• Title/Summary/Keyword: external standard method

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Quantitative NMR Analysis of PTMEG compounds

  • Kim, Gilhoon;Won, Hoshik
    • Journal of the Korean Magnetic Resonance Society
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    • v.20 no.1
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    • pp.7-12
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    • 2016
  • PTMEG(Polytetramethylene ether glycol) is a polymer compound widely used as a wide range of applications in the textile industry. PTMEG substance carrying various 1,800~2,000 molecular weight are mainly used as the raw material of the spandex production. Molecular weight and degree of polymerization value for 4 different PTMEG samples under pilot plant scale synthetic process were determined by a new quantitative NMR method. In NMR experiments, p-toluenesulfonic acid(TSOH) was used for external standard material of PTMEG quantitative analysis. were measuring The concentration of the primary standard TSOH was measured by UV/Vis spectroscopy. By using NMR peak assignments and the integral values of designated proton NMR peaks, We were able to measure the % composition of the synthetic PTMEG polymers, concentrations, molecular weight and the degree of polymerization that show the synthetic process of each manufacturing pilot plant. By utilizing a newly developed quantitative NMR method were able to obtain the molecular weight of PTMEG samples within 0.08 error % range.

A Basic Study on Evaluation Method and Performance of Membrane Waterproofing Layer (멤브레인 방수층 성능 및 평가방법에 관한 기초적 연구)

  • Oh, Mi-Hyun;Kwon, Shi-Won;Kang, Hyo-Jin;Jung, Hee-Won;Choi, In-Sung;Oh, Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2003.11a
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    • pp.17-21
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    • 2003
  • This study is mainly acceptive for physical material performance than waterproofing layer performance on the external condition after construction. The reason are legalized only for material performance quality standard even though it is existed waterproofing materials for membrane. In actuality, waterproofing layer are greatly occurred in performance a decreased developing essential element that are human footprints as a result physical perimeter environment after construction and on the construction. As the result, this present paper purpose for evaluation and performance of the membrane waterproofing layer on the construction.

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A Basic Study on Evaluation Method and Performance of Membrane Waterproofing Layer (멤브레인 방수층 성능 및 평가방법에 관한 기초적 연구)

  • 오미현;권시원;강효진;정희원;최인성;오상근
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2003.05a
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    • pp.17-21
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    • 2003
  • This study is mainly acceptive for physical material performance than waterproofing layer performance on the external condition after construction. The reason are legalized only for material performance duality standard even though it is existed waterproofing materials for membrane. In actuality, waterproofing layer are greatly occurred in performance a decreased developing essential element that are human footprints as a result physical perimeter environment after construction and on the construction. As the result, this present paper purpose for evaluation and performance of the membrane waterproofing layer on the construction.

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A Study on the Optimization for a V-groove GMA Welding Process Using a Dual Response Method (듀얼 반응표면법을 이용한 V-그루브 GMA 용접공정 최적화에 관한 연구)

  • Park, Hyoung-Jin;Ahn, Seung-Ho;Kang, Mun-Jin;Rhee, Se-Hun
    • Journal of Welding and Joining
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    • v.26 no.2
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    • pp.85-91
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    • 2008
  • In general, the quality of a welding process tends to vary with depending on the work environment or external disturbances. Hence, in order to achieve the desirable quality of welding, we should have the optimal welding condition that is not significantly affected by these changes in the environment or external disturbances. In this study, we used a dual response surface method in consideration of both the mean output variables and the standard deviation in order to optimize the V-groove arc welding process. The input variables for GMA welding process with the dual response surface are welding voltage, welding current and welding speed. The output variables are the welding quality function using the shape factor of bead geometry. First, we performed welding experiment on the interested area according to the central composite design. From the results obtained, we derived the regression model on the mean and standard deviation between the input and output variables of the welding process and then obtained the dual response surface. Finally, using the grid search method, we obtained the input variables that minimize the object function which led to the optimal V-groove arc welding process.

