• Title/Summary/Keyword: finer grain size

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Characteristics of Magnesium Alloy Fabricated by Melt Drag Method with Applying Overheating Treatments (과부하 열처리를 적용하여 용융드래그방법으로 제작한 마그네슘합금의 특성)

  • Han, Chang-Suk;Lee, Chan-Woo
    • Korean Journal of Materials Research
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    • v.32 no.10
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    • pp.414-418
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    • 2022
  • Magnesium alloy is the lightest practical metal. It has excellent specific strength and recyclability as well as abundant reserves, and is expected to be a next-generation structural metal material following aluminum alloy. This paper investigated the possibility of thin plate fabrication by applying a overheating treatment to the melt drag method, and investigating the surface shape of the thin plate, grain size, grain size distribution, and Vickers hardness. When the overheating treatment was applied to magnesium alloy, the grains were refined, so it is expected that further refinement of grains can be realized if the overheating treatment is applied to the melt drag method. By applying overheating treatment, it was possible to fabricate a thin plate of magnesium alloy using the melt drag method, and a microstructure with a minimum grain size of around 12 ㎛ was obtained. As the overheating treatment temperature increased, void defects increased on the roll surface of the thin plate, and holding time had no effect on the surface shape of the thin plate. The fabricated thin plate showed uniform grain size distribution. When the holding times were 0 and 30 min, the grain size was refined, and the effect of the holding time became smaller as the overheating treatment temperature increased. As the overheating temperature becomes higher, the grain size becomes finer, and the finer the grain size is, the higher the Vickers hardness.

The Effect of Carbide Size on the Mechanical Properties of AISI E 52100 Steel (AISI E 52100 강(鋼)의 기계적(機械的) 성질(性質)에 미치는 탄화물(炭化物) 크기의 영향(影響))

  • Cho, K.R.;Kim, B.W.;Nam, T.W.;Lee, B.K.
    • Journal of the Korean Society for Heat Treatment
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    • v.3 no.4
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    • pp.10-22
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    • 1990
  • A study has been investigated on the effect of mechanical properties (tension strength, rotary bending fatigue strength, wear resistance, hardness) according to the carbide particle size variation by the treatment of 1) quenching tempering, and 2) quenching, subzero treatment and tempering. The material used in this investigation was a typical bearing steel, high C high Cr, AISI E 52100. The result obtained in this study were as follows : (1) Finer the carbide particle size increasing the hardness and retained austenite in same quenching condition. (2) Finer the carbide particle size reduced the tension and rotary bending fatigue which were resulted from austenite grain growth and carbide precipitation on grain boundry that induced by carbide refine heat treatment. (3) Finer the carbide particel size increasing the wear resistance which were resulted by uniform distribution of carbide and increased hardness induced by microstructural uniform hardenability of matrix. (4) When the carbide particles were refinded, subzero treatment is effective only wear resistance and hardness.

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Effect of Welding Condition on Microstructure of Transient Zone in Overlay Weld of 3Cr-1Mo Steel/STS-309L (3Cr-1Mo강/STS-309L 오버레이 용접부의 천이영역 조직에 미치는 용접조건의 영향)

  • 김동진;김병훈;지병하;김정태;김성곤;강정윤;박화순
    • Journal of Welding and Joining
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    • v.18 no.2
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    • pp.176-176
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    • 2000
  • Recently developed Austenite stainless steel,309L was to overlay on 3Cr-1Mo-V-Ti-B steels, using Electroslag welding process, which wide electrodes were adopted. Transition region in welding interlayer relating to disbonding crack was investigated. Also. the effect of welding condition on the width of transition region and coarsening grains of the austenite were studied.1) With increasing welding speed the width of martensite at transient region was increased, but the amount of delta ferrite in weld metal was reduced, being fine grained.2) The form of martensite at the transition region was occured by reversible transition region, leading to increasing Ms point.3) With increasing welding speed, the grain of austenite formed at the welding interface was finer. With increasing welding current under the same welding speed, the grain size of the austenite was finer. At high current, original grain size of the austenite is coarse, but the austenite has fine grains because the austenite was transformed to martensite during cooling.4) In the case of high welding speed, the width of martensite at the welding interface was increased, but the grain size of austenite at the welding interface was finer. This indicates that the inhibition of disbonding crack may be achieved through dispersening fine carbides in the grain boudary.(Received August 3, 1999)

Interaction fields based on incompatibility tensor in field theory of plasticity-Part II: Application-

