• Title/Summary/Keyword: electrode sensor

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Electrochemical Determination of Epinephrine Using Doubly Modified Electrodes with Ni(II)-Macrocyclic Complex and Polyuretane (니켈(II)-거대고리 착물과 폴리 우레탄으로 변성한 이중 전극에서 에피네피린의 전기화학적 정량)

  • Xu, Guang-Ri;Cho, Hyung-Hwa;Kweon, Soo-Geong;Lee, Sang-Hag;Bae, Zun-Ung
    • Journal of the Korean Electrochemical Society
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    • v.10 no.3
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    • pp.190-195
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    • 2007
  • A new electrochemical sensor to selectively determine epinephrine was developed and its analytical characteristics has been investigated. A glassy carbon electrode was modified with Ni(II)-macrocyclic complex which has electrocatalytic effect. It was further modified with physiologically suitable and negatively charged polyuretane benzyl L-glutamate(PUBLG). The present electrode showed long term stability and it could be applied to the selective determination of epinephrine in urine sample with various coexisting compounds. Under the optimum experimental conditions the linear range was $8.0\;{\times}\;10^{-7}\;-\;2.0\;{\times}\;10^{-4}\;M$ and the limit of detection was $1.0\;{\times}\;10^{-7}\;M$. The recovery of epinephrine in urine sample diluted 5 times with buffer solution was $101.5({\pm}3.2)%$ for 6 measurements.

Electrical and Optical Properties of Asymmetric Dielectric/Metal/Dielectric (D/M/D) Multilayer Electrode Prepared by Radio-Frequency Sputtering for Solar Cells

  • Pandey, Rina;Lim, Ju Won;Lim, Keun Yong;Hwang, Do Kyung;Choi, Won Kook
    • Journal of Sensor Science and Technology
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    • v.24 no.1
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    • pp.15-21
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    • 2015
  • Transparent and conductive multilayer thin films consisting of three alternating layers FZTO/Ag/$WO_3$ have been fabricated by radio-frequency (RF) sputtering for the applications as transparent conducting oxides and the structural and optical properties of the resulting films were carefully studied. The single layer fluorine doped zinc tin oxide (FZTO) and tungsten oxide ($WO_3$) films grown at room temperature are found to have an amorphous structure. Multilayer structured electrode with a few nm Ag layer embedded in FZTO/Ag/$WO_3$ (FAW) was fabricated and showed the optical transmittance of 87.60 % in the visible range (${\lambda}=380{\sim}770nm$), quite low electrical resistivity of ${\sim}10^{-5}{\Omega}cm$ and the corresponding figure of merit ($T^{10}/R_s$) is equivalent to $3.0{\times}10^{-2}{\Omega}^{-1}$. The resultant power conversion efficiency of 2.50% of the multilayer based OPV is lower than that of the reference commercial ITO. Asymmetric D/M/D multilayer is a promising transparent conducting electrode material due to its low resistivity, high transmittance, low temperature deposition and low cost components.

Development of the Novel Intraoperative Neuromonitoring for Thyroid Surgery (갑상선 수술을 위한 새로운 수술 중 신경감시시스템의 개발)

  • Sung, Eui Suk;Lee, Byung Joo
    • International journal of thyroidology
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    • v.11 no.2
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    • pp.109-116
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    • 2018
  • It is very important to identify recurrent laryngeal nerve (RLN) and prevent RLN injury during thyroid surgery. The intraoperative neuromonitoring (IONM) for the prevention of RLN injury is a useful method because it can identify the location and status of RLN and predict postoperative vocal cord function easily. The IONM consists of a stimulating side that applies electrical stimulation to the nerve and a recording side that measures the surface electromyography (EMG) of the vocal cord muscle through electrode endotracheal tube. The nerve stimulator and surgical dissector are separate instruments. So, during IONM for the prevention of the RLN injury in conventional, endoscopic, or robotic thyroid surgery, repeated exchanging between surgical instruments and the nerve stimulator is inconvenient and time consuming. On the recording side, the accuracy of the electrode endotracheal tube which measures the EMG of the vocalis muscle can be affected by contact with between electrode and vocal fold and position change of patient. We would like to introduce recent several researches to overcome the current limitations of IONM.

