• Title/Summary/Keyword: effective sample size

Search Result 374, Processing Time 0.026 seconds

나노 구조를 가지는 다공성 주석 산화물의 전기화학적 특성 (Electrochemical Characterization of Anodic Tin Oxides with Nano-Porous Structure)

  • 이재욱;박수진;신헌철
    • 한국재료학회지
    • /
    • 제21권1호
    • /
    • pp.21-27
    • /
    • 2011
  • A nano-porous structure of tin oxide was prepared using an anodic oxidation process and the sample's electrochemical properties were evaluated for application as an anode in a rechargeable lithium battery. Microscopic images of the as-anodized sample indicated that it has a nano-porous structure with an average pore size of several tens of nanometers and a pore wall size of about 10 nanometers; the structural/compositional analyses proved that it is amorphous stannous oxide (SnO). The powder form of the as-anodized specimen was satisfactorily lithiated and delithiated as the anode in a lithium battery. Furthermore, it showed high initial reversible capacity and superior rate performance when compared to previous fabrication attempts. Its excellent electrode performance is probably due to the effective alleviation of strain arising from a cycling-induced large volume change and the short diffusion length of lithium through the nano-structured sample. To further enhance the rate performance, the attempt was made to create porous tin oxide film on copper substrate by anodizing the electrodeposited tin. Nevertheless, the full anodization of tin film on a copper substrate led to the mechanical disintegration of the anodic tin oxide, due most likely to the vigorous gas evolution and the surface oxidation of copper substrate. The adhesion of anodic tin oxide to the substrate, together with the initial reversibility and cycling stability, needs to be further improved for its application to high-power electrode materials in lithium batteries.

A Cost Effective Reference Data Sampling Algorithm Using Fractal Analysis

  • Lee, Byoung-Kil;Eo, Yang-Dam;Jeong, Jae-Joon;Kim, Yong-Il
    • ETRI Journal
    • /
    • 제23권3호
    • /
    • pp.129-137
    • /
    • 2001
  • A random sampling or systematic sampling method is commonly used to assess the accuracy of classification results. In remote sensing, with these sampling methods, much time and tedious work are required to acquire sufficient ground truth data. So, a more effective sampling method that can represent the characteristics of the population is required. In this study, fractal analysis is adopted as an index for reference sampling. The fractal dimensions of the whole study area and the sub-regions are calculated to select sub-regions that have the most similar dimensionality to that of the whole area. Then the whole area's classification accuracy is compared with those of sub-regions, and it is verified that the accuracies of selected sub-regions are similar to that of whole area. A new kind of reference sampling method using the above procedure is proposed. The results show that it is possible to reduce sampling area and sample size, while keeping the same level of accuracy as the existing methods.

  • PDF

3차원 측정기를 이용한 자유곡면 측정시 최적의 경로 결정에 관한 연구 (A Study on the Optimal Probe Path Generation for Sculptured Surface Inspection Using the Coordinate Measuring Machine)

  • 조명우;이승종;김문기
    • 한국정밀공학회지
    • /
    • 제12권10호
    • /
    • pp.121-129
    • /
    • 1995
  • The objective of this research is to develop an effective inspection planning strategy for sculptured surfaces by using 3-dimensional Coordinate Measuring Machine (CMM). First, the CAD/CAM database is generated by using the Bezier surface patch mathod and variable cutter step size approach for design and machining of the workpiece model. Then, optimum measuring point locations are determained based on the mean curvature analysis to obtain more effective inspection results for the given sample numbers. An optimal probe sequence generation method is proposed by implementing the Traveling Salesperson (TSP) algorithm and new guide point selection methods are suggested based on the concepts of the variable distance between the first and second guide points. Finally, simulation study and experimental work show the effectiveness of the proposed strategy.

