• Title/Summary/Keyword: election microscope

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Flexure Strength of Glass-infiltrated Zirconia Complex (유리침투 지르코니아 복합체의 굴곡 강도)

  • Kim, Sa-Hak
    • Journal of Technologic Dentistry
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    • v.31 no.2
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    • pp.9-14
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    • 2009
  • In this study, to improve the flexure strength of Zirconia, on the Zirconia pellet surface measure the flexure strength to melt or permeate the Alumina (Vita Zahnfabrik, Bad Sachkingen, Germany) of private used In-Cream and observe by Scanning election microscope. In the control group(3Y-TZP group), the average of flexure strength was 1623.7MPa, and in the experimental group(Glass-infiltrated 3Y-TZP group) was 1800.2MPa. As a result of observing the interface between glass and zirconia with a scanning election microscope, it was showed that the glass dissolves to permeate into the surface of zirconia, so filled the zirconia with particles.

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A Characteristic study of SiC Nanowires by RF-Sputtering (RF-Sputtering 법에 의한 SiC 나노와이어의 특성연구)

  • Jeong, Chang-Gu;Kim, Tae-Gyu
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.6
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    • pp.344-349
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    • 2010
  • Silicon carbide nanowires were grown by heat treatment of the films at $1200^{\circ}C$ after amorphous SiC thin films were deposited on graphite substrate by radio frequency magnetron sputtering at $600^{\circ}C$. It was confirmed that SiC nanowires with the diameter of 20-60 nm and length of about 50nm were grown from Field Emission Scanning Election Microscope (FE-SEM) and Transmission Election Microscope (TEM) observation. The diameter of nanowires was increased as heat treatment time is increased. The nanowires were identified to ${\beta}$-SiC single crystalline from X-Ray Diffraction(XRD) analysis. It was observed from this study that deposition temperature of samples was critical to the crystallization of nanowires. On the other hand, the effect of deposition time was insignificant.

A Study on the Valve Regulated Lead-Acid Battery using Sulfuric Acid Gel Electrolyte for New Generation Substitution Energy (황산 겔 전해질을 사용한 차세대 대체에너지용 밀폐형 납축전지에 관한 연구)

  • Park, Keun-Ho;Ju, Chan-Hong
    • Journal of the Korean Applied Science and Technology
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    • v.21 no.2
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    • pp.164-173
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    • 2004
  • The capacity and long life of gel electrolyte batteries is connected with gas recombination producting $PbO_2$ and Pb electrode. We prepared with sulfuric acid gel electrolyte to know gel characteristics per density to assemble valve regulated lead-acid (VRLA) batteries. We studied on actions of sulphuric acid gel electrolyte by measuring electrolyte dispersion using Brewster-angle microscope (BAM), charge-discharge cycle, and electrode structure using scanning election microscope (SEM). Sulphuric acid density 1.210 showed excellent gel dispersion in sol condition, electrode condition after fifty cycles in this study.

A Study on the Valve Regulated Lead-Acid Battery using Phosphoric Acid Gel Electrolyte (인산 겔 전해질을 사용한 밀폐형 납축전지에 관한 연구)

  • Ju, Chan-Hong;Park, Keun-Ho
    • Journal of the Korean Applied Science and Technology
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    • v.20 no.4
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    • pp.296-308
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    • 2003
  • The capacity and long life of gel electrolyte batteries is connected with gas recombination producting $PbO_2$ and Pb electrode. We were prepared with phosphoric acid gel electrolyte to know gel characteristics per density to assemble VRLA batteries. We studied by measuring electrolyte dispersion using Brewster-angle microscope(BAM), charge-discharge cycle and electrode structure using scanning election microscope(SEM) per electrolyte density. As a results, phosphoric acid density 1.210 was excellent gel dispersion in sol condition, electrode condition after fifty cycles in this study.

A Description with Scanning Election Microscopy on the Tick Ixodes persulcatus (Schulze, 1930) Male and Female Specimens (Ixodes persulcutus 진드기 자웅 성충에 대한 주사전자현징집적 관찰소견)

  • 강영배;장두환
    • Parasites, Hosts and Diseases
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    • v.23 no.2
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    • pp.305-312
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    • 1985
  • The surface fine structures of Ixodes persulcatus (Schulze, 1930) male and female specimens were observed by means of a scanning electron microscope. A brief review on the biology of the ticks and their disease relationships was also presented. 1. The sexual dimorphism of the specimen was marked; the male was quite smaller than the female. 2. The genital groove was well developed and deep, the anal groove was distinct and characteristically extending anteriorly around the anus. 3. The 4th article was much reduced and situated on the top of the 3rd article ventrally. The hypostome dentition was usually 3/3. 4. The bottom of the basis capitulum of the male specimen was strictly straight in shape. 5. This species was regarded as one of the most important vectors for infectious diseases of migrating birds.

