• Title/Summary/Keyword: encapsulation technique

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A Case Study of Paraffin Double-walled Microencapsulation Preparation Using Acrylic Polymer and Melamine Polymer for Thermal Energy Storage

  • Nguyen, Hang Vo-Minh;Kim, Chae-Hyun;Kim, Jong-Kuk
    • Journal of the Korean Solar Energy Society
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    • v.39 no.5
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    • pp.65-78
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    • 2019
  • In this study, we investigated the paraffin encapsulation using double-walled encapsulation technique. The first encapsulation used methyl methacrylic acid as the main component in acrylic polymer and the second encapsulation used melamine polymer. Particles size and distribution of the capsules were analyzed using scanning electron microscopy. In the first encapsulation, the stable capsules were obtained at 67% of phase change material ratio to methyl methacrylic acid monomer and the size of the capsule was from 0.2 to $0.3{\mu}m$. In the second encapsulation, the size of the capsules was almost the same with those capsules prepared in the first encapsulation. The particle size of single wall and double wall was about $0.3{\mu}m$. As a result of the encapsulation of paraffin using double-walled encapsulation technique, it was confirmed that the particle size was determined in the process of encapsulating using the acrylic polymer at the first wall material, and the physical and thermal stability of the capsules were imparted using melamine at the secondary wall material.

Cryopreservation of Zygotic Embryos of Herbaceous Peony (Paeonia lactiflora Pall.) by Encapsulation-Dehydration

  • Kim Hyun-Mi;Shin Jong-Hee;Sohn Jea-Keun
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.49 no.4
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    • pp.354-357
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    • 2004
  • A simplified technique which cryoprotects zygotic embryos by encapsulation-dehydration was developed for the germplasm conservation of herbaceous peony (Paeonia lactiflora Pall.). The highest survival rate $(85\%)$ was obtained from embryos treated by encapsulation-dehydration. The zygotic embryos were precultured on MS medium containing 0.3mg/L $GA_3$ for 1 day. The precultured embryos were encapsulated in $3\%$ (w/v) alginate beads and immersed for 1 h in MS medium containing 2 M glycerol and 0.5 M sucrose. The encapsulated embryos were dehydrated for 5h by air drying prior to direct immersion in liquid nitrogen. This encapsulation-dehydration method appears to be a promising technique for germplasm cryopreservation of a herbaceous peony.

Density Compatibility of Encapsulation of White Inorganic $TiO_2$ Particles Using Dispersion Polymerization Technique for Electrophoretic Display

  • Kim, Mi-Kyung;Joung, Meyoung-Ju;Kim, Chul-Am;Lee, Yong-Eui;Ahn, Seong-Deok;Kang, Seung-Roul;Suh, Kyung-Soo
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.825-827
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    • 2002
  • The polymer encapsulation of white inorganic $TiO_2$ pigment particles was prepared by a two stage dispersion polymerization technique for applications in electrophoretic displays (EPDs). In order to give functionality for inorganic pigment particles in the EPD, we have investigated the density of the polymer encapsulated $TiO_2$ particles. The average density of the polymer encapsulated $TiO_2$ particles was 2.2 at 25$^{\circ}C$. The average density of the polymer encapsulated $TiO_2$ particles is suitable to 1.7, due to density matching with suspending media. Therefore, we will attempt density compatibility of dispersion polymerization technique for encapsulation of $TiO_2$ particles in suspending media.

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Encapsulation of Semiconductor Gas Sensors with Gas Barrier Films for USN Application

  • Lee, Hyung-Kun;Yang, Woo Seok;Choi, Nak-Jin;Moon, Seung Eon
    • ETRI Journal
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    • v.34 no.5
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    • pp.713-718
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    • 2012
  • Sensor nodes in ubiquitous sensor networks require autonomous replacement of deteriorated gas sensors with reserved sensors, which has led us to develop an encapsulation technique to avoid poisoning the reserved sensors and an autonomous activation technique to replace a deteriorated sensor with a reserved sensor. Encapsulations of $In_2O_3$ nanoparticles with poly(ethylene-co-vinyl alcohol) (EVOH) or polyvinylidene difluoride (PVDF) as gas barrier layers are reported. The EVOH or PVDF films are used for an encapsulation of $In_2O_3$ as a sensing material and are effective in blocking $In_2O_3$ from contacting formaldehyde (HCHO) gas. The activation process of $In_2O_3$ by removing the EVOH through heating is effective. However, the thermal decomposition of the PVDF affects the property of the $In_2O_3$ in terms of the gas reactivity. The response of the sensor to HCHO gas after removing the EVOH is 26%, which is not significantly different with the response of 28% in a reference sample that was not treated at all. We believe that the selection of gas barrier materials for the encapsulation and activation of $In_2O_3$ should be considered because of the ill effect the byproduct of thermal decomposition has on the sensing materials and other thermal properties of the barrier materials.