H_{\infty} Control Synthesis for Power System Design using LMI Optimization Method (LMI 최적화기법을 적용한 $H_{\infty}$제어 시스템의 전력계통 안정화장치(PSS) 설계)

  • Jeong, Dae-Won;Ju, Un-Pyo;Kim, Geon-Jung
    • The Transactions of the Korean Institute of Electrical Engineers D
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    • v.49 no.4
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    • pp.165-174
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    • 2000
  • This paper presents the application of H$\infty$ control synthesis using LMI optimization method to power system stabilizer(PSS) design. Since power system is usually operated under circumstance of unmeasurable uncertainties and external disturbances, the improvement of small signal stability becomes one of the most important issue for securing system stability and preventing low frequency oscillation phenomena. The LMI optimized H$\infty$ PSS provides robust performance and guarantees the internal stability under these operating conditions. The global optimal H$\infty$ norm is found using LMI convex optimization method which is more systematic than standard two Riccati solution method. The design results are simulated for a case study. We verified that the LMI method shows the best performance characteristic smong standard Riccati method and conventional lead/lag method.

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Determinations of Ergocalciferol and Cholecalciferol in Mushrooms (버섯의 Ergocalciferol(Vit D$_2$)과 Cholecalciferol(Vit D$_3$)의 함량 측정)

  • 이진실;안령미;최희숙
    • Korean journal of food and cookery science
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    • v.13 no.2
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    • pp.173-178
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    • 1997
  • The contents of ergocalcife.of (vit D$_2$) and cholecalciferol (vit D$_3$) in mushrooms (Lentinus edodes, Agaricus bisporus, Pleurotus ostreatus, Flammulina velutipes, Auricularia auricular, Gyropora esculenta, Romaria botftis, Coriorus versicolar, Ganoderma lucidum) were determined by high-performance liquid chromatography (HPLC), using external standard method. The methods included saponification, extraction, drying, filtering and quantification with analytical HPLC (waters Inc.). The contents of vit D$_2$ and D$_3$ found in different mushroom species. A. auricular, and L. edodes contained high amounts of vit D, 167.8, 72.6 $\mu\textrm{g}$/100 g of edible portion, respectively. On the other hand A. bisporus showed the lowest contents of vit D among analyzed mushrooms.

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Complementary measures for Environmental Performance Evaluation Index of External Space of Green Standard for Energy and Environmental Design for Apartment Complex - Focused on the Respect of Response to Climate Change - (공동주택 녹색건축인증기준의 외부공간 환경성능 평가지표 보완방안 - 기후변화 대응 측면을 중심으로 -)

  • Ye, Tae-Gon;Kim, Kwang-Hyun;Kwon, Young-Sang
    • Journal of the Architectural Institute of Korea Planning & Design
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    • v.34 no.1
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    • pp.3-14
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    • 2018
  • An apartment complex is a building use with great potential to contribute to solving problems related to urban ecological environment and climate change. The first goal of this study is to grasp the current situation of application and limitations of the ecological area rate, which is a representative evaluation index used to evaluate the environmental performance of the external space of an apartment complex in Green Standard for Energy and Environmental Design (G-SEED). The second goal is to propose a prototype of the evaluation index for evaluating greenhouse gas (GHG) reduction performance in order to supplement the evaluation index for the environmental performance of the external space in terms of response to climate change. We analyzed 43 cases of apartment complexes certified according to G-SEED, which was enforced since July 1, 2010, and found application characteristics of each space type and the limitations of ecological area rate. We analyzed overseas green building certification systems such as LEED and BREEAM that derived implications for supplementing the limitations of ecological area rate, which is focused on the evaluation of soil and water circulation function, and set up a development direction of complementary measures. Through analysis of previous studies, relevant regulations and standards, and technical documents of the manufacturer, the heat island mitigation performance of the pavement and roof surfaces of the apartment complex and the carbon uptake performance of the trees in the apartment complex was selected as parameters to yield the GHG reduction performance of the external space of the apartment complex. Finally, a quantitative evaluation method for each parameter and a prototype of the evaluation index for the GHG reduction performance were proposed. As a result of applying the prototype to an apartment complex case, the possibility of adoption and applicability as an evaluation index of G-SEED were proved.

