• 한국염색가공학회지
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• 제32권1호
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• pp.44-50
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• 2020

In this study, pre-treatment was performed on kapok, a hydrophobic fiber, to compare dyeability by hydrophilization. The pretreatment conditions of kapok fiber were used with different amounts of sodium oleate(NaO), a fatty acid-based anionic surfactant, and xanthan gum(XG) as a natural thickener. At this time, NaO and XG were separately or mixed treated with 0.01%, 0.1%, 1% aqueous solution at 80℃ for 30 min. Hydrophilicity through dyeing was confirmed using Sappan wood extract. Therefore, SEM observation was performed to investigate the surface change of kapok fiber according to the conditions. The surface color difference was also analyzed. Pretreated kapok fibers were made from nonwoven fabrics and the contact angles were measured to determine their hydrophilization. The surface of the fiber after pretreatment was found to be cracked when NaO and NaO were mixed with XG. The surface color was the highest in a^⁎ and K/S values after the simultaneous treatment of NaO and XG, followed by NaO pretreatment and XG pretreatment. The contact angle of kapok fiber made of nonwoven fabric was slightly lower at 300g/㎡ than the fabric weight of 150g/㎡. Such hydrophilized nonwoven kapok fiber are expected to be used in various fields.

• 한국염색가공학회지
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• 제8권2호
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• pp.56-63
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• 1996

Low-temperature plasma treatment or sputter etching is of interest as one of the techniques to modify polymer surface. In this study, poly(ethylene terephthalate)(PET), nylon 6 and cotton fabrics dyed three black dyes were subjected to low-temperature argon plasma and also sputter etching. In relation to bathochromic effect, the surface characteristics of the treated fabrics and films were investigated by means of critical surface tension, SEM and ESCA measurement. The depth of shade of fabrics more increased by the sputter etching technique than argon plasma treatment. Many microcraters on the fiber surface formed by the sputter etching resulted in increase of surface area of the fiber and wettability, but the hydrophobic group was increased by the results of ESCA analysis. In particular the change in reflective index of the fibers was much more effective than the chemical composition of the fiber surface on increasing of the depth of shade.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1995년도 춘계학술대회 논문집
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• pp.216-219
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• 1995

One of the principal problems encountered in the use of glass fiber reinforced Plastic composites(GFRP) is to establish an active fiber surface to achieve maximum adhesion between resin and fiber surface. In order to develope new process to overcome the disadvantage of chemical agent, we have studied the effect of reactive plasma glass surface treatment on the electrical and mechanical properties of glass fiber reinforced epoxy composites. It is found that the electrical and mechanical characteristics of the composites treated with plasma is improved especially in the dielectric strength by 20% and tensile strength by 15%, whereas the tan $\delta$ is decreased significantly.

• 콘크리트학회논문집
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• 제21권3호
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• pp.275-282
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• 2009

본 연구에서는 CFRP 보강근과 고강도콘크리트의 부착강도에 미치는 보강섬유의 표면처리 방법의 효과를 평가하였다. 표면을 친수성 물질로 코팅된 구조용 PVA 섬유 및 기하학적 변형으로 변형된 절곡형 폴리올레핀계 구조용 합성섬유를 보강섬유로 사용하였다. 섬유의 표면처리 방법에 따른 고강도콘크리트의 강도특성을 평가하기 위하여 압축강도 실험을 실시하였다. 고강도콘크리트와 CFRP 보강근 사이의 부착특성은 직접 부착강도시험을 의하여 평가하였다. 시험 결과는 섬유의 표면처리 방법은 고강도콘크리트와 CFRP 보강근 사이의 부착거동에 영향을 미쳤다. 또한 고강도콘크리트에 섬유의 첨가는 할렬균열의 발생 및 성장을 조절함으로써 고강도콘크리트와 CFRP 보강근 사이의 부착거동, 부착강도 및 상대부착강도의 증가시켰다.

