• Title/Summary/Keyword: epoxy type resin

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Study on the Effect of Resin Mixture Ratios on the Fatigue Crack Propagation Behavior and Mechanical Property in a FRMLs (수지 혼합비가 FRMLs의 피로균열전파거동과 기계적 성질에 미치는 영향에 관한 연구)

  • Kim, Cheol-Woong;Sohn, Se-Won
    • Journal of the Korean Society for Precision Engineering
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    • v.16 no.8
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    • pp.149-154
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    • 1999
  • FRMLs(Fiber Reinforced Metal Laminates) is a new type of hybrid materials. FRMLs consists of high strength metal and fiber which are laminated using a structural adhesive bond(epoxy resin). The effect of resin mixture ratios on the fatigue crack propagation behavior and mechanical property of Aramid fiber reinforced aluminum composites was investigated. The epoxy, diglycidylether of bisphenol A(DGEBA) was cured with methylene dianiline(MDA) with or without accelerator(K-54). Eight kinds of resin mixture ratio were tested for the experiment ; five kinds of FRMLs(1))epoxy & curing agent) and three kinds of FRMLs(2)(epoxy & curing agent & accelerator). FRMLs(2) have a more effective characteristics on the fatigue crack propagation behavior and mechanical property than FRMLs(1)

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A Study on the Strengths of Epoxy Resin Mortar under Heat Exposure (열을 받은 에폭시 수지 모르터의 강도에 관한 연구)

  • 연규석;강신업
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.24 no.4
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    • pp.92-98
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    • 1982
  • The major objective of this study was to investigate the heat resistance of epoxy resin mortar. For this purpose, these tests of compressive and bending strength were accomp- olished with various heating temperature (40˚C, 60˚C, 80˚C, 100˚C, 120˚C), and with various mixing ratio (1: 2, 1: 4, 1: 6, 1: 8, 1:10, 1:12, 1:14). The exprimental resin was to be Epi-Bis type epoxy resin, which is widely used as construction materials. The results obtained are summarized as follows; 1. The variations of color tone started to begin at 60˚C, and it has come out very heavy at 120˚C. It was assumed that the decrement of weight resulted from carbonization were about 0.22% at 100˚C, and about 0.34% at 120˚C. 2. The compressive and bending strength were increased with temperature rise up to 80˚C, but these were made rapid decrease when the given temperature was over. And so, the mean decrement of compressive and bending strength at 120˚C reached up to 35.5% and 26.4%, respectively. 3. The regression equation between compressive and bending strength for epoxy resin mortar under heat exposure were obtained as follows; od=0. 371oc+39. 23 (r=0. 986) And the estimated value of bending strength was corresponded to about 37 percent in comparing with that of the compressive strength. 4. Consquently, the heat resistance temperature of epoxy resin mortar was to be around 80˚C, and it was generally very low values. But it was regarded that the epoxy resin mortar will not be difficult with materials of civil engineering works and agricultural structures.

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Resistance to Chemicals and Water of Epoxy Resin Cured with Phosphazene Derivatives (포스파젠 유도체에 의해 경화된 에폭시수지의 내수.내약품성)

  • 윤흥수;최경식
    • Textile Coloration and Finishing
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    • v.13 no.3
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    • pp.188-196
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    • 2001
  • 1, 1-diamino-3, 3, 5, 5-tetrachlorocyclotriphosphazene, 1, 1-diami-no3, 3, 5, 5-tetra-(p-bromophenoxy)cyclotriphosphazene, and 1, 1-diamino-3, 3, 5, 5-tetra-(p-chlorophenoxy) cyclotri-phosphazene(ACPP) was prepared from hexachlorocyclotriphosphazene and used for the curing agent of bisphenol A type epoxy resin and phenol novolak. The resistance to chemicals and water of the cured epoxy resins were examined by DMTA and compared with those of the epoxy rosins cured with phosphazene derivatives and 4, 4'-diaminodiphenylmethane. The effect of the curing agent on resistance to chemicals and water of the cured epoxy resins were investigated. The epoxy resins cured with 1, 1-diamino-3, 3, 5, 5-tetrachlorocyclotriphosphazene and 1, 1- diamino-3, 3, 5, 5-tetra- (p-bromophenoxy)cyclotriphosphazene showed superior resistance to chemicals and water to those of 1, 1-diamino-3, 3, 5, 5-tetra- (p-chlorophenoxy)cyclotriphosphazene and 4, 4'-diaminodiphenylmethane. It is an effective curing agent for epoxy resins to enhance the resistance to chemicals, water and tome proofing.

