• Title/Summary/Keyword: fine grain size

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The Effect of the Retrogression and Reaging Treatments on the Mechanical Properties and Susceptibility to Stress Cracking of AA 7039 Al Alloy (RRA 처리가 AA 7039 Al 합금의 기계적 성질과 내응력 부식성에 미치는 영향)

  • Jun, Sang-Jo;Kim, Jun-Soo;Kim, Song-Hee
    • Journal of Industrial Technology
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    • v.7
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    • pp.49-58
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    • 1987
  • To investigate the effect of the Retrogression and Reaging (RRA) treatment on the strength and the stress corrosion cracking in AA 7039 the measurement of hardness, tensile properties and the time to failure in a constant rate method were measured. Transmission electron microscope was used to examine the microstructural changes within graln and grain boundary. The results show that the RRA treatment of the T6 condition results in a significant increase in the time to failure without sacrifying the original T6 strength. It is believed that high density and even distribution of precipitates in RRA condition were observed within grain so that the RRA condition could have similar strength to the T6 condition. The presence of fine dispersion of semicohernt ${\eta}^{\prime}$ transition phase is also believed to contribute to that effect. Examination of the grain boundary microstructure shows that the RRA treatments increases significantly the average size of the grain boundary preciptates. It is suggested that the benificial effect of the RRA treatment on the susceptibility to SCC be due to the increase in the size of grain boundary precipitates obtained during the retrogression treatment.

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An Analysis of Micro-landform and Its Grain Size of Tidal Flat in Gomso-Bay using Satellite Remote Sensing (위성원격탐사를 이용한 곰소만 간석지의 미지형과 퇴적물 입도특성 분석)

  • Jo, Wha-Rhong;Jo, Myung-Hee
    • Journal of the Korean Association of Geographic Information Studies
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    • v.3 no.1
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    • pp.44-56
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    • 2000
  • Through the ISODATA method of unsupervised classification, the micro-landform of Gomso-Bay tidal flat was classified into mud, mixed, and sand flats by using Landsat TM image. Each tidal flat shows on apparent differences in its topographical characteristics and grain size compositions. Mud flat is occupied the innermost part of the tidal flat. Sand flat is distributed adjacent to the entrance of the bay, while the mixed one is located in the central part of the bay. Mud flat deposits have fine grain size, more than 4 in average mean phi, bad sorting, more than 1 phi in standard devation, and positive skewness. Mixed and sand flat deposits have coarse grain size, less than 4 average mean phi, good sorting, less than 1 phi in standard daviation, and negative skewness. Topographically, the mud flat consists of flat surfaces and dissected channels. The average depth of dissected channels is about 2 meters. Meanwhile, sand flat has a very flat landform with well-developed ripple marks of less than 10 centimeters in average relief. And the mixed one shows the intermediate topographical characteristics of those of mud and sand flats.

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The Distribution Characteristics of Grain Size and Organic Matters of Surface Sediments from the Nakdong-Goryeong Mid-watershed (낙동·고령 중권역의 표층 퇴적물 입도 조성 및 유기물질 분포 특성 변화)

  • Kim, Shin;Ahn, Jungmin;Kim, Hyounggeun;Kwon, Heongak;Kim, Gyeonghoon;Shin, Dongseok;Yang, Deukseok
    • Journal of Environmental Science International
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    • v.27 no.6
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    • pp.411-423
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    • 2018
  • To investigate the distribution characteristics of grain size and organic matter of surface sediments from the Nakdong-Goryeong Mid-watershed, surface sediments were collected and analyzed. The samples were collected from six sited at four different times between May 2013 and May 2014. The were analyzed for grain size, water content, ignition loss, chemical oxygen demand, total organic carbon and total nitrogen. The surface sediments were mainly composed of medium sand (mean 44.7%) and coarse sand (mean 32.8%) and became coarser in May 2014. Fine sediments at the site NG-2 were poorly sorted and positively skewed, and occur in a tributary environment that is relatively low-energy compared with the other sites. The water content at the studied sites (15.3 ~ 34.9%) averaged 20.25%, and ignition loss (0.4 ~ 5.8%) and total nitrogen (274 ~ 2493 mg/kg) averaged 1.33% and, 696 mg/kg, respectively. These values indicated that the sediments were not seriously contaminated when compared with the sediment pollution evaluation standard of the National Institute of Environmental Research. The chemical oxygen demand (mean 0.17%) was at the non-polluted level compared with United States Environmental Protection Agency sediment quality standards. The total organic carbon (mean 0.18%) at all sites except site NG-2 (lowest effect level) was the no effect level of the Ontario sediment quality guidelines. The COD/IL (0.02 ~ 0.20) and C/N (0.73 ~ 6.76) were less than 1 and 10, respectively. Organic matter in the study area produced naturally from aquatic organisms. Results of principal component analysis showed that fine sediments (very fine sand and silt) were significantly affected by organic matters (ignition loss, chemical oxygen demand, total organic carbon and total nitrogen). In addition, the highest organic matters content in the study area occurred at the site with the finest sediments (NG-2).

