• Title/Summary/Keyword: fiber method analysis

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An Investigation on the Airborne Asbestos Concentrations using PCM and TEM in the Public Buildings in Seoul (PCM과 TEM을 이용한 서울지역 일부 공공 건축물의 실내공기 중 석면농도 조사)

  • Chung, Sook-Nye;Nam, Eun-Jung;Hwang, Soon-Yong;Oh, Seok-Ryul;Shin, Jin-Ho;Eom, Seok Won;Chae, Young-Zoo
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.21 no.3
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    • pp.139-145
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    • 2011
  • Objectives: This investigation is purposed to evaluate the airborne asbestos concentrations in the public buildings having asbestos containing materials(ACMs) in Seoul. Methods: The Seoul Metropolitan Government carried out an asbestos survey to the city-owned public buildings to identify the level of risk exposure, classified into low, moderate and high risk. To evaluate the airborne concentration of asbestos, 11 sampling sites in ten buildings based on the survey were selected. The air samples from the eleven sites were analyzed by Phase Contrast Microscopy(PCM) and Transmission Electron Microscopy (TEM), and compared the analytical results from the both. Results: 1. The airborne fiber concentrations by PCM were less than the detection limit($7f/mm^2$) in 9(82%) out of 11 sampling sites. The highest concentration was 0.0043 f/cc, but it was below the guideline value for indoor air quality(0.01 f/cc), proposed by the Ministry of Environment, Korea. 2. In two sampling sites, having moderate risk level, the chrysotile was identified and showed it's concentrations of 0.0102 s/cc and 0.0058 s/cc, less than $5{\mu}m$ lengths. 3. The ACMs identified in the two sampling sites were a packing material(65% of chrysotile) in mechanical area and a thermal system insulation(5% of chrysotile) in a boiler room. Having more possibility of asbestos emission in the mechanical area, it would be required to set up and carry out the asbestos management plan. Conclusions: Based on the result of this study, the airborne asbestos concentrations in the public buildings with ACMs were generally lower than the guideline value for indoor air quality. There are widespread concerns about the possible health risk resulting from the presence of airborne asbestos fibers in the public buildings. Most of the previous studies about airborne asbestos analysis in Korea were performed based on PCM method that asbestos and non-asbestos fibers are counted together. In the public and commercial buildings, having ACMs, it is suggested that the asbestos be analyzed by TEM method to identify asbestos due to concerns about asbestos exposure to workers and unspecified people.

Conservation of Liaoning-type Bronze Dagger Excavated in Wollae-dong, Yeosu (여수 월내동 출토 비파형동검의 보존)

  • Ahn, Jooyoung;Yun, Eunyoung;Park, Haksoo;Jeon, Hyosoo
    • Conservation Science in Museum
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    • v.13
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    • pp.51-58
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    • 2012
  • The Conservation Science Team of the National Museum of Korea has carried out the conservation on the mandolin-type bronze sword that was excavated from Weolnae-dong, Yeosu as had been requested by the Research Center of Dolmens in Northeast Asia. The mandolin-type bronze sword from Weolnae-dong, Yeosu is accounted to be the longest one among all the bronze swords of the same type that have ever been excavated until now and it was in a treated condition with the primary conservation treatment already achieved. Due to the corrosion in progress, it was in a very brittle condition being in two separate parts of the upper and lower parts. With the upper part exposed and the lower part with earth, they were urgently collected. The Conservation Science Team carried out the conservation treatment on them by connecting the lower part of the mandolin-type bronze sword to the upper part after making the lower part exposed, and then by using an estimated restoration method for lost portions. When carrying out the conservation treatment, the glass fibers of 10 wt% Paraloid B-72 (in Xylene) was used as a method for strengthening the brittle artifact, and a non-destructive analysis was carried out to identify the ingredients using the X-ray fluorescence spectrometer.

Fracture Characteristics of C/SiC Composites for Rocket Nozzle at Elevated Temperature (로켓 노즐목 소재 C/SiC 복합재 고온 파괴 특성)

  • Yoon, Dong Hyun;Lee, Jeong Won;Kim, Jae Hoon;Sihn, Ihn Cheol;Lim, Byung Joo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.40 no.11
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    • pp.927-933
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    • 2016
  • In a solid propulsion system, the rocket nozzle is exposed to high temperature combustion gas. Hence, choosing an appropriate material that could demonstrate adequate performance at high temperature is important. As advanced materials, carbon/silicon carbide composites (C/SiC) have been studied with the aim of using them for the rocket nozzle throat. However, when compared with typical structural materials, C/SiC composites are relatively weak in terms of both strength and toughness, owing to their quasi-brittle behavior and oxidation at high temperatures. Therefore, it is important to evaluate the thermal and mechanical properties of this material before using it in this application. This study presents an experimental method to investigate the fracture behavior of C/SiC composite material manufactured using liquid silicon infiltration (LSI) method at elevated temperatures. In particular, the effects of major parameters, such as temperature, loading, oxidation conditions, and fiber direction on strength and fracture characteristics were investigated. Fractography analysis of the fractured specimens was performed using an SEM.

