• Proceedings of the KSME Conference
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• 2003.04a
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• pp.170-177
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• 2003

This paper proposes a robust method for the Ramberg-Osgood (R-O) fit to accurately estimate elastic-plastic J from engineering fracture mechanics analysis based on deformation plasticity. The proposal is based on engineering stress-strain data to determine the R-O parameters, instead of true stress-strain data. Moreover, for practical applications, the method is given not only for the case when full stress-strain data are available but also for the case when only yield and tensile strengths are available. Reliability of the proposed method for the R-O fit is validated against detailed 3-D Finite Element (FE) analyses for circumferential through-wall cracked pipes under global bending using five different materials, three stainless steels and two ferritic steels. Taking the FE J results based on incremental plasticity using actual stress-strain data as reference, the FE J results based on deformation plasticity using various R-O fits are compared with reference J values. Comparisons show that the proposed R-O fit provides more accurate J values for all cases, compared to existing methods for the R-O fit. Advantages of the proposed R-O fit in practical applications are discussed, together with its accuracy.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.27 no.9
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• pp.1571-1578
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• 2003

This paper proposes a robust method for the Ramberg-Osgood(R-O)fit to accurately estimate elastic-plastic J from engineering fracture mechanics analysis based on deformation plasticity. The proposal is based on engineering stress-strain data to determine the R-O parameters, instead of true stress-strain data. Moreover, for practical applications, the method is given not only for the case when full stress-strain data are available but also for the case when only yield and tensile strengths are available. Reliability of the proposed method for the R-O fit is validated against detailed 3-D Finite Element (FE) analyses for circumferential through-wall cracked pipes under global bending using five different materials, three stainless steels and two ferritic steels. Taking the FE J results based on incremental plasticity using actual stress-strain data as reference, the FE J results based on deformation plasticity using various R-O fits are compared with reference J values. Comparisons show that the proposed R-O fit provides more accurate J values for all cases, compared to existing methods for the R-O fit. Advantages of the proposed R-O fit in practical applications are discussed, together with its accuracy.

• Journal of the Korean Society for Heat Treatment
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• v.23 no.2
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• pp.90-95
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• 2010

The effects of grain size on the corrosion resistance of 429EM ferritic stainless steels for automobile exhaust system were investigated. Using specimens held at maximum service temperature of $950^{\circ}C$ for 10~70 hours, electrochemical polarization tests were conducted. While corrosion current density, $I_{corr}$, was influenced little by grain size, pitting potential, $E_p$, was increased with an increase of grain size. Sensitizaton at grain boundary occurred when the specimen were held at $950^{\circ}C$ for above 50 hours because of the dissolution of precipitates and grain coarsening.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2001.11a
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• pp.103-108
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• 2001

Wear test has been performed to evaluate the wear mechanism of Inconel alloys against ferritic stainless steels in room temperature water. By means of scanning electron microscopy (SEM), the worn surface and microstructure of subsurface layer have been examined. The wear at steady state conditions result in the formation of 5∼7${\mu}$m thick layers with fragmented microstructure. The thickness of these layers seems to depend on the ability of work hardening and deformation accommodation at the contact areas during wear. Therefore, in room temperature water, the wear rate is closely related with the wear resistance of these fragment microstructure which are generated after severe subsurface deformation.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2008.11a
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• pp.31-31
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• 2008

복합 싸이클 시험 모니터링을 통해 NaCl, $CaCl_2$ 제설염 환경에서 11 % Cr, 17 % Cr 페라이트 스테인리스강의 외면부식특성을 조사하고자 하였다. 용액 내 NaCl 및 $CaCl_2$의 농도가 증가함에 따라 용액의 pH가 떨어졌으며, $CaCl_2$의 농도증가에 따른 산성화도가 NaCl에 비해 크게 나타났다. 염수분무-건조-습윤 과정의 반복으로 구성되어 있는 복합싸이클 시험 중 소재의 표면상태 변화를 모니터링 한 결과, 건조 과정 중에 공식이 시작되며, NaCl 환경의 경우엔 습윤과정 중에 $CaCl_2$ 환경의 경우엔 건조 중에 공식성장이 주로 이루어지는 것으로 확인되었다.