Evaluation of Bacillus velezensis for Biological Control of Rhizoctonia solani in Bean by Alginate/Gelatin Encapsulation Supplemented with Nanoparticles

  • Moradi-Pour, Mojde;Saberi-Riseh, Roohallah;Esmaeilzadeh-Salestani, Keyvan;Mohammadinejad, Reza;Loit, Evelin
    • Journal of Microbiology and Biotechnology
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    • v.31 no.10
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    • pp.1373-1382
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    • 2021
  • Plant growth promoting rhizobacteria (PGPR) are a group of bacteria that can increase plant growth; but due to unfavorable environmental conditions, PGPR are biologically unstable and their survival rates in soil are limited. Therefore, the suitable application of PGPR as a plant growth stimulation is one of the significant challenges in agriculture. This study presents an intelligent formulation based on Bacillus velezensis VRU1 encapsulation enriched with nanoparticles that was able to control Rhizoctonia solani on the bean. The spherical structure of the capsule was observed based on the Scanning Electron Microscope image. Results indicated that with increasing gelatin concentration, the swelling ratio and moisture content were increased; and since the highest encapsulation efficiency and bacterial release were observed at a gelatin concentration of 1.5%, this concentration was considered in mixture with alginate for encapsulation. The application of this formulation which is based on encapsulation and nanotechnology appears to be a promising technique to deliver PGPR in soil and is more effective for plants.

A Design of ETWAD(Encapsulation and Tunneling Wormhole Attack Detection) based on Positional Information and Hop Counts on Ad-Hoc (애드 혹 네트워크에서 위치 정보와 홉 카운트 기반 ETWAD(Encapsulation and Tunneling Wormhole Attack Detection) 설계)

  • Lee, Byung-Kwan;Jeong, Eun-Hee
    • Journal of the Korea Society of Computer and Information
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    • v.17 no.11
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    • pp.73-81
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    • 2012
  • This paper proposes an ETWAD(Encapsulation and Tunneling Wormhole Attack Detection) design based on positional information and hop count on Ad-Hoc Network. The ETWAD technique is designed for generating GAK(Group Authentication Key) to ascertain the node ID and group key within Ad-hoc Network and authenticating a member of Ad-hoc Network by appending it to RREQ and RREP. In addition, A GeoWAD algorithm detecting Encapsulation and Tunneling Wormhole Attack by using a hop count about the number of Hops within RREP message and a critical value about the distance between a source node S and a destination node D is also presented in ETWAD technique. Therefore, as this paper is estimated as the average probability of Wormhole Attack detection 91%and average FPR 4.4%, it improves the reliability and probability of Wormhole Attack Detection.

IPv6 over IPv4 tunneling compatible with IPv4 Firewalls (IPv4 방화벽에 호환성을 갖는 IPv6 터널링)

  • Lee, Jung-Nam;Jang, Ju-Wook
    • The KIPS Transactions:PartC
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    • v.10C no.4
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    • pp.519-524
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    • 2003
  • During the period of co-existence of IPv4 and IPv6, Ipv6 over IPv4 tunneling technique is intended as a start-up transition mechanism. However, most of IPv4 firewalls do not support the IPv6 over IPv4 tunneling packet filtering. Finally, it is impossible that a user inside IPv4 firewall connects with an IPv6 host across IPv4 network. Without any additional hardware or changing the policy of IPv4 firewall, we solve this problem using proposed Double-encapsulation and applied-HTTP tunneling technique that are end-to-end solutions. This enables cheaper IPv6 migration solutions.