Electrode Fabrication of MWCNT-PDMS Strain Sensors by Wet-etching (습식 식각을 이용한 MWCNT-PMDS 변형율 센서 전극 생성에 관한 연구)

  • Jung, La-Hee;Hwang, Hui-Yun
    • Composites Research
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    • v.34 no.6
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    • pp.387-393
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    • 2021
  • This paper investigated the electrical properties of multiwall carbon nanotube reinforced polydimethylsiloxane (CNT-PDMS) strain sensors with copper electrodes on the wet-etched surface. MWCNT-PDMS strain sensors were fabricated according to the wt% of MWCNT. Surfaces on the electrode area were wet-etched with various etching duration and silver epoxy adhesives were spread on the wet-etched surface. Finally, we attached the copper electrodes to the MWCNT-PMDS strain sensors. We checked the electric conductivities by the two-probe method and sensing characteristics under the cyclic loading. We observed the electric conductivity of MWCNT-PDMS strain sensors increased sharply and the scattering of the measured data decreased when the surface of the electrode area was wet-etched. Initial resistances of MWCNT-PDMS strain sensors were inversely proportion to wt% of MWCNT and the etching duration. However, the resistance changing rates under 30% strain increased as wt% of MWCNT and the etching duration increased. Decreasing rate of the electric resistance change after 100 repetitions was smaller when wt% of MWCNT was larger and the etching duration was short. This was due to the low initial resistance of the MWCNT-PMDS strain sensors by the wet-etching.

Performance and Stability Evaluation of Muscle Activation (EMG) Measurement Electrodes According to Layer Design (근활성도(EMG) 측정 전극 레이어 설계에 따른 성능 및 안정성 평가)

  • Bon-Hak Koo;Dong-Hee Lee;Joo-Yong Kim
    • Science of Emotion and Sensibility
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    • v.26 no.4
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    • pp.41-50
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    • 2023
  • This study aims to develop electromyography (EMG) textile electrodes and assess their performance and signal stability by examining variations in layer count and fabric types. We fabricated the electrodes through layering and pressing techniques, focusing on configurations with different layer counts (Layer-0, Layer-1, and Layer-2). Our findings indicate that layer presence significantly influences muscle activation measurements, with enhanced performance correlated with increased layer numbers. Subsequently, we created electrodes from five distinct fabrics (neoprene, spandex cushion, 100% polyester, nylon spandex, and cotton canvas), each maintaining a Layer-2 structure. In performance tests, nylon spandex fabric, particularly heavier variants, outperformed others, while the spandex cushion electrodes showed superior stability in muscle activation signal acquisition. This research elucidates the connection between electrode performance and factors like layer number and electrode-skin contact area. It suggests a novel approach to electrode design, focusing on layer properties and targeted pressure application on specific sensor areas, rather than uniformly increasing sleeve pressure.

Fabrication of Gold Nanostructures Using Electrochemical Deposition Integrated with Solution Process (용액 공정을 접목한 전기화학 증착 기법을 활용한 금 나노 구조체 제작)

  • Jihee Kim;Donghyeon Kim;Mijeong Kang
    • Journal of the Korean Electrochemical Society
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    • v.27 no.3
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    • pp.81-87
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    • 2024
  • Nanomaterial electrodes are used to improve the analytical performances of electrochemical measurements in biological and chemical field. Frequently used methods for fabricating metal nanostructures are solution processing and electrodeposition. In the solution process, it is possible to control the characteristics (e.g., direction) of metal growth by using capping agents, thereby fabricating nanoparticles of specific structures. In the electrodeposition, the electrode surface and the deposited metal atoms are in direct contact. Each process has its own limitation as well, and many studies are conducted to overcome such limitation. In this paper, we report an integration of the two fabrication methods and the characteristics, such as structural and electrochemical properties, of the fabricated electrodes. Lastly, we discuss the possibility of using the fabricated nanostructured electrode as a sensor.