• Proceedings of the Korean Nuclear Society Conference
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• 1996.05c
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• pp.79-84
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• 1996

Small punch test was performed on CF8 duplex stainless steel aged at 370 and 400$^{\circ}C$ up to 5,000 h to evaluate the degree of the thermal aging embrittlement. At room temperature, the SP load-displacement curve was in a similar shape to those of ferritic steels and had a good reproducibility in spite of two-phase structure. The aging heat treatment resulted in a slight increase of the yield strength. As test temperature was lowered, the SP load showed a sudden drop followed by serrations before the SP specimen was fractured, resulting from the cracking of ferrite phase. The extent of thermal embrittlement was assessed in terms of the SP energy. Aging treatment at higher temperature led to a larger shift in the transition temperature and the corresponding change in the fracture mode. The main cause of the degradation was the embrittlement of ferrite phase. Additionally the phase boundary separation profoundly contributed to the degradation of the specimen aged at 400$^{\circ}C$.

• Korean Journal of Materials Research
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• v.20 no.7
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• pp.356-363
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• 2010

For this paper, we investigated the area specific resistance (ASR) of commercially available ferritic stainless steels with different chemical compositions for use as solid oxide fuel cells (SOFC) interconnect. After 430h of oxidation, the STS446M alloy demonstrated excellent oxidation resistance and low ASR, of approximately 40 $m{\Omega}cm^2$, of the thermally grown oxide scale, compared to those of other stainless steels. The reason for the low ASR is that the contact resistance between the Pt paste and the oxide scale is reduced due to the plate-like shape of the $Cr_2O_3$(s). However, the acceptable ASR level is considered to be below 100 $m{\Omega}cm^2$ after 40,000 h of use. To further improve the electrical conductivity of the thermally grown oxide on stainless steels, the Co layer was deposited on the stainless steel by means of an electroless deposition method; it was then thermally oxidized to obtain the $Co_3O_4$ layer, which is a highly conductive layer. With the increase of the Co coating thickness, the ASR value decreased. For Co deposited STS444 with 2 ${\mu}m$hickness, the measured ASR at $800^{\circ}$ after 300 h oxidation is around 10 $m{\Omega}cm^2$, which is lower than that of the STS446M, which alloy has a lower ASR value than that of the non-coated STS. The reason for this improved high temperature conductivity seems to be that the Mn is efficiently diffused into the coating layer, which diffusion formed the highly conductive (Mn,Co)$_3O_4$ spinel phases and the thickness of the $Cr_2O_3$(S), which is the rate controlling layer of the electrical conductivity in the SOFC environment and is very thin

• Journal of the Korean Electrochemical Society
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• v.9 no.2
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• pp.70-76
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• 2006

Micro-droplet cell with free droplet as a micro-electrochemical technique has been limited to apply to electrochemical systems with high wetting properties such as an acidic solution and low grade stainless steels(Type 316L). By loading negative pressure to a droplet, control of droplet size, and use of hydrophobic gasket, the cell is modified to be allowed to use for electrochemical systems with high wetting properties. For giving the reliability of new cell, studies on local corrosion were conducted for three different systems-an acidic chloride solution and high chromium ferritic stainless steel, the other acidic chloride solution and type 316, and a neutral chloride solution and type 316. stainless steel. Firstly, the modified micro-droplet cell allows the anodic polarization curves in an acidic chloride solution to show the fact that the local corrosion of high chromium stainless steel near the $\alpha/\sigma$ interface is due to the Cr depleted zone. Secondly, the local anodic polarization test of type 316 L in the other acidic chloride solution can be successfully conducted in the cell. Furthermore, the local polarization curves help elucidating the corrosion of type 316 with $\delta-ferrite$ phase. Finally, the polarization curves of type 316 L in a neutral chloride solution indicates that the factor affecting the pitting corrosion resistance was inclusions rather than $\delta-ferrite$.

• Journal of the Korean Ceramic Society
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• v.42 no.12 s.283
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• pp.833-841
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• 2005

The oxidation resistance and electrical conductivity of various commercial ferritic stainless steels including STS444 were tested in an air atmosphere at $700^{\circ}C$. Crofer22 developed specially for SOFC interconnect was also examined for the aim of comparing with the test results of STS444. Although STS444 exhibited higher oxidation resistance than Corfer22, the electrical conductivity of the scale formed on Crofer22 was higher, indicating that the resistivity of scale formed on Crofer22 is much lower than that of STS444. To gain a better understanding of the relation between oxidation behavior and electrical conductivity, the oxide scales formed on STS444 and Crofer22 were analyzed in terms of the structure, composition, and phase. Consequently, the influence of alloying elements on electrical conductivity of Fe-Cr alloys was discussed.