Development of New Reverse Micellar Microencapsulation Technique to Load Water-Soluble Drug into PLGA Microspheres

  • Kim Hyun Joo;Cho Mi Hyun;Sah Hong Kee
    • Archives of Pharmacal Research
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    • v.28 no.3
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    • pp.370-375
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    • 2005
  • The objective of this study was to develop a new reverse micelle-based microencapsulation technique to load tetracycline hydrochloride into PLGA microspheres. To do so, a reverse micellar system was formulated to dissolve tetracycline hydrochloride and water in ethyl formate with the aid of cetyltrimethylammonium bromide. The resultant micellar solution was used to dissolve 0.3 to 0.75 g of PLGA, and microspheres were prepared following a modified solvent quenching technique. As a control experiment, the drug was encapsulated into PLGA microspheres via a conventional methylene chloride-based emulsion procedure. The micro­spheres were then characterized with regard to drug loading efficiency, their size distribution and morphology. The reverse micellar procedure led to the formation of free-flowing, spherical microspheres with the size mode of 88 ~m. When PLGA microspheres were prepared follow­ing the conventional methylene chloride-based procedure, most of tetracycline hydrochloride leached to the aqueous external phase: A maximal loading efficiency observed our experimental conditions was below $5\%$. Their surfaces had numerous pores, while their internal architecture was honey-combed. In sharp contrast, the new reverse micellar encapsulation technique permitted the attainment of a maximal loading efficiency of 63.19 $\pm$$0.64\%$. Also, the microspheres had smooth and pore-free surfaces, and hollow cavities were absent from their internal matrices. The results of this study demonstrated that PLGA microspheres could be successfully prepared following the new reverse micellar encapsulation technique.

Preparation of Gemcitabine-Loaded Methoxy Poly(ethylene glycol)-b-Poly(L-lactide) Microparticles Using W/O/W Double Emulsion (W/O/W 다중유화법을 이용한 젬시타빈 함유 Methoxy Poly(ethylene glycol)-b-Poly(L-lactide) 미립자 제조)

  • Ryu, Jong-Hoon;Jung, In-Il;Lee, Ji-Eun;Lim, Gio-Bin
    • KSBB Journal
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    • v.26 no.4
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    • pp.333-340
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    • 2011
  • In this study, gemcitabine-loaded methoxy poly(ethylene glycol)-b-poly(L-lactide) (MPEG-PLLA) microparticles with different PEG block lengths were prepared by a W/O/W double emulsion technique. The present study focuses on the investigation of the influence of various preparative parameters such as the ratio of internal water phase and oil phase, polymer concentration, solvent composition of organic phase and salt concentration of external water phase on the morphology and encapsulation efficiency of the microparticles. The microparticles fabricated at high volume ratios of internal water phase to oil phase and at high polymer concentrations showed a relatively high encapsulation efficiency and low porosity. When a dichloromethane/ethyl acetate mixture was used as solvent, both the encapsulation efficiency and drug loading of the microparticles decreased as the level of ethyl acetate increased. The addition of a salt (NaCl) to the external water phase significantly improved the encapsulation efficiency up to 40%, and the microparticles became more spherical with their size and porosity decreased.

Zn-Ion Coated Structural $SiO_2$ Filled LDPE: Effects of Epoxy Resin Encapsulation

  • Reddy C. S.;Das C. K.;Agarwal K.;Mathur G N.
    • Macromolecular Research
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    • v.13 no.3
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    • pp.223-228
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    • 2005
  • In the present work, a low-density polyethylene (LDPE) composite, filled with Zn-ion coated structural silica encapsulated with the diglycidyl ether of bisphenol-A (DGEBA), was synthesized using the conventional melt-blending technique in a sigma internal mixer. The catalytic activity of the Zn-ions (originating from the structural silica) towards the oxirane group (diglycidyl ether of bisphenol-A (DGEBA): encapsulating agent) was assessed by infrared spectroscopy. Two composites, each with a filler content of $2.5 wt\%$ were developed. The first one was obtained by melt blending the Zn-ion coated structural silica with LDPE in a co-rotating sigma internal mixer. The second one was obtained by melt blending the same LDPE, but with DGEBA encapsulated Zn-ion coated structural silica. Epoxy resin encapsulation of the Zn-ion coated structural silica resulted in its having good interfacial adhesion and a homogeneous dispersion in the polymer matrix. Furthermore, the encapsulation of epoxy resin over the Zn-ion coated structural silica showed improvements in both the mechanical and thermal properties, viz. a $33\%$ increase in the elastic modulus and a rise in the onset degradation temperature from 355 to $371^{\circ}C$, in comparison to the Zn-ion coated structural silica.