• 한국축산식품학회지
• /
• 제38권4호
• /
• pp.823-828
• /
• 2018

The purpose of this study was to evaluate the suitability of the released water (RW) method for measuring water-holding capacity (WHC) by pressure and filter-paper absorption within two thin plastic films. One hundred fifty pork loins with considerable variations in WHC (three pork qualities: PSE, pale, soft, and exudative; RFN, reddish-pink, firm, and nonexudative; and DFD, dark, firm, and dry; 50 pork loins in each pork quality group) were used to measure drip loss (DL)% and RW % after applying different loads (1.5, 2.0, 2.5, 3.0 and 3.5 kg). Percentages of DL and RW were significantly (p<0.05) different among pork quality groups. The RW % of 2.5 kg load sample was significantly (p<0.05) higher than that of 2.0 kg or 1.5 kg load sample. However, there were no significant (p>0.05) differences in RW % among 2.5 kg, 3.0 kg, and 3.5 kg load samples for all three pork quality groups. The RW % was highly and positively correlated (r>0.95; p<0.001) with DL %. The highest correlation was observed between DL % and RW % of 2.5 kg load sample (r=0.97; p<0.001). Among all RW loads within each quality groups, the highest correlation between DL % and RW % was observed for 2.5 kg load sample (r=0.43, 0.66, and 0.46 for PSE, RFN and DFD quality groups, respectively, p<0.001). These results imply that applying 2.5 kg load is the best for determination of RW %. It is recommended as a reference method to assess DL % of pork muscles.

• 약학회지
• /
• 제3권1호
• /
• pp.48-50
• /
• 1957

The micro-assay methods of vanillin have been shown quite few, though several methods have been introduced for determination. A new sensitive micro-determination of vanillin, applying the yellow color reaction of vanillin and anillin, is shown in this paper. The absorption maximum of the yellow coloring matter, 4-Oxy-3-methoxy-henzal aniline, was 435 mu. The one dimensional ascending paper chromatographic method is applyed for isolation of vanillin from the mixed sample. The microdetection of vanillin is studied only in this paper. Vanillin was detected by the yellow spot on paper trip by the coloring reagent of aniline after several hours paper strip chromatographic at the following condition; paper strip ................ 2.5 X 35cm Whatman Filter Paper No.2 developing Solvent ......... petroleum-benzene-methanol n-butanol-water coloring agent ............. aniline. The Rf-value on petroleum benzene and methanol was 0.63 and that on n-butanol and water was 0.90. The minimum detectable amount of vanillin by this method was 10 micrograms. It is recommendable, if interference substances as aromatic aldehydes present, that the application of this aniline reaction and Foline Denis reaction on the same paper chromatogram is appreciable.

• 한국식품과학회지
• /
• 제15권2호
• /
• pp.133-134
• /
• 1983

Some metallic ions such as copper, manganese, iron, zinc and cadmium in ginseng extract, originated from white ginseng, were determined by atomic absorption spectrophotometry. The extracts were prepared with water, 35% ethanol, 50% ethanol or 75% ethanol solution followed by filtration or centrifugation. Greater amounts of metallic ions were found in the solution filtrated by filter paper (Toyo No. 5A) or by filter cloth than in that of centrifugation. The residual amount of metallic ions in the extract decreased with increasing concentration of ethanol. The percentages of each metallic ion in ginseng extracts on the basis of original amount of metallic ions were as follows: Cu, 10.4-31.9%, Fe,5.1-19.0%, Mn,3.0-12.2% Zn,7.4-12.0%, Cd,5.9-11.8%.