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Cure monitoring of a composite matrix by dielectrometry (유전기법을 이용한 복합재료 기지재의 경화 모니터링)

  • 여권주;이상관;엄문광;황병선
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2001.05a
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    • pp.110-113
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    • 2001
  • Dielectrometry has been used to monitor the cure of epoxy resin using composite matrix. In this investigation, physical properties of the mixture of epoxy resin(LY564), bisphenol A type, and cycloaliphatic hardener(HY 2954) were observed. Activation energy at maximum tan $\delta$ and gelation point was determined during isothermal scanning. From IonViscosity data, it was found that vitrification peak after gelation was appeared on slow heating rate. It was also measured that the duration time for full cure was necessary and it was about 24 hr at $145^{\circ}C$. Therefore, epoxy resin used in this research is required the extended time for full cure.

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Synthesis of Aminosilane treated Waterborne Poly Urethane/Epoxy Hybrid Resin used for Loudspeaker Damper (스피커 댐퍼용 아미노실란 처리 수분산 폴리우레탄/에폭시 하이브리드 수지의 합성)

  • Choi, Hyun-Seuk;Choi, Dong-Ho;Park, Ju-Yong;Huh, Man-Woo
    • Textile Coloration and Finishing
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    • v.29 no.1
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    • pp.25-36
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    • 2017
  • This study worked on the synthesis of waterborne polyurethane/epoxy hybrid resins containing aminosilane compound to replace conventional phenol resins used for a coating material for loudspeaker dampers, which are not harmful to human being. Waterborne polyurethane resins were synthesized from two diisocyanate of 4,4'-diphenylethane diisocyanate and toluene diisocyanate, two polyols of polyester polyols(PEP), polycarbonatediol(PCD), including and anionic center of dimethylol butanoic acid, a chain extenders of ethylenediamine(EDA), and a neutral agent of triethylamine. Synthesized polyurethane resins and commercially available bisphenol A type waterborne epoxy resin were blended in weight ratios of 80:20 to prepare polyurethane/epoxy hybrid resins. The synthesized waterborne polyurethane/epoxy hybrid resins were reacted with aminosilane compound to improve mechanical properties. Aminosilane-treated polyurethane /epoxy hybrid resins showed better mechanical properties.

Rehabilitation of exterior RC beam-column connections using epoxy resin injection and galvanized steel wire mesh

  • Marthong, Comingstarful
    • Earthquakes and Structures
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    • v.16 no.3
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    • pp.253-263
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    • 2019
  • The efficacy of a galvanized steel wire mesh (GSWM) as an alternative material for the rehabilitation of RC beam-column connections damaged due to reversed cyclic loading was investigated. The repair mainly uses epoxy resin infused under pressure into the damaged zone and then confined using three types of locally available GSWM mesh. The mesh types used herein are (a) Weave type square mesh with 2mm grid opening (GWSM-1) (b) Twisted wire mesh with hexagonal opening of 15 mm (GSWM-2) and (c) welded wire mesh with square opening of 25 mm (GSWM-3). A reduced scale RC beam-column connection detailed as per ductile detailing codes of Indian Standard was considered for the experimental investigation. The rehabilitated specimens were also subjected to similar cyclic displacement. Important parameters related to seismic capacity such as strength, stiffness degradation, energy dissipation, and ductility were evaluated. The rehabilitated connections exhibited equal or better performance and hence the adopted rehabilitation strategies could be considered as satisfactory. Confinement of damaged region using GSWM-1 significantly enhanced the seismic capacity of the connections.

A Study on the Development and Physical Properties of Low Yellowing Epoxy for Ceramic Preservation (도자기 복원용 저황변 Epoxy 수지의 개발 및 물성에 대한 연구)

  • Kim, Woo Hyun;Cheong, Da Som;Bae, Jin Soo;Jee, Joo Yeon;Wi, Koang Chul
    • Journal of Conservation Science
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    • v.30 no.2
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    • pp.181-187
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    • 2014
  • AThe studies on ceramic preservation have been conducted widely in various institutions such as national/ public museums and research labs as well as the excavation institutions and university museums. Although there are some differences in preservation methodologies and materials used across the institutions, the variation is minimal. Specifically, epoxy resin is mostly used for ceramic restoration for its high cohesiveness, low contraction and high strength although there are some variations in for Ceramic Preservation. The synthetic resin type used according to the type of damage in the ceramic. However, the yellowing or the change of color across the time after the restoration is the weakness of epoxy resin. In this study, we aim to develop a material which minimizes this yellowing of epoxy resin while enhancing its cohesiveness and strength as well as other physical properties. We made the new material to have similar properties with those used widely for the ceramic restoration, such as EPO-TEK301$^{(R)}$, L30$^{(R)}$, XTR-311$^{(R)}$ through comparative experiments. The cohesiveness of the newly developed resin was improved to 2.51(MPa), which is similar level of XTR-311$^{(R)}$ of the 2.30(MPa) but about 2x higher than the other resins EPO-TEK301$^{(R)}$, L30$^{(R)}$ (1.21 and 1.81 (MPa), respectively). Especially, the experiment on yellowing shows that the existing resins show the range of color change at 10~25(${\Delta}E^*ab$), but the new low yellowing epoxy resin has the color change value at 8.3 (${\Delta}E^*ab$), the value lowering the yellowing effect to 1 to 3 times of the existing epoxy resin, thereby solving the issue of generating sense of differences due to change of color or yellowing.

