• Title/Summary/Keyword: evolution of microstructure

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Investigation of Through-thickness Microstructural Evolution in a 600 MPa-Grade Reinforced Steel Bar Manufactured by Tempcore Process (Tempcore 공정을 통해 제조된 600 MPa급 철근의 두께방향 미세구조 변화 분석)

  • Jiwon Park;Hyunji Kim;Singon Kang
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.6
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    • pp.367-373
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    • 2023
  • 600 MPa-grade deformed bar samples were manufactured by conventional hot rolling and subsequent Tempcore heat treatment processes. Considering the short-time water quenching step of the Tempcore process for hot-rolled steel, it is inevitable that the temperature profile of the deformed bar depends strongly on its position throughout the sample thickness. As a result, its microstructure can be easily divided into two regions, the surface and the core regions. The former is expected to have a fresh martensite microstructure under rapid cooling conditions, but self-tempering occurs due to the intense heat flow from the hot core region after the process. The latter is generally known to exhibit a mixed microstructure of ferrite and pearlite due to its slow cooling rate. In this study, detailed microstructural evolutions were examined through the thickness direction. The large variation of the microstructure through the thickness direction in the deformed bar samples is partly due to the easy carbon diffusion from the limited additions of alloying elements.

A Comparison of Corrosion Performance of Zirconium Grain Refined MEZ and AZ91 Alloys

  • Song, Guangling;StJohn, David
    • Corrosion Science and Technology
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    • v.2 no.1
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    • pp.30-35
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    • 2003
  • In this study, sand cast AZ91E and zirconium grain refined MEZ are representative of two typical groups of magnesium alloys: those containing aluminium and those containing no aluminium but with zirconium as a grain refiner. The corrosion performance of these two alloys was evaluated and compared in 5%wt NaCI solution through measurements of weight loss and polarisation curves and examination of microstructure. Corrosion damage of AZ91E was deeper and more localised than that of MEZ, while MEZ had a lower rate of cathodic hydrogen evolution and a higher rate of anodic dissolution than AZ91E. These differences in behaviour can be related to the differences in microstructure and chemical composition between the two alloys.

Sintering Behaviour of Al-Cu-Mg-Si Blends

  • Falticeanu, C.L;Chang, I.T.H;Kim, J.S.;Cook, R.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.278-279
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    • 2006
  • The increasing demand for automotive industries to reduce the weight of the vehicles has led to a growing usage of Al alloy powder metallurgy (P/M) parts. In order to control the sintered microstructure and mechanical properties of the aluminium alloy powder metallurgical (P/M) parts, it is essential to establish a fundamental understanding of the microstructural development during the sintering process. This paper presents a detailed study of the effect of temperature and initial starting materials on the evolution of microstructure during the sintering of Al-Cu-Mg-Si blends for PM.

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Parametric Effects of Elastic Property Extraction System of Polycrystalline Thin-Films for Micro-Electro-Mechanical System Devices (MEMS 부품을 위한 다결정 박막의 탄성 물성치 추출 시스템의 매개변수의 영향)

  • 정향남;최재환;정희택;이준기
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.50-54
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    • 2004
  • A numerical system to extract effective elastic properties of polycrystalline thin-films for MEMS devices is already developed. In this system, the statistical model based on lattice system is used for modeling the microstructure evolution simulation and the key kinetics parameters of given micrograph, grain distributions and deposition process can be extracted by inverse method proposed in the system. In this work, the effects of kinetics parameters on the extraction of effective elastic properties of polycrystalline thin-films are studied by using statistical method. The effects of the fraction of the potential site( $f_{P}$ ) and the nucleation probability( $P_{N}$ ) among the parameters for deposition process of microstructure on the extraction of effective elastic properties of polycrystalline thin-films are studied.d.d.

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Elastic Property Extraction System of Polycrystalline Thin-Films for Micro-Electro-Mechanical System Device and Its Applications (MEMS 부품을 위한 다결정 박막의 탄성 물성치 추출 시스템과 적용)

  • Jung Hyang Nam;Choi Jae Hwan;Chung Hee Taeg;Lee June Key
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.12 s.177
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    • pp.170-174
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    • 2005
  • A numerical system to extract effective elastic properties of polycrystalline thin-films for MEMS devices is developed. In this system, the statistical model based on lattice system is used for modeling the microstructure evolution simulation and the key kinetics parameters of given micrograph, grain distributions and deposition process can be extracted by inverse method proposed in the system. In this work, effects of kinetics parameters on the extraction of effective elastic properties of polycrystalline thin-films are studied by using statistical method. Effects of the fraction of the potential site($f_p$) among the parameters for deposition process of microstructure on the extraction of effective elastic properties of polycrystalline thin-films are investigated. For this research, polysilicon is applied to this system as the polycrystalline thin-films.