• Applied Biological Chemistry
• /
• 제12권
• /
• pp.99-105
• /
• 1969

Trichoderma $(O_2-1)$의 조효소(粗酵素)를 Ethanol 및 Acetone 농도별(濃度別)에 따른 회수율(回收率)을 실험(實驗)한 결과(結果) 각(各) cellulase는 현저(顯著)한 차이(差異)가 나타났다. 즉(卽) Ethanol을 사용(使用)하였을 경우 ${\beta}-glucosidase$는 60% C.M.C분해효소(分解酵素), 여지붕괴(濾紙崩壞濾) 효소(酵素)는 80% 일때가 좋았고 Acetone을 사용(使用)하였을 경우 ${\beta}-glucosidase$는 60% 여지붕괴(濾紙崩壞濾) 효소(酵素)는 80%, C.M.C분해효소(分解酵索)는 90% 농도(濃度)일때가 좋은 결과(結果)를 나타내었다. 조정제(粗精製)한 Cellulase를 Silicagel, cellulose powder, Gauze를 사용(使用)한 column chromatography에 의(依)하여 분별(分別)란 결과(結果) 수치(數個)의 구분(區分)으로 분별(分別) 할 수 있었다. C.M.C 분해효소(分解酵索)와 Avicel 분해효소(分解酵索), ${\beta}-glucosidase$의 대부분(大部分)은 흡착(吸着)이 되지않고 유출(流出)되었으며, 대부분(大部分)의 여지붕괴효소(濾紙崩壞濾酵素)와 일부분(一部分)의 Avicel분해효소(分解酵索)는 흡착(吸着)되었다가 증류수(蒸溜水)로서 유출(流出)함으로씨 용출(溶出)되었다. 따라서 C.M.C 분해효소(分解酵索)와 여지붕괴효소(濾紙崩壞濾酵素)는 상이(相異)한 Cellulase 성분(咸分)임을 알았다. 또 C.M.C 분해효소(分解酵索)와 Avicel 분해효소(分解酵索)는 용출구분(溶出區分)에 있어 peak가 상이(相異)한 다른 구분(區分)에서 상대활성(相對活性)이 다르므로 역시 별개(別個)의 종류(種類)로 구분(區分)되었다. 또 여지붕괴효소(濾紙崩壞濾酵素)와 Cellulose powder (여지분말(濾紙粉沫)) 당화효소(糖化酵素)는 흡착구분(吸着區分)과 비흡착(非吸着) 구분(區分)으로 분별(分別)되니 사이(相異)한 Cellulase 성분(成分)이라고 생각된다. 따라서 Trichoderma viride $(O_2-1)$의 Cellulase는 적어도 3종이상(種以上)의 Cellulase 성분(成分)으로 되어 있다고 추찰(推察)된다.

• 보존과학연구
• /
• 통권7호
• /
• pp.56-86
• /
• 1986

The aim of this study is to scientifical conservation for the Sin An Ship. The test object is Pinus massoniana and Cunninghamia lanceolata of Sin An Ship's timber .Comtrast object is water soaked fresh wood of Pinus densiflora and Cryptomeria japonica The results were as follows.1. M. C is 280.9% in high degraded Planking board,237.5% in low degraded Planking board,158.6% in fresh wood of Pinus densiflora,222.6% in Bulkhead167.3% in fresh wood of Cryptomeria japonica2. Absorption rate of P.E.G is good at heating condition ($55∼60^{\circ}C$), especially in highdegraded wood.3. The dimensional change of wood during air drying is somewhat shrinked That's 7.22% in low degraded Planking board9.8% in high degraded Planking board and 4.11% in water soaked Pinus densiflora.4. The dimensional change of wood during P.E.G treatment is mostly swollen of wery small quantity.5. Salinity in desalinization tank showed below 50 p.p.m. It's indicate the end of desalinization treatment.6. Filtration with filter paper was possible up to 40% concentration only. Key words :M.c ; Moisture Content, Absorption rate, Dimension change, Salinity, Filtration.

• 조명전기설비학회논문지
• /
• 제14권1호
• /
• pp.53-58
• /
• 2000

본 논문에서는 에폭시 복합 절연재료를 옥외에서 사용할 경우 수분의 영향을 고찰하기 위하여 비등홉수조건에 서 기계적 강도와 절연파괴강도의 변화를 측정하였다. 또한 내습성을 개선하기 위한 방법으로 이전에 보고하였던 상호침입망목 수법을 도입하여 그 효과를 비교 검토하였다. 두 종류의 모체수지에 충진재를 0, 50, 100 [phr] 첨가하여 총 6종류의 시편을 제작하였다. 그 결과, 비등흡수시간과 충진재 함량이 증가함에 따라 수분 흡수율이 증가되었고, 기계적 강도와 절연파괴강 도가 저하됨올 확인하였다. 반면 상호침입망목 시편의 경우에서는 접착강도의 개선에 의하여 홉수율이 낮아지고, 기계적 강도와 절연파괴 강도의 저하율이 완화됨을 확인하였다.

• 한국식품영양과학회지
• /
• 제7권1호
• /
• pp.43-52
• /
• 1978

It is well known that water holding capacity plays an important role in processing such meat products as frankfurter-type sausage and fish meat paste products as kamaboko and fish sausage. Consumer qualities of meat products, such as appearance, flavor, as well as drip and shrinkage on cooking, depend greatly on the degree of water binding. In this paper, the water holding capacities of fish paste and salt added paste of white corvenia, Argyrosomus argentatus and file fish, Novodon modestus were measured by centrifuging and press method before and after cooking. And the effects of the addition of phosphates and starch to enhance water binding and stabilize gel formation were also discussed. In addition, the experimental conditions which are suitable to determine the water binding of fish meat paste product were suggested. The results were expressed in percent of water absorbed by the filter paper when pressed or released by pressor or centrifuge to the weight of sample. From the results. a proper condition to measure the water holding capacity of fish meat paste was that 3.0 g of sample which was previously added with 10 percent water was centrifuged at 13,400 G or 12,000 rpm for 15 minutes for the centriguging method and for press method, 0.3 g sample with 10 percent of water added was extracted by an oil pressor at $30\;kg/cm^2$ for 1 minute. Water holding capacity of fresh paste of white corvenia was relatively higher than that of file fish and the difference between species of fish was greater than the difference between measurments by two methods. Sodium chloride had a great effect on enhancing the water holding capacity of fish meat paste giving better effect when 3.0 percent of salt was added. Phosphates used except calcium phosphate revealed a certain enhancement in water binding, yielding best effect at 0.3 percent addition, and metaphosphate seemed to be more effective in order. The addition of corn starch, however, appeared to be not so effective for enhancement of water binding in fresh-salt-added fish meat paste but in cooked fish paste which might be attributed to absorption of water by starch grain and swelling during the heating and consequently enforced gel strength of cooked fish paste. And the water holding capacity of cooked fish paste was proportionally related to its gel strength.