Study on the Development and Properties of Ceramics Restoration Purpose Urethane resin with Excellent Reversibility (가역성이 우수한 도자기 복원용 Urethane resin의 개발 및 물성에 대한 연구)

  • Oh, Seung Jun;Park, Gi Jung;Wi, Koang Chul
    • Journal of Conservation Science
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    • v.31 no.1
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    • pp.37-46
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    • 2015
  • In the case of adhesives & restoration agents currently being used for the preservation treatment of ceramics and earthenware, epoxy type, cellulose type and cellulose type are mainly being used. However, they are showing various problems such as re-detachment from severe contraction, color change from yellowing, work inconvenience of staining on tools and hand during usage and irreversibility. For the purpose of solving the issues of yellowing and irreversibility of epoxy resin being used to restore ceramics, urethane synthetic resin with low yellowing excellent reversibility has been developed in this study. The adhesive strength of urethane resin that has been developed has excellent properties with 2.07MPa for undiluted solution, which is 1.5 times higher than that of existing material EPO-$TEK301^{(R)}$ 1.21MPa. The result of workability measurement showed that the wear rate of urethane resin (in Talc 50wt%) was 1.09%, which was somewhat higher than that of existing material Quick $Wood^{(R)}$ (1.02%). In addition, its wear rate is two times higher than that of $EPO-TEK301^{(R)}$ (0.41%) and $L30^{(R)}$ (0.39%), thereby showing an advantage in its forming process compared to existing materials. As for the advantage of urethane resin of reversibility experiment, 12 hours after acetone, ethyl alcohol deposition, urethane resin and filler talc were dissolved 100% while showing powdering phenomenon. Compared to 0% reversibility of existing epoxy resin, it has much superior reversibility. The result of UV rays experiment to evaluate its durability showed that ${\Delta}E^*ab$ color change value based on undiluted solution of urethane resin was 2.76 before & after UV rays exposure, which was a decrease by about 7-20 times compared to that of existing resin, thereby minimizing the issue of heterogeneity.

Study on the Compositional Construction of Epoxy Based Powder Paint (환경친화형 에폭시계 분체도료의 조성구축 연구)

  • Lim, Hong-Joon;Chung, Kyung-Ho
    • Clean Technology
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    • v.12 no.1
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    • pp.27-35
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    • 2006
  • Main compositions of powder paint based on thermoset type epoxy resin consist of epoxy resin for powder coating, curing agent, filler and pigment. The curing system used in this study was based on diglycidyl ether of bisphenol-A (DGEBA) and dicyan diamide (DICY). The curing behavior and rheological properties of powder coating material were investigated using DSC and rheometer, respectively. And the adhesion strength between steel and powder coating material was measured using lap shear geometry. The optimum formulation of epoxy powder paint obtained from this study was base resin of 100 phr, DICY of 6 phr, $CaCO_3$ of 20 phr, and $TiO_2$ of 10 phr.

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A Study on the Manufacturing of Screw Rotors for Air-Compressors Using RTM Process (Resin Transfer Molding을 이용한 공기 압축기용 스크류로터 제작에 관한 연구)

  • 서정도;이대길
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 1999.11a
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    • pp.139-142
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    • 1999
  • Screw rotors are core parts of screw type air compressors, compressors in refrigerating machines and super chargers of automobiles etc. They are composed of a female and a male rotors which have complex section profiles and helically swept geometry. Screw type compressors have advantages of low noise, high efficiency, less needs in maintenance etc. Usually, machining process of screw rotors requires long machining time using CNC machine designed only for screw rotors, which increase the cost of production. In this work, the screw rotors for air-compressors were manufactured with fiber reinforced epoxy composite materials by resin transfer molding process. The mold for the RTM process was made of aluminum and silicon rubber and was designed for release of helical shape products. Composite screw rotors, manufactured by RTM process, have advantages of lightweight, less cost of production, good characteristics of vibration etc.

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