• KSCE Journal of Civil and Environmental Engineering Research
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• v.29 no.2D
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• pp.209-216
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• 2009

This study was conducted to develop a thin paving technique using polymer epoxy resin materials which is considered as a durable pavement materials. The mechanical performance characteristics of the polymer epoxy resin materials were also evaluated to confirm the validity as a pavement materials. To estimate the performance properties of the materials, bending tests and bonding tests were performed using freeze-thaw and ultra-violet rays to accelerate the aging of materials. In addition, HYUNStay, a commercial structural analysis program for cable-stayed bridges, was used to compare the effect of paving materials between the polymer epoxy resin materials and the conventional ones on the reduction of cable tension and on the stability of the main tower. According to the test results, it is noted that the thin paving technique using polymer epoxy resin materials can improve the performance and durability of pavement compared to the conventional one.

• Journal of the Microelectronics and Packaging Society
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• v.8 no.4
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• pp.11-15
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• 2001

In this paper, hermetic sealing technology was studied for wafer level packaging of the RF-MEMS devices. With the flip-chip bonding method. this non-conductive B-stage epoxy sealing will be profit to the MEMS device sealing. It will be particularly profit to the RF-MEMS device sealing. B-stage epoxy can be cured by 2-step and hermetic sealing can be obtained. After defining 500 $\mu\textrm{m}$-width seal-lines on the glass cap substrate by screen printing, it was pre-baked at $90^{\circ}C$ for about 30 minutes. It was, then, aligned and bonded with device substrate followed by post-baked at $175^{\circ}C$ for about 30 minutes. By using this 2-step baking characteristic, the width and the height of the seal-line could be maintained during the sealing process. The height of the seal-line was controlled within $\pm$0.6 $\mu\textrm{m}$ in the 4 inches wafer and the bonding strength was measured to about 20MPa by pull test. The leak rate, that is sealing characteristic of the B-stage epoxy, was about $10^{-7}$ cc/sec from the leak test.

• Korean Chemical Engineering Research
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• v.43 no.3
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• pp.401-406
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• 2005

In this work, the effect of chemical treatment of multiwalled carbon nanotubes (MWNTs) on glass transition temperature (Tg), thermal stability, and dynamic viscoelastic behaviors of MWNTs-reinforced epoxy matrix composites has been studied by differencial scanning calorimeter (DSC), thermogravimetric analysis (TGA), and dynamic mechanical analysis (DMA) measurements. The MWNTs were chemically treated with 35 wt％ $H_3PO_4$ (A-MWNTs) or 35 wt％ KOH (B-MWNTs) solutions and the changes of surface properties of chemically treated MWNTs were examined by pH, acid and base values, Fourier transfer-infrared spectroscopy (FT-IR), and x-ray photoelectron spectroscopy (XPS) analyses. The chemical treatments based on acid and base reactions led to a significant change of surface characteristics and chemical compositions of the MWNTs, especially A-MWNTs/epoxy composites had higher thermal stability and dynamic viscoelastic properties than those of B-MWNTs and non-treated MWNTs/epoxy composites. These results were probably due to the improvement of interfacial bonding strength, resulting from the acid-base interaction and hydrogen bonding between the epoxy resins and the MWNT fillers.

• Steel and Composite Structures
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• v.14 no.1
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• pp.41-55
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• 2013

Fiber reinforced polymers (FRP) materials are increasingly being used for strengthening and repair of steel structures. An issue that concerns engineers in steel members which are retrofitted with FRP is stress experienced due to temperature changes. The changing temperature affects the interface bond between the FRP and Steel. This research focused on the effects of cyclical thermal loadings on the interface properties of FRP bounded to steel members. Over fifty tests were conducted to investigate the thermal effects on bonding between FRP and steel, which were cycled from temperature of $-11^{\circ}C$ ($12^{\circ}F$) to $60^{\circ}C$ ($140^{\circ}F$) for 21-36 days. This investigation consisted of two test protocols, 1) the tensile test of epoxy resin, tack coat, FRP and FRP-steel plate, 2) tensile test of each FRP compound and FRP with steel after going through thermal cyclic loading. This investigation reveals an extensive reduction in the composite's strength.

• Composites Research
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• v.28 no.1
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• pp.1-5
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• 2015

In this paper the influence of fiber orientation of basalt and carbon inter-ply fabrics on the flexural properties of hybrid composite laminates was experimentally investigated. Four types of basalt/carbon/epoxy inter-ply hybrid composite laminates with varying angle ply orientation of reinforced basalt fiber and fixed orientation of carbon fiber were fabricated using hand lay-up technique. Three point bending test was performed according to ASTM 7264. The fracture surface analysis was carried out by scanning electron microscope (SEM). The results obtained from the four laminates were compared. Lay-up pattern of $[0B/+30B/-30B/0C]_S$ exhibits the best properties in terms of flexural strength and flexural modulus. Scanning electron microscopy results on the fracture surface showed that the interfacial de-bonding between the fibers and epoxy resin is a dominant fracture mode for all fiber lay-up schemes.