Effects of nanomaterials on hydration reaction, microstructure and mechanical characteristics of cementitious nanocomposites: A review

  • Kim, Gwang Mok
    • Journal of Urban Science
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    • v.9 no.1
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    • pp.7-16
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    • 2020
  • Application of nanomaterials to cementitious composites has been attempted with the rapid development of nanotechnology since the 1990s. Various nanomaterials such as carbon nanotube, graphene, nano-SiO2, nano-TiO2, nano-Al2O3, nano-Clay, and nano-Magnetite have been applied to cementitious composites to improve the mechanical properties and the durability, and to impart a variety of functionality. In-depth information on the effect of nanomaterials on the hydration reaction, the microstructure, and the mechanical properties of cementitious nanocomposites is provided in the present study. Specifically, this paper mostly deals with the previous studies on the heat evolution characteristics of cementitious nanomaterials at an early age of curing, and the pore and the compressive strength characteristics of cementitious nanocomposites. Furthermore, the effect of nanomaterials on the cementitious nanocomposites was systematically discussed with the reviews.

Sn Effects on Microstructure and Mechanical Properties of Ultrafine Ti-Fe-Sn Alloys (Sn 첨가에 따른 극미세 Ti-Fe-Sn 합금의 미세조직 및 기계적 성질 변화)

  • Han, Jun-Hee;Song, Gi-An;Pi, Dong-Hyouk;Bang, Chang-Wook;Kim, Ki-Buem
    • Journal of Korea Foundry Society
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    • v.28 no.2
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    • pp.69-73
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    • 2008
  • In the present study, microstructural evolution and mechanical properties of Ti-Fe-Sn ultrafine eutectic alloys have been investigated. Ultrafine eutectic microstructure consisting of a mixture of ${\beta}$-Ti solid solution and TiFe intermetallic compound homogeneously formed in $(Ti_{70.5}Fe_{29.5})_{100-x}Sn_x$ alloys with x = 0, 1 and 3. Addition of Sn is effective to modify the eutectic colony into the spherical shape with decreasing the lamellar spacing and colony size. This results in enhancing the macroscopic plasticity up to 3.1% of the Ti-Fe-Sn ultrafine eutectic alloys.

Coarsening Effects on the Formation of Microporous Membranes

  • Song, Seung-Won
    • Proceedings of the Membrane Society of Korea Conference
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    • 1995.04a
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    • pp.1-4
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    • 1995
  • The microstructure of polymer membranes produced via thermally induced phase separation (TIPS) of polymer solutions is a strong function of both the early-stage (by spinodal decomposition or nucleation & growth) and the late-stage phase separation (referred to in general as coarsening). In the case of early stage effects, the membrane morphology resulting from a nucleation & growth mechanism is either a poorly interconnecsed, stringy, beady structure which is mechanically fragile or a well interconnected structure with highly nonuniform pore sizes. In contrast, spinodal decomposition results in a well interconnected, mechanically strong membrane with highly uniform pore sizes. Here I describe recent quantitative studies of the coarsening effects on the microstructure of membranes produced via TIPS process. The dependence of microstructure on coarsening time, quench depth, solution viscosity, and polymer molecular weight was investigated in order to distinguish among three possible coarsening mechanisms, Ostwald ripening, coalescence, and hydrodynamic flow, which may be responsible for structural evolution after the early-stage phase Separation (spinodal decomposition or nucleation & growth).

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Mechanical and Electrical Properties of Submicrocrystalline Cu-3%Ag Alloy (초미세 결정립 Cu-3%Ag 합금의 기계적/전기적 특성)

  • Ko, Y.G.;Lee, C.W.;NamGung, S.;Lee, D.H.;Shin, D.H.
    • Transactions of Materials Processing
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    • v.18 no.6
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    • pp.476-481
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    • 2009
  • The present work demonstrates the mechanical and electrical responses of submicrocrystalline Cu-3%Ag alloy as a function of strain imposed by equal channel angular pressing(ECAP). From transmission electron microscope observation, the resulting microstructures of Cu-3%Ag alloy deformed by ECAP for 8-pass or more consist of reasonably fine, equiaxed grains without having a strong preferred orientation, suggesting that microstructure evolution is slower than that of pure-Al and its alloys owing to low stacking fault energy. The results of room temperature tension tests reveal that, as the amount of applied strain increases, the tensile strength of submicrocrystalline Cu-3%Ag alloy increases whereas losing both the ductility and the electrical conductivity. Such phenomenon can be explained based on microstructure featured by the non-equilibrium grain boundaries.

Effects of Al in TRIP steels on microstructure and phase transformation (TRIP강에서 Al이 미세구조와 상변태에 미치는 영향)

  • Lim, N.S.;Kim, S.I.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.213-216
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    • 2009
  • In this study, three cold-rolled TRIP steels containing different Al content (0.04wt%, 1.0 wt.% and 2.00wt%) were fabricated to understand the complex effects of Al in TRIP steel. The influences of Al on microstructural evolution of cold-rolled TRIP steels have been analyzed by using advanced analysis techniques, such as transmission electron microscope (TEM) and three dimensional atom probe tomography (3D-APT). TEM results revealed that second phases such as bainte and retained austenite decrease with increase of Al content. In addition, 3D-APT was used to characterize atomic-scale distribution of alloying elements at the constituent phases. Through these analysis techniques, the advanced characteristics of constituent microstructure in TRIP steels were identified depending on Al contents in TRIP steels.

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