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The biocompatibility and mechanical properties of plasma sprayed zirconia coated abutment

  • Huang, Zhengfei;Wang, Zhifeng;Yin, Kaifeng;Li, Chuanhua;Guo, Meihua;Lan, Jing
    • The Journal of Advanced Prosthodontics
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    • v.12 no.3
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    • pp.157-166
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    • 2020
  • PURPOSE. The aim of this study was to evaluate the clinical performance and reliability of plasma sprayed nanostructured zirconia (NSZ) coating. MATERIALS AND METHODS. This study consisted of three areas of analysis: (1) Mechanical property: surface roughness of NSZ coating and bond strength between NSZ coating and titanium specimens were measured, and the microstructure of bonding interface was also observed by scanning election microscope (SEM). (2) Biocompatibility: hemolysis tests, cell proliferation tests, and rat subcutaneous implant test were conducted to evaluate the biocompatibility of NSZ coating. (3) Mechanical compatibility: fracture and artificial aging tests were performed to measure the mechanical compatibility of NSZ-coated titanium abutments. RESULTS. In the mechanical study, 400 ㎛ thick NSZ coatings had the highest bond strength (71.22 ± 1.02 MPa), and a compact transition layer could be observed. In addition, NSZ coating showed excellent biocompatibility in both hemolysis tests and cell proliferation tests. In subcutaneous implant test, NSZ-coated plates showed similar inflammation elimination and fibrous tissue formation processes with that of titanium specimens. Regarding fatigue tests, all NSZ-coated abutments survived in the five-year fatigue test and showed sufficient fracture strength (407.65-663.7 N) for incisor teeth. CONCLUSION. In this study, the plasmasprayed NSZ-coated titanium abutments presented sufficient fracture strength and biocompatibility, and it was demonstrated that plasma spray was a reliable method to prepare high-quality zirconia coating.

A Study on the Liquid Phase Sintering of Tungsten-Nickel-Manganese alloy (텅스텐-니켈-망간 합금의 액상소결에 관한연구)

  • Hong, Mun-Hui;Lee, Seong;Roh, Jun-Ung;Paik, Un-Hyeong
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 1995.11a
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    • pp.25-25
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    • 1995
  • Liquid phase sintering of 90W-6Ni-4Mn alloy has been investigated as functions of sintering atmosphere, heating rate, and reduction temperature. The present work accounts for the thermodynamic oxidatiodreduction reactions of constituent powders of W, Ni and Mn. By discounting these reactions, the previous investigations would obtain only the alloy with large pores and the lowered relative sintered density, by the liquid phase sintering under a dry hydrogen atmosphere. the sintering cycle consisted of a rapid heating to reduction temperatures under high purity nitrogen atmosphere, and holding for 4 hours and sintering at $1260^{\circ}C$ for 1 hour under a dry hydrogen gas. The relative density of the sintered alloy increased with increasing heating rate. As the reduction temperature increased, the relative density increased to the lm theotical density at the duction temture above $1150^{\circ}C$. The mimsturcatre of sintered alloys has been analysed by a scanning election microscope. The sintered density was compared with those obtained from the other investigators. It was found that the reduction $1150^{\circ}C$ results in the lowered densification of 90W-6Ni-4Mn alloy. This is caused by the fact that reducing reactions of W and Ni oxides contained in W an Ni powders concomitantly leads to oxidizing reaction of Mn powder the oxidized Mn is hardly reduced at sintering temperature and thereby remains large pores in the alloy. It is concluded that the W-Ni-Mn alloy with full density can be obtained by the precise control of atmosphere, heating rate, and sintering temperature.

