• Title/Summary/Keyword: ethyl alcohol

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Analysis of Volatile Flavor Constituents in Green Tea Flower (녹차나무꽃의 향기성분 분석)

  • Baik, Soon Ok;Bock, Jin Young;Han, Sang Bin;Cho, Kyung Suk;Bang, Guk PiI;Kim, Il Kwang
    • Analytical Science and Technology
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    • v.9 no.4
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    • pp.331-335
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    • 1996
  • Flavor constituents of green tea flower produced in Korea were analyzed by gas chromatography and mass spectrometry. 56 compounds in sample were separated and indentified as 22 hydrocarbons, 14 alcohols, 6 aldehydes, 5 esters, and 9 others. Higher concentrated substances were heneicosyl formate, ${\alpha}$-phenyl ethyl alcohol, and acetophenone. Germacrene D as a sesquiterpene were also identified.

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Analysis of Cytotoxic Constituent of Berberis koreana Palibin (매자나무 세포독성성분 분석)

  • Kim, Young-Kyoon;Kwak, Byung-Man
    • Journal of the Korean Wood Science and Technology
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    • v.26 no.3
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    • pp.100-107
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    • 1998
  • Methanol extracts of five Berberidaceae species were examined against tissue factor inhibitory and tumour cell growth inhibitory activity. Methanol extracts of Berberis koreana Palibin showed a strong cytotoxicity activity against SK-MEL-2 (Melanoma) tumour cell lines with more than 90% in $25{\mu}g/m\ell$ and against A549 (Lung carcinoma), SK-OV-3 (Ovarian cancer), XF498 (CNS cancer) and HCTl5 (Colon cancer), other Berberidaceae species except B. koreana species have no effect on the tumour cells. Biologically active compound, therefore, was isolated through the activity guided fractionation and purification. The structure was confirmed by NMR. FT-IR and MS to 2-(3,4-dihydroxybenzyl)-ethyl alcohol. It showed cytotoxicity activity against SNU-C4 tumour cell lines with 50.7% in $50{\mu}g/m\ell$. Methanol extracts of 5 Berberidacae species have no effect on the tissue factor inhibitory activity.

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Studies on Antifatigue Activity of Crude Drug Extracts.( I ) -Ethanol Extracts of Polygonatum Officinale- (수종추출제제(數種抽出製劑)의 항피로효과(抗疲勞效果)에 관(關)한 연구(硏究) (제1보)(第1報) -Polygonatum Officinale의 Ethanol 추출제(抽出劑)-)

  • Jung, Ki-Hwa
    • Journal of Pharmaceutical Investigation
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    • v.14 no.4
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    • pp.178-182
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    • 1984
  • Extract of drugs in commerce was administered to mice for 3 days and 7 days and its antifatigue effects were compared with those of P. ginseng extract and A. sessiliflorum extract. Mice were used for these experiments divided into ethyl alcohol and water extract of R. glutinosa(saengjihwang), R. glutinosa (sookjihwang), A. japonica(changchool), A. japonica(baekchool), P. officinale, C. japonica, C. morifolium, A. calamus were given ordinary dose rally. For antifatigue test, swimming performance were determined after the extract administration. The group of P. officinale gave high improvement of the swimming performance in ethyl alcohol extract group.

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Studies on Antifatigue Activity of Crude Drug Extracts( II ) -Extracts of Poria Cocos and Sophora japonica- (수종추출체제(數種抽出製劑)의 항피로효과(抗疲勞效果)에 관(關)한 연구(硏究) (제 2 보)(第 2 報) -Poria cocos 및 Sophora japonica의 추출제(抽出劑)-)

  • Jung, Ki-Hwa
    • Journal of Pharmaceutical Investigation
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    • v.14 no.4
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    • pp.195-199
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    • 1984
  • Extract of drugs in commerce was administered to mice for 3 days and its fatigue effects were compared with those of P. ginseng extract and A. sessiliflorum extract. Mice were used for these experiments divided into ethyl alcohol and water extract of P. cocos, S. japonica, P. multiflorum, L. chinense, A. cochinchinensis, S. indicum, N. nucifera were given ordinary dose orally. For antifatigue test, swimming performance were determined after administration of the extract The group of P. cocos gave high improvement of the swimming performance in ethyl alcohol extract group. And the group of S. japonica an improvement was also observed in water extract group.