Analysis of Nutritional Compositions and Antioxidative Activities of Korean Commercial Blueberry and Raspberry (국내 시판 블루베리와 라즈베리의 영양성분 분석 및 항산화 활성)

  • Jeong, Chang-Ho;Choi, Sung-Gil;Heo, Ho-Jin
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.37 no.11
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    • pp.1375-1381
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    • 2008
  • The nutritional compositions and antioxidative activities of Korean commercial blueberry and raspberry were investigated. The proximate compositions were 10.47% and 22.67% in moisture, 2.66% and 2.64% in crude protein, 2.04% and 1.67% in crude fat, 81.36% and 70.19% in nitrogen free extracts, 1.48% and 0.85% in crude fiber, and 1.99% and 1.98% in ash of blueberry and raspberry, respectively. Total phenolics content were higher in blueberry (9.028 mg/g) than in raspberry (5.340 mg/g). Major elements of blueberry and raspberry were Ca (451.34 and 97.48 mg/100 g), K (355.40 and 215.20 mg/100 g), P (321.10 and 294.04 mg/100 g), and Na (137.58 and 137.67 mg/100 g). The total amino acid contents of blueberry and raspberry were 2,011.44 mg /100 g and 2,098.82 mg/100 g, respectively. Amino acid were mainly composed of glutamic acid, aspartic acid and leucine. The DPPH and ABTS radical scavenging activities of the 80% methanol extract from blueberry and raspberry were 88.67% and 62.77%, 76.34% and 30.53% at a concentration of 5 mg/mL. The 80% methanol extract from blueberry and raspberry showed considerable antioxidative activity against reducing power in dose-dependent manner. Antioxidative activities using $\beta$-carotene-linoleate and FTC method were twice higher in blueberry than raspberry.

The Fundamental Studies and Development of Modified Electrothermal Vaporization Hollow Cathode Glow Discharge Cell (개선된 전열증기화 속빈음극관 글로우 방전셀의 기초연구 및 개발)

  • Lee, Seong-Hun;Cho, Won-Bo;Jeong, Jong-Pil;Choi, Woo-Chang;Kim, Kyu-Whan;Woo, Jeong-Su;Lee, Chang-Su;Kang, Dong-Hyun;Lee, Sang-Chun
    • Analytical Science and Technology
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    • v.15 no.6
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    • pp.514-520
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    • 2002
  • The electrothermal vaporization (ETV) hollow cathode glow discharge atomic emission spectrometer for analysis of liquid sample has been developed and characterized. This system has improved the sample introduction method of electrothermal vaporization and the hollow cathode glow discharge. The sample introduction method was possible to provide high analyte transport efficiency to the plasma by helix coil made of tungsten material. In addition, small volume samples (<$30{\mu}{\ell}$) could be used. The system has glow discharge cell with special design for improvement of precision. The effect of discharge parameters such as discharge power, gas flow rate has been studied to find optimum condition. The emitted light was effectively carried into detector by fiber optic cable in UV region. The calibration curve of Pb, Cd were obtained with 3 samples.

Characterization of fine organic aerosols from biomass burning emissions using FTIR method (분광학적 방법을 이용한 바이오매스 연소 배출 유기 입자의 화학적 특성)

