• 한국세라믹학회지
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• 제48권6호
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• pp.630-635
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• 2011

Bismuth vanadate($BiVO_4$) with monoclinic phase as photocatalyst under visible light is synthesized by precipitation reaction in hot water. Properties such as crystal phase, particle morphology and visual light absorbance as well as the effects of thermal treatment for $BiVO_4$ powders are investigated. $BiVO_4$ powders with both single monoclinic phase and 0.2 ${\mu}m$ in particle size are synthesized when precipitate is stirred in water for 5 h at 95$^{\circ}C$. Well-developed monoclinic phase and light absorption property under 535 nm are observed as a result of thermal treatment for 1 h at 300$^{\circ}C$ after precipitation reaction in water for 5 h at 95$^{\circ}C$. Degradation of monoclinic crystal is found in firing above 350$^{\circ}C$, and particle growth is occurred in firing above 550$^{\circ}C$.

• 한국전산유체공학회:학술대회논문집
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• 한국전산유체공학회 2008년도 춘계학술대회논문집
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• pp.538-541
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• 2008

The carbon laden suspensions in water with no surfactants have poor stability caused by the hydrophobic layer of particles. In this study, the water-based carbon nano colloide(CNC) was successfully produced using electro-chemical one-step method without agent. The properties of CNC were characterized by using various techniques such as particle size analyzer, TEM, FT-IR, turbidity meter, viscometer, and transient hot-wire method. The average size of the suspended in the CNC was 15 nm in diameter. The thermal conductivity of CNC compared with water was increased up to 14% with 4.2wt% concentration. The CNC was stable over 600hr. The enhanced colloidal stability of CNC may be caused by the chemical structures, such as, hydroxide and carboxyl groups formed in outer atomic layer of carbon, which (i) made the carbon nanofparticles hydrophilic and (ii) prevented the aggregation among nanoparticles.

• Structural Engineering and Mechanics
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• 제58권5호
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• pp.931-947
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• 2016

The effects of nanotechnology and smartness on the buckling reduction of pipes are the main contributions of present work. For this ends, the pipe is simulated with classical piezoelectric polymeric cylindrical shell reinforced by armchair double walled boron nitride nanotubes (DWBNNTs), The structure is subjected to combined electro-thermo-mechanical loads. The surrounding elastic foundation is modeled with a novel model namely as orthotropic nonhomogeneous Pasternak medium. Using representative volume element (RVE) based on micromechanical modeling, mechanical, electrical and thermal characteristics of the equivalent composite are determined. Employing nonlinear strains-displacements and stress-strain relations as well as the charge equation for coupling of electrical and mechanical fields, the governing equations are derived based on Hamilton's principal. Based on differential quadrature method (DQM), the buckling load of pipe is calculated. The influences of electrical and thermal loads, geometrical parameters of shell, elastic foundation, orientation angle and volume percent of DWBNNTs in polymer are investigated on the buckling of pipe. Results showed that the generated ${\Phi}$ improved sensor and actuator applications in several process industries, because it increases the stability of structure. Furthermore, using nanotechnology in reinforcing the pipe, the buckling load of structure increases.

• Macromolecular Research
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• 제16권7호
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• pp.626-630
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• 2008

Poly(vinyl pyrrolidone) was used successfully to control the size and distribution of silver nanoparticles generated on inorganic silica nanofibers. The inorganic nanofibers were electro spun using sol-gel chemistry of silicates, and the diameter of the prepared nanofibers was unaffected by adding up to 7% of poly(vinyl pyrrolidone). The silver ions, in the form of silver nitrate, were introduced into the silica nanofibers and reduced to metallic silver by ultraviolet irradiation with a subsequent thermal treatment. The size of the generated silver particles was decreased dramatically by adding poly(vinyl pyrrolidone). The size of the silver nanoparticles was 73 nm when no poly(vinyl pyrrolidone) was added but 23 nm with the addition of only 1% of poly(vinyl pyrrolidone). The extent of reduction could be checked by determining the concentration of silver ions leached into water from the silica nanofibers. After thermal treatment of the silica nanofibers, more than 99% of the silver remained in the nanofibers, indicating almost complete reduction of the silver ions to silver metal.

• 한국세라믹학회지
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• 제45권4호
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• pp.191-195
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• 2008

Highly ordered silver nanowire with a diameter of 10 nm was arrayed by electroless deposition in a porous anodic aluminum oxide(AAO) membrane. The AAO membrane was fabricated electrochemically in an oxalic acid solution via a two-step anodization process, while growth of the silver nanowire was initiated by using electroless deposition at the long-range-ordered nanochannels of the AAO membrane followed by thermal reduction of a silver nitrate aqueous solution by increasing the temperature up to $350^{\circ}C$ for an hour. An additional electro-chemical procedure was applied after the two-step anodization to control the pore size and channel density of AAO, which enabled us to fabricate highly-ordered silver nanowire on a large scale. Electroless deposition of silver nitrate aqueous solution into the AAO membrane and thermal reduction of silver nanowires was performed by increasing the temperature up to $350^{\circ}C$ for 1 h. The morphologies of silver nanowires arrayed in the AAO membrane were investigated using SEM. The chemical composition and crystalline structure were confirmed by XRD and EDX. The electroless-deposited silver nanowires in AAO revealed a well-crystallized self-ordered array with a width of 10 nm.