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Cryopreservation of Human Multi-Pronuclear (PN) Zygote by Ultra-Rapid Freezing (인간 다-전핵기 (>2PN) 수정란의 초급속 동결에 관한 연구)

  • Kim, E.Y.;Yi, B.K.;Nam, H.K.;Lee, K.S.;Yoon, S.H.;Park, S.P.;Chung, K.S.;Lim, J.H.
    • Clinical and Experimental Reproductive Medicine
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    • v.25 no.2
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    • pp.129-134
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    • 1998
  • The objective of this study was to test whether the developmental capacity of human multi-pronuclear (PN) zygotes after ultra-rapid freezing using EM grid can be maintained. For this experiment, multi-PN zygotes which produced in human IVF program were used as an alternatives of normal 2PN zygotes, and they were separated into 3PN or $\geq4PN$ zygotes to compare their in vitro development and cryoinjury according to PN number. As freezing solution, EFS30 which consisted of 30% ethylene glycol, 18% bcoll, 0.5 M sucrose and 10% FBS added D-PBS was used. The result obtained in this experiment was summarized as follows; When the multi..PN zygotes were ultrarapidly frozen and thawed, the high mean percentages (85.5%) were survived. Also when the cleavage rates between control and freezing group were compared with PN number, there were not significantly different in each group (3PN; 81.3% & 85.4% and $\geq4PN$; 90.0% & 95.7%). When the in vitro development rates after thawing were examined, freezing 3PN group (22.0%) was not differed to control 3PN group (38.5%), although the development result of freezing $\geq4PN$ group (45%) was significantly lower than that of control $\geq4PN$ group (44.4%) (p<0.05). These results demonstrate that developmental capacity of human zygote can be obtained by ultra-rapid freezing method using EM grid and EFS30.

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Physicochemical Properties of Chufa (Cyperus esculentus L., var sativus Boeck) Starch (기름골 전분의 이화학적 특성)

  • Han Sang-Ha;Lee Hyun-Yu;Kum Jun-Seok;Park Jong-Dae
    • Food Science and Preservation
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    • v.13 no.3
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    • pp.382-388
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    • 2006
  • Physicochemical properties of chufa starch were investigated The result are summarized as follow: Moisture content crude protein and crude fat were 10.10%, 0.31% and 0.41,% respectively. Amylose content of chufa starch was 41.6% and blue value was 0.49. Lightness and whiteness of chufa starch was 96.36 and 92.23 of Hunter's color value. In iodine reaction, maximum absorbance wavelength (${\lambda}max$) was 628 nm. Water binding capacity was 83% and swelling power and solubility of chufa starch were increased slowly to $60^{\circ}C$, but increased rapidly after $60^{\circ}C$. Scanning election microscope(SEM) showed that granule type of chufa starch was round or elliptic type, and average granule size was $10{\mu}m$. The results by differential scanning calorimetry(DSC) revealed that gelatinization patterns were similar to those of potato or rice starch. In rapid viscoanalyzer(RVA) examination, pasting temperature was $79.95^{\circ}C$ and peak viscosity of chufa starch was 385.08.

Morphology and Intracellular Appearance of Euonymus Vein Clear Virus (사철나무 엽맥 바이러스의 형상과 세포내출현)

  • Chang Moo Ung
    • Korean Journal Plant Pathology
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    • v.2 no.1
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    • pp.1-11
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    • 1986
  • Negatively stained dip preparations from Euonymus showing vein clear symptoms revealed bacilliform particles. The particles tentatively referred to as the Euonymus vein clear virus(EVCV) have a relatively complex structure, measuring 230-280nm in length and 70-80nm in diameter. They have an envelope, 8-10nm thick, provided with evenly spaced beadlike projection about 5-6nm long. The inner tubular core which had no envelope showed helical structures, 200-220nm long, and 50-55nm in diameter. This inner tubular core is interpreted as the virus nucleocapsid. A striking association of virus particles with the nuclei of infected cells was apparent from sections which showed numberous virus particles at the nuclear periphery and in what appeared to be intranuclear virus particle inclusions. Careful examination of these apparent inclusions revealed the presence of the nuclear envelope surrounding them, in addition to cytoplasmic organelles within them. Such profiles were interpreted as having arisen when the sections passed through invaginations of the cytoplasm into the nucleus. In all the sections showing virus particles associated with the nucleus, large number of virus particles were found to be present in expanded areas between the two lamellae of the nuclear envelope. This location is suggested as a possible site of virus assembly. Serveal micrographs of particles found in this location suggested incorporation of the inner lamella of the nuclear envelope into the viral envelope. Various micrographs indicated a possible helical arrangement of certain components present in the virus core.

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