  • Son, Se-Chang;Park, Tae-Eon;Park, Seungshik
    • Particle and aerosol research
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    • v.17 no.4
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    • pp.125-132
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    • 2021
  • Fresh PM2.5 smokes emitted from combustion of four biomass materials (pellet, palm fruit fiber (PFF), PKS, and sawdust) in a laboratory-controlled environment were characterized using an attenuated total reflectance-fourier transform infrared (ATR-FTIR) technique. In smoke samples emitted from combustion of pellets, PFF and PKS, which is being used as boiler fuels for greenhouses in rural areas, the organic carbon/elemental carbon (OC/EC) ratios in PM2.5 were very high (14.0-35.5), whereas in sawdust smoke samples they were significantly low (<4.0) due to the combustion method close to flaming combustion. ATR-FTIR analysis showed that OH(3400-3250 cm-1), CH3(2958-2840 cm-1), CH2(2910 cm-1 and 2850 cm-1), ketone(1726-1697 cm-1), C=C(1607-1606 cm-1 and 1515-1514 cm-1), lignin (1463-1462 cm-1 and 1430-1428 cm-1) and -NO2(1360-1370 cm-1) peaks were identified in all biomass burning (BB) smoke samples. However, additional peaks appeared depending on the type of biomass. Among the four types of biomass materials, an additional peak of the methylene group CH3(2872-2870 cm-1) appeared only in PFF and PKS smoke samples, and a peak of C=O(1685 cm-1) was also confirmed. And in the case of PKS smoke samples, a peak of aromatic C=C(1593 cm-1 and 1476 cm-1) that did not appear in other BB samples was also observed. This indicates that the molecular structure of organic compounds emitted during BB differs depending on the type of biomass materials. The results of this study are expected to provide valuable information to more specifically reveal the effect of BB on PM2.5 collected in the atmospheric environment.

Effect of Seeding Methods and Nitrogen Fertilizer Rates on the Forage Quality and Productivity of Whole Crop Rice (파종방법 및 질소시비량이 총체 벼의 수량 및 사료가치에 미치는 영향)

  • Kim, Jong Geun;Park, Hyung Soo;Lee, Sang Hoon;Jung, Jeong Sung;Ko, Han Jong
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.35 no.2
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    • pp.87-92
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    • 2015
  • This experiment was conducted to evaluate the effect of seeding methods and application levels of nitrogen fertilizer on the yield and forage quality of whole crop rice (WCR). The WCR variety "Namil" was directly seeded on April 25 and transplanted on May 25. Five levels of nitrogen fertilizer were applied (90, 110, 140, 170 and 200 kg/ha). There were no significant differences (p<0.05) of the emergence date, heading date and disease resistance based on the nitrogen fertilizer rates; however, the WCR became dark at higher nitrogen fertilizer rates. The plant height increased at higher nitrogen fertilizer rates and the tiller number showed the same trend. In contrast to a direct seeding method, transplanting increased the tiller number. The dry matter (DM) content did not show a certain tendency based on nitrogen fertilizer rates, while the fresh and dry matter yields increased with incremental changes of the nitrogen fertilizer rates (p<0.01), and the transplant method increased the yield size. In yield analysis, the plot direct-seeded with 140 kg N/ha and the transplanting with 170kg N/ha showed the highest yields. The crude protein (CP) content increased with higher nitrogen fertilizer rate, but there was no significant differences between transplant and direct-seeding methods. The content of ADF (acid detergent fiber) and NDF (neutral detergent fiber) increased with higher nitrogen fertilizer rate, but total digestible nutrient (TDN) content decreased with increased nitrogen levels. Although high nitrogen applications increased the fresh and DM yields, the 140 kg/ha nitrogen fertilizer level is recommended as the proper nitrogen fertilizer level, considering both yield and the environments.

A Study on the Nutrient Intake and Food Habits of College Students in Chung-Nam Area (충남 일부지역 대학생의 식이섭취 및 식습관 실태조사)

  • Kim Myung-Hee;Lee Ye-Seung
    • The Korean Journal of Community Living Science
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    • v.17 no.3
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    • pp.143-158
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    • 2006
  • The study examined nutritional conditions to enhance the quality of meals and to provide the basic data for more proper dietary life of college students. Our analysis was based on the body measurement, food intake and food habits for 200 students of Chung-Nam. The nutrient intake was examined using the 24-hour recall method. The data were analyzed by the Computer Aided Nutritional Analysis Program and then the diet quality was estimated using the Mean Adequacy Ratio(MAR), the Nutrient Adequacy Ratio(NAR) and the Index of Nutritional Quality(INQ). The average weight and height of male students were $67.57{\pm}8.66kg,\;174.64{\pm}5.87cm$, while those of female students were $53.46{\pm}6.86kg,\;159.10{\pm}4.19cm$, respectively. The total energy intake of the male students was $3221.71{\pm}200.39kcal$, while that of the female students was $1884.67{\pm}100.93kcal$. The male students are higher than female in % of RDA. The percentages of carbohydrate, protein and lipid for male students were $57.18{\pm}7.83%,\;15.15{\jpm}3.36%\;and\; 27.67{\pm}6.68%$, while those of female students were $58.77{\pm}7.68%,\;15.51{\pm}4.55%\;and\;25.72{\pm}6.20%$, respectively. There was no significant difference in calcium intakes for both groups, however they are less than the RDA. In terms of iron, the male students took $16.98{\pm}5.57mg$ and the female students took $11.35{\pm}2.68mg$, with significant difference (p<0.001). The male and female students showed sufficient intake of vitamins, with significant difference between two groups except for vitamin A. The mean MAR, an index of overall dietary quality, was significantly higher in the male students than female students(p<0.01). Male and female students enjoying two meals or more a day were 59%, and those having enough time for one meal or less a day were 36.5%. Male and female students having no breakfast were 39%. Male and female students having vegetables intake were 53.5%, and having milk or milk products every day were 29.5% of them. In conclusion, nutritional education is recommended to increase the calcium intake and fruit and vegetable consumption for dietary fiber, and to emphasize regularity of meal time.