  • PDF

Effects of Mechanically Activated Milling and Calcination Process on the Phase Stability and Particle Morphology of Monoclinic Zirconia Synthesized by Hydrolysis of ZrOCl2 Solution

  • Lee, Young-Geun;Ur, Soon-Chul;Mahmud, Iqbal;Yoon, Man-Soon
    • 한국재료학회지
    • /
    • 제23권10호
    • /
    • pp.543-549
    • /
    • 2013
  • The purpose of this paper was to investigate the effect of a high-energy milling (HEM) process on the particle morphology and the correlation between a thermal treatment and tetragonal/monoclinic nanostructured zirconia powders obtained by a precipitation process. To eliminate chloride residue ions from hydrous zirconia, a modified washing method was used. It was found that the used washing method was effective in removing the chloride from the precipitated gel. In order to investigate the effect of a pre-milling process on the particle morphology of the precipitate, dried $Zr(OH)_4$ was milled using a HEM machine with distilled water. The particle size of the $Zr(OH)_4$ powder exposed to HEM reduced to 100~150 nm, whereas that of fresh $Zr(OH)_4$ powder without a pre-milling process had a large and irregular size of 100 nm~1.5 ${\mu}m$. Additionally, modified heat treatment process was proposed to achieve nano-sized zirconia having a pure monoclinic phase. It was evident that two-step calcining process was effective in perfectly eliminating the tetragonal phase, having a small average particle of ~100 nm with good uniformity compared to the sample calcined by a single-step process, showing a large average particle size of ~300 nm with an irregular particle shape and a broad particle size distribution. The modified method is considered to be a promising process for nano-sized zirconia having a fully monoclinic phase.

The Effects of Non-pharmacological Interventions on Sleep among Older Adults in Korean Long-term Care Facilities: A Systematic Review and Meta-analysis

  • Jung, Sun Ok;Kim, Hyeyoung;Choi, Eunju
    • 지역사회간호학회지
    • /
    • 제33권3호
    • /
    • pp.340-355
    • /
    • 2022
  • Purpose: This study aimed to examine the effects of non-pharmacological sleep intervention programs in improving sleep quality among older adults in long-term care facilities. Methods: A literature search and selection was performed on nine different databases using the guidelines of PRISMA (Preferred Reporting Items for Systematic Reviews and Meta-Analyses). Overall, 14 studies met the inclusion criteria and were systematically reviewed. For the meta-analysis, the effect size was estimated using the random-effects model in Review Manager (RevMan) desktop version 5.4 of the Cochrane Library. Results: The meta-analysis of overall non-pharmacological interventions obtained a total effect size of 1.0 (standardized mean difference [SMD]=1.0, 95% confidence interval [CI]: 0.64~1.35), which was statistically significant (Z=5.55, p<.001). The most frequently studied non-pharmacological intervention was aroma therapy, with an effect size of 0.61 (SMD=0.61, 95% CI: 0.14~1.08), which was statistically significant (Z=2.55, p=.010). In the subgroup analysis, group-based interventions, interventions for >4 weeks, and untreated control studies were more effective. Conclusion: This study confirms that non-pharmacological interventions are effective in improving sleep quality among older adults in long-term care facilities. However, the sample size was small and the risk of bias in assessing the interventions of individual studies was unclear or high, thereby limiting the generalizability of the results. Further reviews that evaluate randomized control trials, evidence-based interventions that consider older adult participants' physical activity levels, different intervention methods and durations, and different control group intervention types are needed to obtain more conclusive evidence.

The Characteristics of Hydrogeological Parameters of Unconsolidated Sediments in the Nakdong River Delta of Busan City, Korea