• International Journal of Automotive Technology
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• 제7권3호
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• pp.329-336
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• 2006

The resistance spot-welded region in most current finite element crash models is characterized as a rigid beam at the location of the welded spot. The region is modeled to fail with a failure criterion which is a function of the axial and shear load at the rigid beam. The calculation of the load acting on the rigid beam is important to evaluate the failure of the spot-weld. In this paper, numerical simulation is carried out to evaluate the calculation of the load at the rigid beam. At first, the load on the spot-welded region is calculated with the precise finite element model considering the residual stress due to the thermal history during the spot welding procedure. And then, the load is compared with the one obtained from the model used in the crash analysis with respect to the element size, the element shape and the number of imposed constraints. Analysis results demonstrate that the load acting on the spot-welded element is correctly calculated by the change of the element shape around the welded region and the location of welded constrains. The results provide a guideline for an accurate finite element modeling of the spot-welded region in the crash analysis of vehicles.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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• pp.637-638
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• 2005

AAO templates were fabricated using a two-step anodization process with pretreatment such as electro polishing and annealing. To reduce process time and get well-aligned pore array, rapid thermal processor by an halogen lamp was employed in vacuum state at $500^{\circ}C$ for various time. The pore array of AAO template annealed at $500^{\circ}C$ for 2 h is comparable to a template annealed in conventional furnace at $500^{\circ}C$ for 30 h. The well-fabricated AAO template has the mean pore diameter of 70 nm, the barrierlayer thickness of 25 nm, and the pore depth of $9{\mu}m$. And the pore density can be as high as $2.0\times10^{10}cm^{-2}$.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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• pp.314-314
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• 2012

The dilute magnetic semiconductors (DMS) have been developed to multi-functional electro-magnetic devices. Specially, the Si based DMS formed by ion implantation have strong advantages to improve magnetic properties because of the controllable effects of carrier concentration on ferromagnetism. In this study, we investigated the deep level states of Fe- and Co-ions implanted Si wafer during rapid thermal annealing (RTA) process. The p-type Si (100) wafers with hole concentration of $1{\times}10^{16}cm^{-3}$ were uniformly implanted by Fe and Co ions at a dose of $1{\times}10^{16}cm^{-2}$ with an energy of 60 keV. After RTA process at temperature ranges of $500{\sim}900^{\circ}C$ for 5 min in nitrogen ambient, the Au electrodes with thickness of 100 nm were deposited to fabricate a Schottky contact by thermal evaporator. The surface morphology, the crystal structure, and the defect state for Fe- and Co- ion implanted p-type Si wafers were investigated by an atomic force microscopy, a x-ray diffraction, and a deep level transient spectroscopy, respectively. Finally, we will discuss the physical relationship between the electrical properties and the variation of defect states for Fe- and Co-ions implanted Si wafer after RTA.

• 대한전자공학회논문지TC
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• 제42권9호
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• pp.49-56
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• 2005

RF 전력증폭기 및 Doherty 전력증폭기의 열 메모리 효과는 변조신호의 대역폭과 동작 전력의 레벨에 따라 민감하게 영향을 미친다. 본 논문에서는 전기적인 비선형성을 정확히 모델링하고 열 메모리 효과가 Doherty 증폭기의 왜곡형성에 어떤 영향을 미치는지에 대해 연구하였다. Doherty 증폭기의 열 메모리 특성을 모델링하기 위하여 순시적으로 소모되는 전력과 순시 접합온도의 정확한 관계식을 정립하여 제안하였다. 제안된 모델의 파라미터는 서로 다른 여기상태에 따라 전력증폭기의 특성이 결정되는데, 트랜지스터의 열 메모리 효과는 대역폭이 넓은 W-CDMA 및 UMTS 시스템에서 충분히 고려되어야 한다. 이러한 열 메모리 효과를 사전왜곡 함수에 적응하여 선형화된 전력증폭기의 출력스펙트럼에서 최대 20 dB정도의 ACLR 개선효과를 보인다. 측정결과는 60W급 LDMOS Doherty 전력증폭기로 측정하였으며, 열 메모리 보상기는 ADS로 검증하였다.

• 항공우주기술
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• 제7권1호
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• pp.115-120
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• 2008

인공위성에 사용되는 온도 측정 센서는 서미스터(Thermistor) 와 AD590이 주로 많이 사용되고 있다. AD590은 IC chip으로 서미스터에 비해 고가이며 $1^{\circ}C$ 온도 변화에 출력 전류가 약 $1{\mu}A$ 변하는 특성을 가진다. 이에 비해 서 미스터는 온도 변화에 따라 저항 값이 변하므로 외부에서 전류나 혹은 전압 stimulus를 인가해 주어야한다. 또한 일반적으로 AD590에 비해 저가이며 NTC(Negative Temperature Coefficient)와 PTC(Positive Temperature Coefficient) 두 가지 형태의 센서가 사용되고 있다. 고 정밀 저궤도 지구관측용 인공위성의 경우 온도에 따른 카메라 구조물의 변형이 최종 영상 품질에 영향을 미치게 되므로 고 품질의 영상획득을 위하여 카메라 구조물의 정밀 온도 제어가 필수적으로 요구되며 이를 구현하기 위해서 매우 정확한 온도측정 요구조건이 주어지게 된다. 저궤도 인공위성의 경우 카메라 시스템에 부착된 온도센서의 측정 정확도 요구조건이 $0.3^{\circ}C$ 까지 요구되는 경우도 있다. 본 논문은 저 궤도 인공위성에 적용된 서 미스터의 온도 측정 정확도에 대한 분석 내용을 나타내었다.