Change in Distribution Characteristics of Surface Sediments of Weir Section in Nakdong River (낙동강 수계 보 구간 표층 퇴적물의 분포 변화)

  • Lee, Kwon Chul;Kim, Hyoung Geun;Lee, Hye Yun;Yang, Deuk Seok;Kim, Shin
    • Korean Journal of Ecology and Environment
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    • v.53 no.4
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    • pp.355-364
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    • 2020
  • This study was carried out to investigated changes in sediments in the eight weir sections of Nakdong River. Sediments were collected and analyzed for Grain Size, Ignition loss, Total Organic Carbon, Total Nitrogen, Total Phosphorus, and Meta. The upstream of the weir was found that fine-grained sediments have repeated increases and decreases. It was found that coarse-grained sediments were being maintained in the downstream part of the weir. The sediments Ignition Loss, Total Organic Carbon, Total Nitrogen, Total Phosphorus are strongly correlated with Grain Size, and these increased at the point where sediments are fine. In the case of metal, the concentration increased across the board, and the correlation with Grain Size, Ignition loss, Total Organic Carbon, Total Nitrogen, and Total Phosphorus was weak. Although there were some sections where fine-grained sediments, organic materials, nutrients, metals increased in the Nakdong River, the overall pollution level is considered weak.

Effect of Seeding on Microstructural Development of Silicon Nitride Ceramics (질화규소 세라믹스의 미세조직 형성에 미치는 Seed 첨가의 영향)

  • 이창주
    • Journal of Powder Materials
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    • v.5 no.2
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    • pp.133-138
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    • 1998
  • The effect of $\beta$-$Si_3N_4$ seeding on microstructural development of silicon nitride based materials has been investigated. In particular, to observe more distinctly the abnormal grain growth in pressureless sintering, fine $\alpha$-$Si_3N_4$(mean particle size: 0.26 ${\mu}m$) powder classified by sedimentation method was used. It was possible to prepare silicon nitride with abnormally grown grains under low nitrogen pressure of 1 atm thanks to the heterogeneous nucleation on $Si_3N_4$ seed particles. The size and morphology of silicon nitride grains were strongly influenced by the presence of $\beta$-$Si_3N_4$ seed and overall chemical composition. For specimens with initially low $\beta$-content, the large grains grew without a significant impingement by other large grains. On the contrary, for specimens with initially high $\beta$-content, steric hindrance was effective. The resulting microstructure was less inhomogeneous and characterized by unimodal grain size distribution.

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Fabrication of Undoped PbTiO3 Ceramics via Sol-Gel Processing (Sol-Gel Processing에 의한 순수 $PbTiO_3$ Ceramics 제조)

  • 김선욱;윤만순;임종인;김성숭;김남흥
    • Journal of the Korean Ceramic Society
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    • v.29 no.3
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    • pp.211-215
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    • 1992
  • Crack free PbTiO3 ceramics were produced by sol-gel processing using alkoxide, which has not been reported to be successful. The PbTiO3 gels were prepared from Ti alkoxide and lead acetate without any dopants. They were calcined at $600^{\circ}C$ and miled to produce fine PbTiO3 powder. It was pressed into discs and they were sintered at 110$0^{\circ}C$ for a few hours. The sintered ceramics were relativley hard and dense as having about 96% of theoretical density of PbTiO3. Fabrication of pure PbTiO3 ceramics by sol-gel processing is possibly due to their small grain size and uniform distribution of residual stress created during cubic-tetragonal transition over large number of small grains in fine grain PbTiO3 ceramics.

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A Study of the Effect of Tungsten Oxide on W, WC Powder and Alloy Properties

  • Jiang, Cijin;Shen, Paul;Wang, Huan
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.654-655
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    • 2006
  • This is about the effects deoxidization, carbonization and alloying preparation on fine grain W, WC, and grade YG8 powder reduced by "yellow tungsten oxide" and "blue tungsten oxide". The result indicates that yellow tungsten has single composition and blue tungsten oxide has complex composition. With this feature, yellow tungsten oxide got better uniformity and concentration distribution on fine particle size W and WC powder than blue tungsten oxide's. The grade alloy YG8 that made of this W or WC powder has uniform alloy construction, concentrated WC grain distribution and better alloy properties.