• 한국염색가공학회지
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• 제27권1호
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• pp.18-26
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• 2015

para-aramid fibers were treated by atmosphere air plasma to improve the interfacial adhesion. The wettability of plasma-treated aramid fiber was observed by means of dynamic contact angle surface free energy measurement. Surface roughness were investigated with the help of scanning electron microscopy and atomic force microscopy. The tensile test of aramid fiber roving was carried out to determine the effect of plasma surface treatments on the mechanical properties of the fibers. A pull-out force test was carried out to observe the interfacial adhesion effect with matrix material. It was found that surface modification and a chemical component ratio of the aramid fibers improved wettability and adhesion characterization. After oxygen plasma, it was indicated that modified the surface roughness of aramid fiber increased mechanical interlocking between the fiber surface and vinylester resin. Consequently the oxygen plasma treatment is able to improve fiber-matrix adhesion through excited functional group and etching effect on fiber surface.

• 한국연초학회지
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• 제25권2호
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• pp.111-119
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• 2003

In this work, Rayon-based activated carbon fiber(KF-1500) was treated by HN $O_3$ and $H_2$S $O_4$ with different conditions. Specific surface areas(SSA, $S_{BET}$) of the treated activated carbon fibers were decreased by acidic treatment but, total surface acidities and surface functional groups were increased. In spite of the decrease of SSA, propylamin(PPA) adsorption and removal ability by activated carbon fiber(ACF) were increased by nitric acid treatment compared with the raw-ACF(KF-1500) and coconut based activated carbon. However, acidic treated activated carbon fibers were available to removal for various amines and contaminants by adsorption.n.

• 대한금속재료학회지
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• 제46권8호
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• pp.471-476
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• 2008

There has been a growing interest for the use of natural fibers in composite applications due to their low cost, environmental friendliness, and good mechanical properties. It was demonstrated to determine the characteristic of tensile behaviors under the variation of test temperature on sisal fiber reinforced polymer composites by RTM process. Especially, the permanganate-treated-fibers improved tensile strength by increasing the coherence with matrix. Material deformation is restricted to increment of cohesion for surface treatment of fiber and then elongation decreas.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 1999년도 추계학술발표대회 논문집
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• pp.40-43
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• 1999

Electrochemical surface treatment of PAN-based carbon fibers in acidic electrolyte has been studied in increasing the surface functional groups on fiber surfaces for the improvement of fiber-matrix adhesion of the resulting composites. According to the FT-IR and XPS measurements, it reveals that the oxygen functional groups on fibers are largely influence on the composite mechanical behaviors, whereas the nitrogen functional groups are not affected in the system. In this work, a good correlation between surface functionality and mechanical properties is established.

• 폴리머
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• 제31권1호
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• pp.31-36
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• 2007

플라스마 표면처리는 전체적인 물성은 유지하고 표면의 특성만을 변화시킨다고 전해지고 있다. 이번 연구에서는 플라스마 처리에 의해 높은 발수성을 나타내는 나일론 6 섬유로의 개질을 시도하였다. 발수성을 나타내는 나일론 섬유는 가스 종류, 처리시간, 인가 파워를 변수로 하여 RF 진공 플라스마 시스템에서 처리되었다. 플라스마 처리된 섬유의 표면을 scanning electron microscopy(SEM)과 atomic force microscopy(AFM)으로 모폴로지 변화를 살펴보았으며, 기계적 특성과 고분자 고유의 특성을 인장강도와 Differential scanning calorimetry(DSC), thermo-gravimetric analysis (TGA)로 각각 분석하였다. 또한 나일론 섬유의 발수성 평가는 물방울 흡수시간으로 테스트를 실시하였다. 이러한 결과들은 플라스마 표면처리로 인해서 나일론 섬유의 발수성이 향상됨을 나타내었다.

• 한국섬유공학회:학술대회논문집
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• 한국섬유공학회 1993년도 ACT 93
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• pp.622-626
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• 1993