• Title/Summary/Keyword: electrohydrodynamic

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Polycarprolactone Ultrafine Fiber Membrane Fabricated Using a Charge-reduced Electrohydrodynamic Process

  • Kim, Geun-Hyung;Yoon, Hyeon;Lee, Haeng-Nam;Park, Gil-Moon;Koh, Young-Ho
    • Macromolecular Research
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    • v.17 no.7
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    • pp.533-537
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    • 2009
  • This paper introduces a modified electro spinning system for biomedical wound-healing applications. The conventional electrospinning process requires a grounded electrode on which highly charged electro spun ultrafine fibers are deposited. Biomedical wound-healing membranes, however, require a very low charge and a low level of remnant solvent on the electrospun membrane, which the conventional process cannot provide. An electrohydrodynamic process complemented with field-controllable electrodes (an auxiliary electrode and guiding electrodes) and an air blowing system was used to produce a membrane, with a considerably reduced charge and low remnant solvent concentration compared to one fabricated using the conventional method. The membrane had a small average pore size (102 nm) and high porosity (85.1%) for prevention of bacterial contamination. In vivo tests on rats showed that these directly electro spun fibrous membranes produced using the modified electro spinning process supported the good healing of skin bums.

An Experimental Study on Electrohydrodynamic Atomization of Non-Conducting Liquid (비전도성 액체의 전기수력학적 분무에 관한 실험적 연구)

  • Lee, Ki-Joon;Park, Jong-Seung;Lee, Sang-Yong
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.1322-1327
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    • 2004
  • In the present work, a series of experiments have been performed on electro-hydrodynamic atomization of non-conducting liquid using a charge injection type nozzle. Effects of liquid flow rate, input voltage, and distance between the needle and the ground electrode (nozzle-embedded metal plate) have been examined. For fixed electrode distances, total and spray currents increase with increase of liquid flow rate and input voltage. When the distance between the needle and the ground electrode becomes closer, total, leakage and spray current increase, but the onset voltage for dielectric breakdown decreases. When the electric field strength of the liquid jet exceeds that for the air breakdown, a portion of the electric charges in the liquid jet is dissipated into the ambient air, and the charge density shows a limiting value. Atomization quality can be improved by increasing the flow rate because the higher charge density is achieved with the larger liquid velocity in addition to the enhanced aerodynamic effect.

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An Experimental Study on the Effect of Electrohydrodynamic Monodisperse Atomization According to Nozzle Characteristics (노즐 특성에 따른 전기수력학적 단분산 미립화 효과에 관한 실험적 연구)

  • Sung, K.A.;Lee, C.S.
    • Journal of ILASS-Korea
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    • v.10 no.2
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    • pp.18-31
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    • 2005
  • This study was performed to explore the liquid breakup and atomization characteristics for the classification of drop formation mode and background of uniform droplets generation in electrohydrodynmaic atomization according to the change of experimental parameters such as nozzle material (stainless steel. teflon). fluid flow rate, applied electrical field and intensity, and frequency. In results, from the classification map of drop formation modes according to the variation of applied AC voltage and frequency at a stainless nozzle, the droplet size was smaller than the outer diameter of the nozzle tip relatively in the spindle mode. The transition points became clearly to be moved toward the high applied voltage by rising the applied AC frequency beyond 450Hz. Also the droplet radius can be observed quite small in the frequency bandwidth of $350{\sim}450Hz$. The droplet radiuses decrease as the applied voltage increases for a fixed applied AC frequency within the range from 50Hz to 400Hz Over 400Hz, the relation between the power intensity and the droplet size was not consistent with a continuous mechanism of liquid breakup. Thus, it is showed that the droplet size distribution using the teflon nozzle was analogous to the results of stainless steel, but the droplet size was bigger than that of stainless steel relatively in case of a teflon nozzle.