  • Hasebe, Tadashi
    • Interaction and multiscale mechanics
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    • v.2 no.1
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    • pp.15-30
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    • 2009
  • The theoretical framework of the interaction fields for multiple scales based on field theory is applied to one-dimensional problem mimicking dislocation substructure sensitive intra-granular inhomogeneity evolution under fatigue of Cu-added steels. Three distinct scale levels corresponding respectively to the orders of (A)dislocation substructures, (B)grain size and (C)grain aggregates are set-up based on FE-RKPM (reproducing kernel particle method) based interpolated strain distribution to obtain the incompatibility term in the interaction field. Comparisons between analytical conditions with and without the interaction, and that among different cell size in the scale A are simulated. The effect of interaction field on the B-scale field evolution is extensively examined. Finer and larger fluctuation is demonstrated to be obtained by taking account of the field interactions. Finer cell size exhibits larger field fluctuation whereas the coarse cell size yields negligible interaction effects.

Characteristics of Particles Size and Element Distribution in the Coastal Bottom Sediments in the Vicinity of Youngkwang Nuclear Power Plant (영광 원자력발전소 주변해역 표층퇴적물의 입도와 원소분포 특성)

  • 은고요나
    • Economic and Environmental Geology
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    • v.33 no.3
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    • pp.195-204
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    • 2000
  • order to investigate physical characteristics and element concentrations of sediments, coastal bottom sediments were collected at 20 stations in the vicinity of Youngkwang Nuclear Power Plant. After air drying of samples in the laboratory. article size distribution was examined by Master sizer (X-350F), radio-activity by HPGe ${\gamma}$-spectrphotometer, and element concentrations by ICP-AES and AAS. According to particle size analysis , sediments are mainly composed of silt fraction weith 23% of sand, 65% of silt and 12% of clay on average. Most sediments are derived from muddy environment that silt dominates with the characteristics of 5.3${\varsigma}$ mean particle size, poorly sorted, very fine skewed and lepto-kurtic. Only two sediments are well sorted with sandy silt owing to wind, winnowing action, tide and current andits complex reactions. Element concentrations in the coastal bottom sediments are relatively high at finer sediment and show significant relationship with grain size. Index of geoaccumulation by heavy metals at every sampling station is classified as practically unpolluted. The radioactivities of the sediments were measured for 15 isotope elements, and 2 elements of K-40 and Cs-137 were detected in most sediments. The K-40 is the natural nuclide and the artificial nuclide of Cs-137 was thought to be derived from the fallout of past nuclear weapon test. The results of correlation coefficient between grain size and radioactivity shows that the activity of Cs-137 significantly increases in finer grain.

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Effect of Welding Condition on Microstructure of Transient Zone in Overlay Weld of 3Cr-1Mo Steel/STS-309L (3Cr-1Mo강/STS-309L 오버레이 용접부의 천이영역 조직에 미치는 용접조건의 영향)

  • 김동진;김병훈;지병하;김정태;김성곤;강정윤;박화순
    • Journal of Welding and Joining
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    • v.18 no.2
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    • pp.49-56
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    • 2000
  • Recently developed Austenite stainless steel, 309L was used to overlay on 3Cr-1Mo-V-Ti-B steels, using Electroslag welding process, which wide electrodes were adopted. Transition region in welding interlayer relating to disbonding crack was investigated. Also, the effect of welding condition on the width of transition region and coarsening grains of the austenite were studied. 1) With increasing welding speed the width of martensite at transient region was increased, but the amount of delta ferrite in weld metal was reduced, being fine grained. 2) The form of martensite at the transition region was occurred by reversible transformation during cooling since the interdiffusion of Cr and Ni from weld metal and Fe and C from base metals at the transition region, causes to lowering the concentration of Cr and Ni at the transition region, leading to increasing Ms point. 3) With increasing welding speed, the grain of austenite formed at the welding interface was finer. With increasing welding current under the same welding speed, the grain size of the austenite was finer. At high current, original grain size of the austenite is coarse, but the austenite has fine grains because the austenite was transformed to martensite during cooling. 4) In the case of high welding speed, the width of martensite at the welding interface was increased, but the grain size of austenite at the welding interface was finer. This indicates that the inhibition of disbonding crack may be achieved through dispersening fine carbides in the gain boundary.