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Mandibular Nerve Block for Trigeminal Neuralgia -A case report- (삼차신경통 환자에서의 하악신경 차단 -1예 보고-)

  • Lim, Jae-Jin;Lee, Kwang-Ho;Kim, Chan
    • The Korean Journal of Pain
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    • v.6 no.2
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    • pp.247-250
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    • 1993
  • Trigeminal neuralgia(tic douloureux) is a condition characterized by excruciating paroxysms of pain in lips, gums, cheek or chin. There are many treatments of trigeminal neuralgia, such as carbamazepine, electrical stimulation, radiation therapy and ablative procedures. We blocked the mandibular nerve via lateral extra-oral route with pure ethyl alcohol in patient with localized gingival pain. The results were as follows; 1) The mandibular nerve block with pure ethyl alcohol was effective. 2) No complications were noted.

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Bleaching of Kraft Bagasse Pulp in Presence of Polyoxometalate Catalyst

  • Ibrahim A. A.;El-Sakhawy Mohamed;Kamel Samir
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.37 no.5 s.113
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    • pp.56-62
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    • 2005
  • The catalytic effect of molybdovandophosphate heteropolyanion (HPAs) on the delignification of kraft bagasse pulp by hydrogen peroxide has been investigated. Very small amounts of the catalyst (0.05 0.3 mM/l) gave convenient results. Partial reduction of the catalyst was also studied. The effect of reaction medium (water, ethyl alcohol and acetone) on the bleaching was also studied. The results obtained show that the optimum condition for bleaching in presence of polyoxometalate were 0.05 mM/l catalyst concentration at $70^{\circ}C$ reaction temperature and $7\%$ consistency at pH 2 in aqueous medium. The ratio of water to solvent of 60:40 from acetone gives higher brightness than ethyl alcohol. The catalyst solution can be reused for 5 times without any reduction in brightness. ESR for the blank and exhausted solutions under different conditions was also carried out to find the relation between reduced metals and pulp brightness.

Quantitative Analysis of Ethyl Carbamate in Korean Alcoholic Beverages by Chromatography with Mass Selective Detection (GC/MS 를 이용한 한국 주류 중의 Ethyl Carbamate 정량)

  • Park, Gyo-Beom;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.15 no.1
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    • pp.26-30
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    • 2002
  • In order to determine the contents of ethyl carbamate in Korean traditional alcoholic beverages and general beverages, GC/MS-SIM method was used after extraction of beverages with dichloromethane. The contents of ethyl carbamate in Korean traditional alcoholic beverages, non-distilled alcohol, and whisky were detected in the range of $4.6-50.2{\mu}g/L$, $27.8-45.4{\mu}g/L$, and $24.8-55.1{\mu}g/L$, respectively. The recoveries were ranged from 83.3 to 104.8 %. The values of relative standard deviation were ranged from 1.8 to 14.8 % and the detection limit was $0.3{\mu}g/L$.

Antibacterial and Antimutagenic Effects of Sweetpotato Tips Extract (고구마 끝순 추출물의 항균 및 항돌연변이 효과)