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Grain Size and Texture of Silver Minerals from Duk-Eum Ore Deposits (덕음광산(德音鑛山) 은광물(銀鑛物)의 입도(粒度)와 조직(組織))

  • Yang, Dong Yun;Chi, Jeong Mahn
    • Economic and Environmental Geology
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    • v.19 no.spc
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    • pp.227-237
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    • 1986
  • The Duk-Eum mine located in Kongsan-myeon, Naju-gun, Cheolanamdo is producing silver ore mainly, with rare gold association. The grade-up and recovery of the concentrates have been concerned to the main problem. And then, this study aimed at applying the basic data for ore processing. In the first half of the study, the attempts were made to identify the ore minerals, this followed by determination of the mineral texture, paragenesis, grain size, and size distribution by employing the microscopical method and the etching test. The results of the study are as follows: 1. The ore deposit is composed of the hydrothermal fissure linked veins, and filling cavities are mostly tensile fractures or joints, in rhyolitic rocks as a wall rock. 2. The principle ore minerals are native silver, acanthite, canfieldite, pyrargyrite, galena, tetrahedrite, sphalerite, pyrrhotite, chalcopyrite, chalcocite, covellite, zincite, and the gangue minerals are quartz and calcite. 3. The grain size of each ore minerals before grinding are; max. $2\frac{1}{2}$ mesh, medium 48-100 mesh(main size, contained over 80%), min. 3200mesh. And the grain size of each ore minerals after grinding is; max. 42mesh, medium 65-250mesh(main size, contained over 80%), min. 3200mesh. 4. The properties of the mineral texture effected on the ore dressing are follows; a) Inclusion texture; the fine grains of chalcopyrite is included in most acanthite, and rarely, that of galena included in acanthite. b) Exsolution texture; pyrargyrite is exsolved in acanthite. c) Replacement texture; native silver replaced pyrargyrite, and acanthite replaced galena. d) Interlocking paragenetic texture; the interlocking paragenetic minerals are pyrite, chalcopyrite, chalcocite, canfieldite. e) Fissure filling texture; chalcopyrite was filled along the cracks in acanthite. Among of the above texture, it is impossible to liberate the grains of a), and more difficult to liberate those of b) and c), while easy to liberate those of d) and e).

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Effects of Y2O3 and Al2O3 Addition on the Properties of Hot Pressed AlN Ceramics (AlN 세라믹의 hot pressing에 사용되는 Y2O3 및 Al2O3 소결조제의 효과)

  • Kong, Man-Sik;Hong, Hyun-Seon;Lee, Sung-Kyu;Seo, Min-Hye;Jung, Hang-Chul
    • Korean Journal of Materials Research
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    • v.17 no.10
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    • pp.560-566
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    • 2007
  • AlN plates were fabricated by hot pressing at $1700-1900^{\circ}C$ using yttria and alumina (3 and $10\;{\mu}m$ particle size) powders as additives and characterized: density, thermal conductivity, transverse rupture strength, and grain size measurement by SEM and EDS. Density values of $3.31-3.34\;g/cm^3$ are largely attributed to hot pressing of powder mixtures in carbon mold under $N_2$ atmosphere which caused effective degree of oxygen removal from yttrium-aluminate phase expected to form at $1100^{\circ}C$. The grain size of hot pressed AlN was almost homogeneous, with size approximately from 3.2 to $4.0\;{\mu}m$ after hot pressing. $Al_2O_3$ powder of $3\;{\mu}m$ particle size resulted in better transverse rupture strength and finer grain size compared to $10\;{\mu}m$ $Al_2O_3$ powder. The thermal conductivity of AlN ranged between $83-92.7\;W/m{\cdot}K$ and decreased with $Al_2O_3$ addition. Fine grain size is preferred for better mechanical properties and thermal conductivity.

Effect of Aggregates on the Sintering Behavior of $BaTiO_3$ (응집입자가 $BaTiO_3$의 소결거동에 미치는 영향)

  • 김진호
    • Journal of the Korean Ceramic Society
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    • v.28 no.11
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    • pp.926-934
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    • 1991
  • The effect of aggregates on the forming and sintering behaviors of BaTiO3 was studied. Aggregates and deaggregates of fine crystallite were obtained by thermal decomposition of oxalate coprecipitates and subsequently crushing them with a press, respectively. Large voids formed by packing of aggregates were not easily eliminated despite the successive destruction of aggregates with increasing forming pressure. As a result, compacts of aggregates showed inhomogeneity with larger mid-pore size and broader pore size distribution with respect to those of deaggregates. This inhomogeneity caused differential shrinkage and consequental internal stress, which retarded densification. The differential sintering increased the size of mid-pores in the initial stage, and formed duplex structure composed of dense region with abnormally grown grains and porous region with fine grains. The driving force of this abnormal grain growth shown in the specimens of aggregates was attributed to the minimization of the elastic strain energy due to internal stress.

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