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An Experimental Study on Charge Injection to Non-Conducting Liquid for Electrohydrodynamic Atomization (비전도성 액체의 전기수력학적 미립화를 위한 전하 주입 특성에 관한 실험적 연구)

  • Lee, Ki-Joon;Park, Jong-Seung;Lee, Sang-Yong
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.28 no.11
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    • pp.1376-1383
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    • 2004
  • In the present work, a series of experiments have been performed on electro-hydrodynamic atomization of non-conducting liquid using a charge injection type nozzle. Effects of liquid flow rate, input voltage, and distance between the needle and the ground electrode (nozzle-embedded metal plate) have been examined. For fixed electrode distances, total and spray currents increase with the increase of liquid flow rate and input voltage. When the distance between the needle tip and the ground electrode becomes closer, the total, leakage and spray currents increase, while the onset voltage for the dielectric breakdown decreases. When the electric field strength of the liquid jet exceeds that for the air breakdown, a portion of the electric charges in the liquid jet is dissipated into the ambient air, and the charge density shows a limiting value. Atomization quality can be improved by increasing the liquid flow rate due to the higher charge density and the enhanced aerodynamic effect.

A Study on Micro-Electrode Pattern of Repair Process Using Electrohydrodynamic Printing System (전기수력학 프린팅 기술을 이용한 미세전극 패턴의 리페어 공정 적용에 관한 연구)

  • Yang, Young-Jin;Kim, Soo-Wan;Kim, Hyun-Bum;Yang, Hyung-Chan;Lim, Jong-Hwan;Choi, Kyung-Hyun
    • Clean Technology
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    • v.22 no.4
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    • pp.232-240
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    • 2016
  • Recently, various research studies have been conducted and many are in progress for the suitable alternative materials for ITO based touch screen panel (TSP) due to limitations in size and flexibility. Various researches from all over the world have been attempted to fabricate the fine electrode less than $5{\mu}m$ for the rapid developing of display technology. Research is also being carried out in metal mesh methods using the existing technologies and alternative materials at commercial level. However, by using the existing technologies certain discrepancies are observed like low transparency and low yield which also results in the distortion of patterns. For repairing the damaged pattern, the conventional laser CVD technique has also been used but there are some challenges observed in CVD technique like achieving a stable fine electrode of $10{\mu}m$ or less and avoiding the formation of satellite drops. To overcome these issues, a new printing process named Electrohydrodynamic (EHD) printing, has been introduced by which $5{\mu}m$ fine patterns can be printed in one step. This EHDA printing technique has been applied to print very fine electrodes of $5{\mu}m$ or less by using conductive inks of various viscosities. This study also presents the optimized process parameters for printing $5{\mu}m$ fine electrode patterns during experiments by controlling the applied voltage and supply flow rate. The $5{\mu}m$ repair electrodes were fabricated for repairing $50{\mu}m$ shorted electrode samples.

Electrohydrodynamic Process Supplemented by Multiple-Nozzle and Auxiliary Electrodes for Fabricating PCL Nanofibers (멀티노즐/보조전극-Electrohydrodynamic 공정을 통한 PCL 나노파이버 제작)

  • Yoon, Hyeon;Kim, Geun-Hyung;Kim, Wan-Doo
    • Polymer(Korea)
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    • v.32 no.4
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    • pp.334-339
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    • 2008
  • Recently electro spinning is a widely used simple technique to prepared micro- to nanometer-sized fiber of various polymers. In general, a normal multiple-nozzle electro spinning system has been difficult to achieve high production-rate fabricating micro/nanofibers due to the interference of electric field between individual nozzles in the process. To reduce the interference effect of electric field between nozzles, we developed a multi-nozzle electrospinning system supplemented with auxiliary electrodes. Poly($\varepsilon$-carprolactone)(PCL), which has good mechanical property and biocompatibility, was electrospun by the multi-nozzle electro spinning system. Electrospinnability, product rate, and size uniformity of spun fibers for the system with and without auxiliary electrodes were characterized. As a result, the multi-nozzle electrospinning system supplemented with auxiliary electrodes provides excellently stable processability and showed high mass productivity of PCL-nanofibers relative to a normal multi-nozzle electro spinning system.