• 한국식품과학회지
• /
• 제17권6호
• /
• pp.522-525
• /
• 1985

건조된 콩우유 비지의 첨가가 두부의 품질(品質)에 어떠한 영향을 미치는지 조사하고자 제조된 두부의 부피, 견고성, 보수력 그리고 관능적 성질을 비교하였다. Acetone으로 세척하여 건조(乾燥)된 비지를 건물량 기준으로 원료(原料) 대두(大豆)에 10-30% 되게 여과된 대두 추출액에 혼합하여 두부를 제조하였을 때 부피 및 보수력(保水力)의 감소와 침입도(針入度)의 증가가 있었다. 건조비지의 혼합비율(混合比率)을 10%로 할때는 침입도(針入度)는 감소하였으나 Sag의 값이 감소함으로서 딱딱함은 오히려 증가하였고 부피의 감소는 비교적 적었다. 또한 관능적(官能的) 성질(性質)인 부서짐성과 과립성이 향상되어 10% 범위 내에서의 건조비지 혼합에 의한 두부제조의 가능성을 보여주었다. 또한 두부의 보수력(保水力) 비교를 위하여 여과지에 비결합수(非結合水)를 흡착시켜 측정함이 간편하며 비교성이 좋은 방법(方法)임이 밝혀졌다.

• Applied Biological Chemistry
• /
• 제33권3호
• /
• pp.203-208
• /
• 1990

대두의 주요품질중 텍스쳐, 보수력, 색 및 Sag값 등 물리적 특성을 국내에서 재배되는 14가지의 콩 품종에 대해여 비교하였다. 텍스쳐는 rheometer로 측정하였으며 보수력은 여과지 흡수방법으로 측정하였다. 그 결과 두부의 보수력은 밀양-21호, 단엽콩, 황금콩이 높았고, 수원-138호, 수원-141호, 수원-142호는 낮았다. Sag값은 모두(-)값을 보여 성형시 가해졌던 압력을 제거하였을 때 두부가 부풀었음을 알 수 있었고 부풀음 정도는 수원-l38호로 제조한 두부가 가장 높았고, 수원-142호의 두부가 낮았다. 두부의 견고성은 품종별로 큰 차이가 있어 일반적으로 두부의 수분함량이 견고성에 영향을 주었으나 유의적인 관계는 없었다. 가장 단단한 두부는 수원-133호와 장엽이었고 가장 연한 두부는 팔당과 수원-142호이었다. 탄력성과 응집성은 수원-138호 이외에는 큰 차이가 없었으며 그 외의 관능적, 텍스쳐 성질인 부서짐성, 부착성, 검성은 품종간의 차이가 많았다.

• 한국대기환경학회지
• /
• 제22권1호
• /
• pp.117-126
• /
• 2006

The purpose of this study is to develop a badge-type passive sampler for the measurement of short-term nitrogen dioxide and to evaluate its performance. The principle of the method is a colorimetric reaction of nitrogen dioxide with sulfanilic acid, N-1-naphthylethylendiamine, and phosphoric acid. First, it has been shown that the filter paper should be rinsed with ultrapure water and ultrasound, and then dried in a vacuumed desiccator. The concentration and volume of absorption reagent (triethanolamine) were $20\%$ and 100 ${\mu}L$, respectively. The extraction time was determined as 60 min. Second, duplicate measurements (n= 116) were carried out for evaluating the precision of the passive sampler. The relative error and the correlation coefficient between duplicates are $3.4\pm 3.0\%$ and 0.994, respectively. In addition, the $95\%$ confidence interval of intraclass correlation coefficient and the estimated value are 0.992$\sim$0.996 and 0.994, respectively. Third, a paired t-test was carried out for evaluating the accuracy of the passive sampler (n=40). In the result of the test, the $95\%$ confidence interval of the difference was -1.710 ppb <$\gamma$< 0.788 ppb. Finally, the average concentration of blanks, measurement detection limit, limit of detection, and limit of quantification are $2.4\pm 0.4$ ppb, 104 ppb, 3.8 ppb, and 7.0 ppb, respectively.