  • Khakimov, Elyorbek;Chung, Sang Yong;Senapathi, Venkatramanan;Elzain, Hussam Eldin;Son, JooHyeong
    • 한국지하수토양환경학회지:지하수토양환경
    • /
    • 제22권3호
    • /
    • pp.27-41
    • /
    • 2017
  • This study dealt with the characteristics and the interrelations of hydrogeological parameters such as hydraulic conductivity, dispersivity and effective porosity of unconsolidated sediments for providing the basic data necessary for the planning of the management and preservation of groundwater quality in the Nakdong River Delta of Busan City, Korea. Groundwater quality in this area has been deteriorated due to seawater intrusion, agricultural fertilizer and pesticide, industrial wastewater, and contaminated river water. The physical properties (grain size distribution, sediment type, sorting) and aquifer parameters (hydraulic conductivity, effective porosity, longitudinal dispersivity) were determined from grain size analysis, laboratory permeability test and column tracer test. Among 36 samples, there were 18 Sand (S), 7 Gravelly Sand (gS), 5 Silty Sand (zS), 5 Muddy Sand (mS), and 1 Sandy Silt (sZ). Hydraulic conductivity was determined through a falling head test, and ranged from $9.2{\times}10^{-5}$ to $2.9{\times}10^{-2}cm/sec$ (0.08 to 25.6 m/day). From breakthrough curves, dispersivity was calculated to be 0.35~3.92 cm. Also, effective porosity and average linear velocity were obtained through the column tracer test, and their values were 0.04~0.46 and 1.06E-04~6.49E-02 cm/sec, respectively. Statistical methods were used to understand the interrelations among aquifer parameters of hydraulic conductivity, effective porosity and dispersivity. The relation between dispersivity and hydraulic conductivity or effective porosity considered the sample length, because dispersivity was affected by experimental scale. The relations between dispersivity and hydraulic conductivity or effective porosity were all in inverse proportion for all long and short samples. The reason was because dispersivity was in inverse proportion to the groundwater velocity in case of steady hydrodynamic dispersion coefficient, and groundwater velocity was in proportion to the hydraulic conductivity or effective porosity. This study also elucidated that longitudinal dispersivity was dependent on the scale of column tracer test, and all hydrogeological parameters were low to high values due to the sand quantity of sediments. It is expected that the hydrogeological parameter data of sediments will be very useful for the planning of groundwater management and preservation in the Nakdong River Delta of Busan City, Korea.

초임계 이산화탄소를 이용한 가다랑어 내장으로부터 지방산 추출 및 단백질 농축물의 제조 (Processing of Protein Concentrate and Fatty Acid Extraction from Tuna Viscera using Supercritical Carbon Dioxide)

  • 전병수;윤성옥;이승진
    • 한국수산과학회지
    • /
    • 제34권3호
    • /
    • pp.207-212
    • /
    • 2001
  • 초임계 이산화탄소를 이용한 가다랑어 내장으로부터 지방산 추출 및 단백질 농축물의 제조를 위하여 초임계 추출장치의 조건을 압력 1,500-2,000psig, 온도$25^{\circ}C\~40^{\circ}C$으로 하여 추출실험을 하였다. 유속 50mL/min, 압력 1,800psig, 온도 $35^{\circ}C$, 입자크기 0.25mm에서 약 $97\%$ 이상의 지질 추출효율을 보였고, Fig. 5와 6에서 알 수 있듯이 압력 1,800psig, 온도 $35^{\circ}C$, 입자크기 0.25mm의 조건에서 지질을 제거함으로 인하여 약 $50\%$의 단백질이 회수되었고 대부분의 이 취가 제거된 것을 관능적으로 확인할 수 있었다. 이 조건에서 추출된 지질의 주요 지방산으로는 palmitic acid (16: 0), oleic acid(18:1) 등이었고, 주요 유리 아미노산는 taurine 등이었으며, 주요구성 아미노산은 glutamic acid, leucine, lysine 등이었다.

  • PDF

불안 및 스트레스에 대한 간호중재 효과의 메타 분석 (Effects of Nursing Interventions on Anxiety and / or Stress : A Meta-Analysis)