A Study on the Organic-Inorganic Multilayer Barrier Thin Films Using R2R Low-Temperature Atmospheric-Pressure Atomic Layer Deposition System (연속공정기반 저온 상압 원자층 증착 시스템을 이용한 유무기 멀티레이어 배리어 박막에 관한 연구)

  • Lee, Jae-Wook;Kim, Hyun-Bum;Choi, Kyung-Hyun
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.3
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    • pp.51-58
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    • 2018
  • In this paper, the organic material Poly(methyl methacrylate) PMMA is used with inorganic $Al_2O_3$ to fabricate organic-inorganic multilayer barrier thin films. The organic thin films are developed using a roll-to-roll electrohydrodynamic atomization system, whereas the inorganic are grown using a roll-to-roll low-temperature atmospheric pressure atomic layer deposition system. For the first time, these two technologies are used together to develop organic-inorganic multilayer barrier thin films in atmospheric condition. The films are grown under optimized parameters and classified into three classes based on the layer structures, when the total thickness of the barrier is maintained at ~ 160 nm. All classes of barriers show good morphological, optical and chemical properties. The $Al_2O_3$ films with a low average arithmetic roughness of 1.58 nm conceal the non-uniformity and irregularities in PMMA thin films with a roughness of 5.20 nm. All classes of barriers show a notably good optical transmission of ~ 85 %. The hybrid organic-inorganic barriers show water vapor and oxygen permeation in the range of ${\sim}3.2{\times}10^{-2}g/m^2/day$ and $0.015cc/m^2/day$ at $23^{\circ}C$ and 100% relative humidity. It has been confirmed that it can be mass-produced and used as a low-cost barrier thin film in various printing electronic devices.

Drug Delivery System Using Electrospun Nanofiber Mats (전기방사된 나노파이버 매트를 이용한 약물전달시스템에 관한 연구)

  • Yoon, Hyeon;Park, Yoon-Kyung;Kim, Geun-Hyung
    • Polymer(Korea)
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    • v.33 no.3
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    • pp.219-223
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    • 2009
  • The nanofibers fabricated by using an electrohydrodynamic process has been used as various applications, such as nano-device, filtering system, protective clothes, wound dressing, and drug delivery system (DDS). Of these applications, the DDS should be needed to minimize side effects of drugs, maximize the properties of medicine, and efficiently deliver the required amount of drugs to the diseased area. In this paper, by using the electro spinning process, which is one of electrohydrodynamic processes, two different types, polycarprolactone and poly(ethylene oxide)/Rhodamine B, of electrospun mats were fabricated layer by layer and the release behavior of Rhodamine B was characterized with time. In addition, to show the feasibility of DDS of this type, we tested release behavior of a peptide of the nanofiber system, a PCL/(Peptide+PEO)/PCL nanofiber mat. The released peptide did not loss biological activities. From these results, we believe that the layered nanofiber mat as a DDS has enough function of a new drug delivery system.

The growth effect of agglomerated and nonagglomerated particles in Condensation Nuclei Counter (CNC) (응집입자와 비응집 입자의 CNC 내에서 응축성장에 관한 실험적 연구)

  • Kim, Y.W.;Moon, H.W.;Yoon, J.U.;Ahn, K.H.
    • Proceedings of the KSME Conference
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    • 2001.06d
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    • pp.579-584
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    • 2001
  • Agglomerated and nonagglomerated SiO2 particles are synthesized in furnace by the electrohydrodynamic spraying method and the vapor feeding method for the test particle generator this study. These polydispersed particles are classified with DMA to extract equal mobility particles. Then these particles are introduced into CNC (Condensation Nuclei Counter) to see the pulse height using Multi-channel Analyzer. The response characteristics of these two kinds of particles in CNCs (TSI CNC 3022 and 3025A) have been studied as a function of particle size using mono disperse particles classified by DMA. The results show that the higher drag resistance particles, so called agglomerated particles have generated a lower CNC pulse height than the spherical particles for these two different CNCs, which means the nonagglomerated particles may start to grow larger than the agglomerated particles.

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