거동에 관한 통계적 해석)

  • Jung, Ik-Hee;Kim, Woo-Gon;Yin, Song-Nan;Ryu, Woo-Seog;Kim, Seon-Jin
    • Korean Journal of Metals and Materials
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    • v.47 no.5
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    • pp.283-289
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    • 2009
  • This paper dealt with a statistical analysis for evaluating the creep crack growth rate (CCGR) for Modified 9Cr-1Mo (ASTM Grade 91) steel. The CCGR data was obtained by the creep crack growth (CCG) tests conducted under various applied loads at $600^{\circ}C$. To obtain logically the B and q values used in the CCGR equation, three methods such as the least square fitting method (LSFM), the mean value method (MVM) and the probabilistic distribution method (PDM) were adopted and their CCGR lines were compared, respectively. In addition, a number of random variables were generated by using the Monte Carlo simulation (MCS), and the CCGR lines were predicted probabilistically. It was found that both the B and q coefficients followed a 2-parameter Weibull distribution well. In the case of the ranges of 10-90% for the probability variables, P(B, q), the CCGR lines were predicted. Fractographic study was conducted from the specimen after the CCG tests.

Fracture Behavior of Pressure Tube Materials Based on Fractography (금속재료의 재료시험법 교과내용 개선을 위한 Fractography 신개념 소개 및 도입에 대한 연구)

  • Oh, Dong-Joon
    • The Journal of Korean Institute for Practical Engineering Education
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    • v.2 no.1
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    • pp.126-134
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    • 2010
  • Material Testing Method subject of Metal Materials, which is one of curriculum of engineering major high school, is not properly updated even though both science and technology are advancing rapidly. Especially, the need of fractographic technique, which can analyze the fracture surface with the advanced testing equipment and technique, is increasing. The importance and the analyzing method of Fractography are proved by the characteristic analysis of pressure tube fracture surface of HWPR. In the future, in order to increase the professional knowledge and their pride of engineering major high school student, these advanced subject should be included in the new crriculum of engineering major high school. This activity to involve the advanced subject should be carried out voluntary by the first line teacher before the responsible body.

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Effect of Rubber Particle Size and Polymer Properties on Impact Strength and Fracture Behavior of Rubber/Polymer Composites (고무입자의 크기와 폴리머의 물성이 고무/폴리머 복합재료의 충격강도 및 파괴거동에 미치는 영향)

  • 이창수;강병일;조길원;황운봉
    • Composites Research
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    • v.12 no.6
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    • pp.83-89
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    • 1999
  • The impact strength and fracture behavior of rubber/polymer composites were investigated with respect to two factors: (i) characteristic ratio, $C_{\infty}$ as a measure of chain flexibility of the polymer matrix and (ii) the rubber particle size in polymer blend system. In this study C was controlled by the composition ratio of polyphenylene oxide (PPO) and polystyene (PS). Izod impact test and fractographic observation of the fracture surface using scanning electron microscope were conducted. Finite element analysis were carried out to gain understanding of plastic deformation mechanism (shear yielding and crazing) of these materials. Shear yielding was found to be enhanced when the flexibility of matrix polymer was relatively low and the rubber particles were small.

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