An Introduction of Febrile Disease in Mongolian Traditional Medicine (몽골전통의학의 관점에서 본 발열성 질환에 대한 고찰)

  • Kim, Tae-Hun;Luvsannaym, B.;Kim, Jong-In;Choi, Jun-Yong;Choi, Sun-Mi
    • Journal of Acupuncture Research
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    • v.26 no.4
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    • pp.91-98
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    • 2009
  • Objectives : The objective of this review is to introduce the basic concepts on the febrile disease in the Mongolian Traditional Medicine(MTM). Methods : We comprehensively reviewed related textbooks in Mongolian and articles searched from China National Knowledge Infrastructure(CNKI) on febrile disease about MTM and summarized the pathophysiologic basis of, and treatment principles in MTM. Results and Conclusions : 1. In MTM, there are basic concepts such as theory of Arga-Bilig, theory of five elements, theory of three elements(人體三素), theory of seven constitutions and three discharges(七元三濊). Most of all, theory of three elements, which is about the basic elements of human body in MTM, is important fundamental notions for explaining human physiology and pathology. In MTM, It is explained that the imbalance of three elements, namely khii, shar, bad-kan is the root of all disease. Especially, febrile disease is treated by suppressing activated shar and blood(血液), which have fire characters, and managing various additional symptoms by balancing three elements and eliminating miasma(邪氣), inappropriate substances such as bile water(shar yc, 黃水) or blood stasis(惡血) simultaneously. 2. In MTM, both of internal treatment modalities(various medicinal therapy) and external treatment modalities(physical therapy) have been used for febrile disease. Food therapy and life style modification also have been recognized as important treatment methods. These aspects correspond to wholism theory of Korean Traditional Medicine(KTM). Further studies about details of each treatment methods will discover new applicable treatment method and make broaden the external boundaries of the KTM.

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The Case Study on the Application of the Standard Method for the Estimation of Range and Degree of Fisheries Damages Caused by Warm Water Drained by Generating Plants (발전소 온배수에 의한 어업피해범위와 정도 및 어업처분을 결정하는 표준화 방안의 적용사례분석)

  • Kang Yong-Joo;Kim Ki-Soo
    • The Journal of Fisheries Business Administration
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    • v.37 no.1 s.70
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    • pp.73-93
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    • 2006
  • This paper tries to apply the standard method for the estimation of range and degree of fisheries damages caused by warm water drained by generating plants to a real situation. The theoretic foundation of the study has been shown in the article published on the journal of fisheries business administration of last year. The paper tries to examine the degree of external appicability of the theoretic model through empirical study. The results of the study are as follows. The model has been found a successful device for the estimation of fisheries damages caused by warm water drained by generating plants. It also shows a possibility to work in any other fisheries damage cases caused by several kinds of public undertaking on coastal areas. The key of the model is the successful derivation of the quantity amount of the critical variation of environmental factors for example, in this case, water thermal variation. Therefore the countinous and appropriate collection of law data on the environmental factors under a viewpoint of statistics is essential to the usefulness of the model.

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Nondestructive Prediction of Fatty Acid Composition in Sesame Seeds by Near Infrared Reflectance Spectroscopy

  • Kim, Kwan-Su;Park, Si-Hyung;Choung, Myoung-Gun;Kim, Sun-Lim
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.51 no.spc1
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    • pp.304-309
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    • 2006
  • Near infrared reflectance spectroscopy (NIRS) was used to develop a rapid and nondestructive method for the determination of fatty acid composition in sesame (Sesamum indicum L.) seed oil. A total of ninety-three samples of intact seeds were scanned in the reflectance mode of a scanning monochromator, and reference values for fatty acid composition were measured by gas-liquid chromatography. Calibration equations were developed using modified partial least square regression with internal cross validation (n=63). The equations obtained had low standard errors of cross-validation and moderate $R^2$ (coefficient of determination in calibration). Prediction of an external validation set (n=30) showed significant correlation between reference values and NIRS estimated values based on the SEP (standard error of prediction), $r^2$ (coefficient of determination in prediction) and the ratio of standard deviation (SD) of reference data to SEP. The models developed in this study had relatively higher values (more than 2.0) of SD/SEP(C) for oleic and linoleic acid, having good correlation between reference and NIRS estimate. The results indicated that NIRS, a nondestructive screening method could be used to rapidly determine fatty acid composition in sesame seeds in the breeding programs for high quality sesame oil.