• Macromolecular Research
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• v.9 no.1
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• pp.20-29
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• 2001

Interfacial adhesion and nondestructive behavior of electrodeposited (ED) carbon fiber rein-forced composites were evaluated using electro-micromechanical techniques and acoustic emission (AE). The interfacial shear strength (IFSS) of the ED carbon fiber/epoxy composites was higher than that of the untreated fiber. This might be expected because of the possibility of chemical or hydrogen bonding in an electrically adsorbed polymeric interlayer. The logarithmic electrical resistivity of the untreated single-carbon fiber composite increased suddenly to infinity when fiber fracture occurred, whereas that of the ED composite increased relatively gradually to infinity. This behavior may arise from the retarded fracture time due to enhanced IFSS. In single- and ten-carbon fiber composites, the number of AE signals coming from interlayer failure of the ED carbon fiber composite was much larger than that of the untreated composite. As the number of the each first fiber fractures increased in the ten-carbon fiber composite, the electrical resistivity increased stepwise, and the slope of the logarithmic electrical resistance increased.

• Proceedings of the Korea Concrete Institute Conference
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• 2003.05a
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• pp.531-536
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• 2003

It is generally known that RC flexural members strengthened by GFRP(Glass Fiber Reinforced Polymers) tend to be failed by premature bond failure near the flexural-shear cracks happened at the mid-span of beams. It is therefore strongly recommended that premature bond failure must be avoided to insure the intended strengthening effects sufficiently. The various methodologies such as increasing bonded length of GFRP and bonding details including U-shape wrappings and epoxy shear-keys are examined in this study. The bonded length of GFRP are calculated based on the assumed bond strengths of epoxy saturating resin. Total six half scale RC beam specimens were constructed and tested to investigate the effectiveness of each methodologies to prevent the bond failure of GFRP. Test results of each specimens are discussed in this paper.

• Transactions of the Korean Society of Automotive Engineers
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• v.1 no.3
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• pp.109-117
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• 1993

A carbon/epoxy composite drive shaft used for the power transmission of the automobiles with steel joints. Compared with the metallic drive shaft, the composite one has the weight saving of 50% with equivalent torsional strength and fatigue characteristics. In this study, the filament winding technique for the composite tube and composite/metal joining technique are estabilished. The performance test of the drive shaft is carried out. The optimal condition of the surface roughness of the steel adherend was $1.5{{\mu}m}$ to $2.5{{\mu}m}$, and the optimal condition of the bonding thickness was 0.15mm. Maximum torque and torsional stiffness of the composite drive shaft manufactured by filament winding process were found to be $210kg{\cdot}m$ and $18.5kg{\cdot}m/deg$, respectively.

• Macromolecular Research
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• v.10 no.1
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• pp.24-33
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• 2002

Interfacial and microfailure properties of carbon fiber/epoxy composites were evaluated using both tensile fragmentation and compressive Broutman tests. A monomeric and two polymeric coupling agents were applied via the electrodeposition (ED) and the dipping applications. A monomeric and a polymeric coupling agent showed significant and comparable improvements in interfacial shear strength (IFSS) compared to the untreated case under both tensile and compressive tests. Typical microfailure modes including cone-shaped fiber break, matrix cracking, and partial interlayer failure were observed under tension, whereas the diagonal slipped failure at both ends of the fractured fiber appeared under compression. Adsorption and shear displacement mechanisms at the interface were described in terms of electrical attraction and primary and secondary bonding forces.

• International Journal of Highway Engineering
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• v.16 no.4
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• pp.21-33
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• 2014

PURPOSES: The purpose of this study was to break away from the workforce method using cold-mix asphalt mixtures and has a constant quality and has develop repair materials of pre-production asphalt-precast types. METHODS: The selection of the repair material was determined as the results obtained through physical properties of materials and the field applicability. In case of repair materials, values obtained through Marshall stability test & the dynamic stability test & retained stability test as well as the site conditions was considered. In case of adhesive, test results were obtained through examination of the bond strength(tensile, shear) and the field applicability of the adhesive was examined through combined specimens to simulate field applications. RESULTS : According to the results of laboratory tests, in the case of repair materials, Marshall stability and dynamic stability, retained stability of cold-mix reaction type asphalt mixture is the highest. In the case of adhesive, two-component epoxy-urea has a very high bonding strength(tensile, shear) was most excellent. According to the results of field tests, when epoxy-urea was excellent workability. Also, the repair body through actual mock-up test did not occur large deformation and fracture after 12 months. CONCLUSIONS : A suitable repair material is cold-mix reaction type mixture of asphalt-precast, a suitable adhesive is a two-component epoxy-urea.