  • 이은옥;송혜향;김주현;이병숙;이은희;이은주;박재순;전경자;정면숙
    • 대한간호학회지
    • /
    • 제22권4호
    • /
    • pp.526-551
    • /
    • 1992
  • The purpose of this study was to identify the commonalities of various nursing interventions and effective intervention methods in each intervention through analysis and synthesis of many accumulated research papers. The study analyzed the effects of various nursing interventions on anxiety and /or stress. For this purpose, 64 experimental studies with randomized or nonequivalent control group pre-test-posttest design were selected from journals of medical and nursing schools, the Korean Nurse, the Korean Nurses' Academic Society Journal, the Cetnral Journal of Medicine, the New Medical Journal, the Nurse Monthly, and from theses and dissertations conducted from 1970 to 1991. The selected studies nor classified according to three characteristics : 1) the research samuel, 2) types and methods of nursing interventions, and 3) statistical tests. The following analysis was done : 1) Confirmation of the accuracy of data drawn from each study by paired review, 2) Estimation of the homogenity of pre-test scores of the dependent variable between control and experimental groups warranted the effect size of post-scores, 3) If the homogenity of pre-test scores did not warrant, the change scores from pre-test to post-test were used to estimate the effect size, 4) Use of the effect size of each study among homogenious studies was tested for each intervention method, such as relaxation, information, and touch and /or support. Finally, for the studies not showing homogenity, an ANOVA test was used to identify patterns for each intervention. Some findings are summarized as follow : The effect sizes for relaxation and information were greater than those for touch and /or supportive technique. Studies using random assignment had greater effect sizes than nonrandomized sample studies using the same intervention. For healthy people, group education was more effective than individual teaching. However, for patients, relaxation and touch and /or supportive techniques given on individual basis were more effective than when given in a group situation. Measuring anxiety and stress by biological indicators was less effective than by self-report. Budzynski's relaxation method was the most effective. The more frequently the techniques applied, the larger the effect size. On the bases of these findings, the following recommendations were made : 1. A combination of information, relaxtion, and touch-supportive techniques should be used for greater effect in reducing the level of anxiety and /or stress. 2. Information is the first choice of intervention to reduce the level of anxiety and /or stress of healthy People : other interventions may be added depending on the conditions of the subjects.

  • PDF

Experimental investigation of organic fouling mitigation in membrane filtration and removal by magnetic iron oxide particles

  • Jung, Jaehyun;Sibag, Mark;Shind, Bora;Cho, Jinwoo
    • Membrane and Water Treatment
    • /
    • 제11권3호
    • /
    • pp.223-229
    • /
    • 2020
  • Here magnetic iron oxide particles (MIOPs) were synthesized under atmospheric air and which size was controlled by regulating the flow rate of alkali addition and used for efficient removal of bovine serum albumin (BSA) from water. The MIOPs were characterized using field-emission scanning electron microscopy (FE-SEM), Fourier transformation-Infrared spectroscopy (FT-IR) and vibrating sample magnetometer (VSM). The results revealed a successful preparation of the MIOPs. The removal efficiency for BSA using MIOPs was found to be about 100% at lower concentrations (≥ 10 mg/L). The maximum adsorption of 64.7 mg/g for BSA was achieved as per the Langmuir adsorption model. In addition, microfiltration membrane for removal of BSA as model protein organic foulant is also studied. The effect of various MIOPs adsorbent sizes of 210, 680 and 1130 nm on the absorption capacity of BSA was investigated. Water permeability of the BSA integrated with the smallest size MIOPs membrane was increased by approximately 22% compared by the neat BSA membrane during dead-end filtration. Furthermore, the presence of small size MIOPs were also effective in increasing the permeate flux.

유치도뇨관 크기 감소 및 정보제공이 수술 후 유치도뇨관으로 인한 불편감과 간호요구도에 미치는 효과: 회복실에 입실한 성인남자 환자를 중심으로 (The Effect of a Decrease Indwelling Catheter Size and Preoperative Education on Bladder Discomfort and Patient's Nursing Needs)

  • 백현주;이혜미
    • 가정∙방문간호학회지
    • /
    • 제21권2호
    • /
    • pp.120-126
    • /
    • 2014
  • Purpose: This study was carried out to investigate the effect of a decrease in indwelling catheter size and preoperative education on bladder discomfort and nursing needs. The study was conducted on patients in the recovery room after their surgery. Methods: This study is a randomized control trial. Data were collected from September 2011 to February 2012 at a university hospital in Bundang, Korea. The sample consisted of 75 patients, excluding one patient from the experimental group 2. From among the patients that were sent to the ICU, 24 were in experimental group 1, 24 were in experimental group 2, and 27 were in the control group. Data were collected and analyzed using a chi-square test, t-test, and one-way ANOVA. Results: There were significant differences between the bladder discomfort experienced by patients in experimental group 1 and the control group, and experimental group 2 and the control group. Then nursing needs of the control group were higher than those of the experimental groups 1 and 2. Conclusion: The decrease in indwelling catheter size and preoperative nursing education is an effective nursing intervention in perioperative care.