  • Lee, Joon-Seol;Shin, Mee-Jin;Park, Yang-Kyun;Ahn, Young-Sup;Chung, Mi-Nam;Kim, Hag-Sin;Kim, Jeong-Mok
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.52 no.3
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    • pp.303-310
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    • 2007
  • Sweetpotato shoot tops (leaves, tips and petioles) are known to be very useful parts as vegetables because of their high nutritive values and great biomass yield. In this study, the phenolic compound contents, antibacterial activity, mutagenic activity, and antimutagenic activity were investigated in sweetpotato tips that were 10-15cm of shoot top including stems, petioles and tender leaves after sprout of storage roots. The study was done by extracting sweetpotato tips with 80% ethanol and the ethanol fraction was re-extracted with hexane, chloroform, ethyl acetate, butanol and water. In ethyl acetate and butanol fractions, total phenolic compounds contained 95. 6mg/g extract and 69.3 mg/g extract, respectively, The antibacterial activity was measured using the paper disk method with concentrations of 1, 2, 5 and 10 mg/disk of butanol and ethyl acetate fractions against L. monocytogenes and S. Typhimurium strains. Higher doses of solvent extracts showed the higher antibacterial activities. In addition, 5, 10 and 20 mg/mL of the extracts were tested to determine the antibacterial activity in liquid culture. The sweetpotato leaf extract by ethyl acetate showed 1 log reduction compared to control after 24 hrs on Listeria monocytogenes, but 20 mg/ml of butanol extract completely inhibited the growth of the pathogen after 12 hrs. The extracts from ethyl acetate or butanol on Salmonella Typhimurium did less than 1 log reduction during cultivation compared to control. The numbers of S. Typhimirium TA98 and TA100 revertant colonies were 29-33 and 159-188 CFU/plate, respectively, indicating that solvent extracts were no mutagenic activity. The antimutagenic test was performed by adding direct mutagen 2-NF and MMS, and butanol and ethyl acetate showed antimutagenic effect. Thus, this study showed that sweetpotato tips had high phenolic contents and both antimicrobiol and antimutagenic properties. Sweetpotato tips would be good nutritive source because of their high nutrient content without any toxicity in consuming.

A study on Enhanced Efficiencies of Methane Fermented Alcohol Wastewater Treatment by Supplement of Nutrients (영양물질 주입에 의한 메탄 발효 주정폐액의 효율증진에 관한 연구)

  • 안승구;이인학;진서형
    • Journal of Environmental Health Sciences
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    • v.23 no.3
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    • pp.40-49
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    • 1997
  • In Korea, naked barley and tapioca are main raw materials for the production of fermentation ethyl alcohol, and one million drums bf 95% fermentation ethyl alcohol is produced per year by use of them. Stillage of alcoholic fermentation is mostly digested by methane fermentation process, and methane gas occured if methane fermentation process is recovered and mixed with fuel to decrease 25-30% for total fuel used in factories. In the anaerobic digestion process of naked barley stillage, supplement of nutrients is necessary to slove the problems caused by inhibitory materials contained if stillage and deficiency of nutrients. Therefore, the objective of this study was to examine why the anaerobic digesters using the naked barley distillery wastewater have shown the poor digestability frequently and how to control it. As the poor digestion was supposed to be occurred by the lack of iron as trace nutrient, the experiments were carried out to find out the optimum dosage and the way of addition of iron and to assess the quantitative evaluation of the type of iron in digesters. Initially, bottle test as batch digesters and lab-scaled continuous flow digesters were used in order to determine the digestion characteristics with tapioca and naked barley distillery wastewater. According to the results of batch tests, the poor digestion was caused by volatile fatty acids and could be improved by adding of calcium. The activity of the methanogenic bacteria were increased remarkably when the iron was added to the digester in the form of mixture with substrates.

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Purification and Properties of Extracellular Esterases of Aspergillus oryzae which synthesize Ethyl Caproate

  • Lee, Jong-Hoon;Sato, Toshitsugu;Kawai, Yuri;Enei, Hitoshi
    • Journal of Microbiology and Biotechnology
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    • v.5 no.5
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    • pp.274-279
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    • 1995
  • Ethyl caproate, one of the major flavor compounds deciding the quality of sake (Japanese wine), is produced during the brewing by the action of alcohol acyltransferase and esterases of sake yeast and koji mold. Extracellular esterases of Aspergillus oryzae required for ethyl caproate synthesis were purified partially. The enzymes had different optimum pH and affinity toward substrates. Substrate preferences and inhibition features showed the three enzymes to be B-type esterases or carboxylesterases (EC 3.1.1.1).

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