Gas Typed Digital X-ray Image Sensor Using PDP Fabrication Process (PDP공정을 이용한 가스 방식의 디지털 X-ray 영상 센서)

  • Kim, Chang Man;Kim, Si Hyung;Nam, Ki Chang;Kim, Sang Hee;Song, Kwang Soup
    • Journal of the Institute of Electronics and Information Engineers
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    • v.49 no.9
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    • pp.322-327
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    • 2012
  • Parallel-plate-type scanning sensors have been commercially used for X-ray imaging sensors. In this study, we manufactured the scan typed 1D X-ray image sensor that can be used to obtain scanning images, by using the plasma display panel (PDP) fabrication process. We fabricated drift and pixel electrodes in the glass chamber and injected Xe gas at atmospheric pressure. We evaluated the intensity of a pixel signal depending on the bias voltage on the drift electrode and investigated the characteristics of shielding effect on the single pixel using lead (Pb). The adsorption rate of X-ray photon is low (4%) on the soda lime glass (1.1mm) and the electrical signal detected on the X-ray sensor was increased in the high bias voltage. We acquired digital X-ray scanning image with our DAS (data acquisition system) and sensor scanning system.

Synthesis of Mesoporous Tin Oxide and Its Application as a Gas Sensor (메조세공을 갖는 이산화 주석의 합성 및 가스센서로서의 응용)

  • Kim, Nam-Hyon;Kim, Geon-Joong
    • Applied Chemistry for Engineering
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    • v.18 no.2
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    • pp.142-147
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    • 2007
  • In this study, mesoporous tin oxide was synthesized by sol-gel method using $C_{16}TMABr$ surfactant as a template in a basic condition. The optimum conditions for the synthesis of mesoporous $SnO_2$ were investigated and the obtained samples were characterized by XRD, nitrogen adsorption and TEM analysis. A mesoporous and nanostructured $SnO_2$ gas sensor with Au electrode and Pt heater has been fabricated on alumina substrate as one unit via a screen printing process. Sensing abilities of fabricated sensors were examined for CO and $CH_4$ gases, respectively, at $350^{\circ}C$ in the concentration range of 1~10,000 ppm. Influence of loading amount of palladium impregnated on $SnO_2$ was also tested in detection of those gases. High sensitivity to detecting gases and the fast response speed with stability were obtained with the mesoporous tin oxide sensor as compared to a non-porous one under the same detection conditions.

Investigation of Impact Detection Characteristics of Piezoelectric Paint According to Boundary Conditions (구조물의 경계조건에 따른 압전 페인트 센서의 충격검출 특성 평가)

  • Park, Seung-Bok;Han, Dae-Hyun;Kang, Lae-Hyong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.38 no.12
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    • pp.1335-1343
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    • 2014
  • Piezoelectric paint can be used to monitor vibrations or impacts occurring in large engineering structures such as ships and airplanes. This study investigated the impact detection characteristics of a piezoelectric paint sensor and possible errors in detecting impacts according to boundary conditions. The piezoelectric paint sensor used in this study was coated on an aluminum plate with four different electrode areas. After the occurrence of the poling process, the output voltages from the paint sensors were obtained when impact occurred in a certain sensor region. The experimental results revealed a large difference in magnitudes between the sensor signal in the impact region and those in the other regions, and this relation was maintained regardless of the changes in the boundary conditions.

Humidity-Sensitive Characteristics and Reliabilities of Polymeric Humidity Sensors Using 2-Methacryloxyethyl dimethyl 2-hydroxyethyl ammonium brornide (2-Methacryloxyethyl dimethyl 2-hydroxyethyl ammonium bromide를 이용한 고분자 습도센서의 감습 특성 및 신뢰성)

  • Lee, Chil-Won;Gong, Myoung-Seon
    • Applied Chemistry for Engineering
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    • v.10 no.3
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    • pp.461-466
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    • 1999
  • The humidity sensor containing ammonium salt was prepared from the copolymer of 2-methacryloxyethyl dimethyl 2-hydroxyethyl ammonium bromide (MDHAB)/MMA/DAEMA = 6/3/1. The humid membrane was fabricated on the gold/alumina electrode by dipping. The impedances were $298k{\Omega},\;11k{\Omega}$, and $2.3k{\Omega}$ at 40%RH, 70%RH and 90%RH, respectively, at $5^{\circ}C$ and the humidity-sensitive characteristics were suitable for low temperature humidity sensor. The temperature-dependent coefficient between $5^{\circ}C$ and $20^{\circ}C$ was found to be $-0.80%RH/^{\circ}C$ and the hysteresis falled in the ${\pm}2%RH$ range. The response time was found to be 38 sec for the relative humidity ranging from 34%RH to 88%RH at $20^{\circ}C$. The reliabilities such as temperature cycle, humidity cycle, high temperature and humidity resistance, electrical load stability, stability of long-term storage and water durability were measured and evaluated for the application as a humidity sensor.

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