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Bandwidth Analysis of High-order Pulse for the Transmission of Ultrashort Laser Pulses (극초단펄스 전송을 위한 고차원펄스의 스펙트럼 대역 분석)

  • 전진성;조형래;오용선
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 1999.05a
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    • pp.237-242
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    • 1999
  • In this paper, we analyze transmission characteristics of ultrashort laser pulses using the property of high-order pulses which are systematically obtained following their orders. The high-order pulses are easily derived from a modified PRS system model. But we make clear they are very useful to cover wider area and more accurate transmission characteristics of ultrashort pulses than Gaussian or Sech pulse approximations used conventionally. This may be based on the fact that the spectra and bandwidths of the high-order pulses are beautifully related to their orders. first modifying the generalized PRS system model, we propose a new model for deriving any type of high-order pulse. And we offer a novel analysis method of ultrashort pulse transmission which has any shape and FWHM, using the proposed model. In addition, by fixing the pulse range $\tau$=1(ps) and varying the order of the pulse from n:1 to n=100, we obtain spectra of ultrashort pulses with 1(ps)-150(fs) FWHM's, which are widely used in fiber communications. As a one-step further, we derive PSD's of their pulse trains when they are applied to Unipolar signaling scheme. These PSD's are decided in the range of possible pulse intervals. All of these results are not only coincided with some conventional experimental works but also will be applied to any pioneering ultrashort pulse in the future.

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A Study on the Concentration Distribution of Airborne Heavy Metals in Major Industrial Complexes in Korea (국내 주요 산업단지 대기 중 중금속농도 분포에 관한 연구)

  • Kang, Byung-Wook;Kim, Min-Ji;Baek, Kyung-Min;Seo, Young-Kyo;Lee, Hak Sung;Kim, Jong-Ho;Han, Jin-Seok;Baek, Sung-Ok
    • Journal of Korean Society for Atmospheric Environment
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    • v.34 no.2
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    • pp.269-280
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    • 2018
  • This paper reports the results of field evaluation to determine the levels of heavy metals in major industrial complexes in Korea over a seven year period (2007~2013). The measurement of heavy metal was conducted using quartz fiber filter sampling and ICP-AES analysis. In order to validate the analytical performance of these methods, studies were also carried out to investigate data quality control(QC) parameters, such as the method detection limit (MDL), repeatability, and recovery efficiencies. The average concentrations of total suspended particulates (TSP) for the nine industrial complexes in Korea were $104{\sim}169{\mu}g/m^3$, which was higher than other industrial complexes and urban areas. The Sihwa and Banwol industrial complexes were shown to be the biggest contributing sources to high TSP emission ($159{\mu}g/m^3$ and $169{\mu}g/m^3$, respectively). The concentrations of heavy metals in TSP were higher in the order of Fe>Cu>Zn, Pb, Mn>Cr, Ni, As and Cd. It was observed that Fe was the highest in the Gwangyang and Pohang steel industrial complexes. The concentrations of Zn and Pb were high in Onsan, Sihwa and Banwol industrial complexes, and this was attributed to the emission from the nonferrous industry. Additionally, Cr and Ni concentrations were high in the Sihwa and Banwol industrial complexes due to plating industry. On the other hand, Ulsan and Onsan industrial complexes showed high Cr and Ni concentrations as a response to the emission of metal industry related to automobile. The correlation analysis revealed the high correlation between Cr and Ni in plating industry from Sihwa and Banwol industrial complexes. Adding to this, components related to coal combustion and road dust showed high correlation in Pohang and Gwangyang industrial complexes. Then Onsan and Ulsan industrial complexes showed high correlation among components related to the nonferrous metals.