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Coercivity of Nd-Fe-B-type Fine Particles Prepared from Different Precursor Materials

  • Kim, K.M.;Kwon, H.W.;Lee, J.G.;Yu, J.H.
    • Journal of Magnetics
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    • v.20 no.1
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    • pp.21-25
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    • 2015
  • Fine Nd-Fe-B-type particles were prepared by ball milling of different types of Nd-Fe-B precursor materials, such as die-upset magnet, HDDR-treated material, and sintered magnets. Coercivity dependence on the grain and particle size of the powder was investigated. Coercivity of the milled particles was reduced as the particle size decreased, and the extent of coercivity loss was dependent upon the precursor material. Coercivity loss in the finely milled particles was attributed to the surface oxidation. The extent of coercivity loss in the fine particles was closely linked to grain size of the precursor materials. Coercivity loss was more profound for the fine particles with larger grain size. Contrary to the fine particles from the sintered magnets with larger grain size the fine particles (~10 um) from the die-upset magnet and HDDR-treated material with much finer grain size still retained high coercivity (> 10 kOe for die-upset magnet, > 4 kOe for HDDR-treated material).

Study on the Soil Compaction (흙의 다짐에 관한 연구(I))

  • 강문묵
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.11 no.4
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    • pp.1783-1790
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    • 1969
  • It is one of the most economical method of soil stabilization works to compact soil, which increases soil density artificially. Compaction effort is to lessen void of soils, and consequently its aim is to enlarge friction and cohesion force, and reduce permeability of soil. Factors in compaction effort are moisture content, grain size, grain size distribution, physical properties, compaction method and temperature of soils etc. The results obtained in this study on the effects that grain size, gradation and physical properties influence upon compaction effort for 20 samples under the constant compaction method, are summarized as follows: 1. The bigger the maximum dry density is, the smaller the optimum moisture content is, on the other hand, the smaller the maximum dry densityis, the bigger the optimum moisture content is, ingeneral. 2. The coarser the grain size is, the bigger the maximum dry density is, and the optimum moisture content becomes small, and dry density-moisture content curve has the sharp peak, generally. Also, the finer the grain size is the smaller the maximum dry density is, and the optimum moisture content shows the big value, and dry density-moisture content curve has the dull peak. 3. The maximum dry density shows the biggest value on the sample to be about 15% of particles finer than No. 200 sieve. The more the percent passing of No. 10 sieve increase, the smaller the maximum dry density is. Soils which have uniformity coefficient less than 5 in particles larger than 0.074mm hardly show dry density-moisture content curve. 4. There is a relation which is ramax=2.3948-0.0376 Wopt between the maximum dry density and the optimum moisture content, namely, the maximum dry density is increased in proportion to decrease of the optimum moisture content. 5. There are relations to be the straight lines which the maximum dry density decrease, on the other hand, the optimum moisture content increase in accordance with enlargement of Atterberg Limit(LL, PL, PL) in compacted soils.

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Fine Granulation of Recording Layer in Perpendicular Magnetic Recording Media Using Oxide-interlayer (산화막중간층에 의한 수직자기기록층의 입자크기 미세화)

  • 김경환;공석현
    • Journal of the Korean institute of surface engineering
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    • v.37 no.4
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    • pp.196-199
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    • 2004
  • Seedlayers with low surface energy which increases the density of nucleation sites in the initial growth region of the recording layer deposited on them was studied to reduce grain size in recording layer. The seedlayer with low surface energy was so effective to attain finer grain in magnetic upper-layers. The Ni-Fe-O intermediate layer with low surface energy was found to be effective in reduction of grain size as well as magnetic cluster size of Co-Cr-Ta-Pt recording layer. Furthermore, the reduction of grain size in Co-Cr-Ta-Pt recording layer on Ni-Fe-O intermediate layer with low surface energy led to decrease the noise level in the high recording density region.

Microstructure and Yield Asymmetry Behavior of Indirect-extruded Mg-Sn-Al-Zn Alloys (Mg-Sn-Al-Zn 마그네슘 합금 간접압출재의 미세조직 및 소성이방성)

  • Park, S.H.;Kim, Y.M.;Kim, H.S.;Yim, C.D.;You, B.S.
    • Transactions of Materials Processing
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    • v.21 no.5
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    • pp.324-329
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    • 2012
  • Mg-(9-x)Sn-xAl-1Zn (x=1, 2, 3 and 4 wt.%) alloys were subjected to indirect extrusion, and the microstructure and mechanical properties of the as-extruded Mg-Sn-Al-Zn (TAZ) alloys were investigated. The TAZ 811 alloy exhibited a finer grain structure than the TAZ 541 alloy due to a larger number of Mg2Sn particles, which pinned the grain boundaries and prevented growth of recrystallized grains. The TAZ alloys showed an unusual yield asymmetry behavior. The tension-compression yield asymmetry increased with decreasing average grain size. The TAZ 811 alloy with a small grain size exhibited a larger yield asymmetry than that of the TAZ 541 alloy having a relatively large grain size, which is mainly attributed to the low Al content and large number of second phase particles in the TAZ 811 alloy.