• Journal of the Korean Society of Clothing and Textiles
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• v.24 no.5
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• pp.619-627
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• 2000

Historically, dyed textiles were symbols of status and, because of their expense, reserved only for people of wealth and specalist, Early dye sources probably included plant, animal and mineral extracts. As synthetic dyes have been developed, beginning with synthetic indigo in 1897, reliance on natural dye sources diminished. But renewed interest in natural dyes is fueled by a pro-environment consumer aware of the ecological liabilities of the dye industry. Han Jee was imported from China where it was influenced to period of the three kingdoms(Silla, Baekje, Kokuryo). After that, Han Jee was used for paper in old Korea for long thime before paper was came with civilization. In this paper, dyeing of Han Jee with loess were investigated according to dyeing temperature, dyeing time, loess concentration, and effects of additives. As a reuslts, λmax of Han Jee dyed by loess was 710nm. ΔE values of Han Jee increased by loess concentration, dyeing time, dyeing temperature. Dyeing with additives treatment increased dyeability. Especially, Han Jee treated with aluminium acetate shows the largest dyeability of the Han Jee. The Han Jee dyed loess had very good lightfastness.

• Textile Coloration and Finishing
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• v.18 no.5 s.90
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• pp.22-29
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• 2006

The purpose of this study was to investigate the dyeability and antibacterial activity on wool fabric dyed with cochineal at variable dyeing conditions. Al, Cr, Fe, Cu and Sn were used as mordants and adsorption was compared with different mordanting methods. The optimum dyeing conditions of wool fabrics were dyeing concentration 2.0%(o.w.s), dyeing temperature $60^{\circ}C$, pH 3 and dyeing time 30 minutes. The pre-mordanting method was preferred for Al and Cr, and the post-mordanting one was preferred for Cu, Sn and Fe to achieve better dyeing. The optimum mordanting conditions of wool fabrics dyed with cochineal were mordanting concentration of 1%(o.w.s), mordanting temperature $60^{\circ}C$, and dyeing time 30 minutes. Wool fabrics dyed with cochineal showed a little antibacterial activity, but it was increased by Cu and Sn mordanting. The light fastness and perspiration fastness of wool fabric treated with cochineal were improved by mordanting.

• Journal of the Korean Society of Clothing and Textiles
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• v.33 no.11
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• pp.1774-1780
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• 2009

The dyeing properties of cotton fabric with Inonotus obliquus are studied by investigating the effect of dyeing conditions on dye uptakes such as, the concentration of Inonotus obliquus, dyeing temperature, time, and pH values. In addition, the effects of mordants on dye uptakes and antibacterial activities are also investigated. The results are summarized as follows: The dye uptakes of dyed fabrics were increased gradually with an increasing concentration of Inonotus obliquus. K/S values were the highest when the dyeing temperature and time were at $60^{\circ}C$ and 60 minutes, respectively. As for the changes of pH values of dyeing solution, K/S values recorded the highest at pH3-pH5. Antibacterial activities of Inonotus obliquus dyeing solution showed a significant effect in dyed cotton fabric with mordanting.

• Textile Coloration and Finishing
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• v.9 no.5
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• pp.10-18
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• 1997

In order to study the properties of safflower yellow colors, thermodynamic parameters and dyeing properties on the silk in several dyeing conditions were investigated. The uv-visible spectra of safflower yellow colors in several solvents show hypsochromic shift with the polarity of solvent but bathochromic shift with increasing acidity of solution. The apparent diffusion coefficients and standard affinities of dyeing increased with the increase of dyeing temperature. The standard heat of dyeing(${\Delta}H^0$), entropy change(${\Delta}S^0$) and activation energy($E_{act}$) were calculated to be - 1.144kcal/mol, -7.498(5$0^{\circ}C$)~-3.804(9$0^{\circ}C$)cal/molㆍdeg and 0.123kcal/mol, respectively. The concentration of safflower yellow colors in the silk fiber increased with dyeing temperature, time, concentration of colors and acidity of initial dyebath. Silk fabrics were dyed bright yellow by pre-mordanting with tin chloride. Lightfastness of silk fabrics pre-mordanted by tin chloride was not excellent.

• Textile Coloration and Finishing
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• v.11 no.4
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• pp.39-49
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• 1999

In order to study the properties of cochineal colors, uv-visible spectra of cochineal colors solution, dyeing properties on the wool in several dyeing conditions and thermodynamic parameters were investigated. UV-visible spectra of cochineal colors solution showed hypochromic effect with the lapse of irradiation time but bathochromic shift with decreasing acidity of solution and addition of metallic ions. The concentration of cochineal colors in wool fiber increased with the increase of dyeing temperature, time, and acidity of initial dyebath. The value of apparent diffusion coefficients and standard affinities of dyeing decreased with the increase of dyeing temperature. The standard heats of dyeing$(\Delta{H}^\circ)$ and variation of entropy$(\Delta{S}^\circ)$ increased with the increase of concentration of initial dyebath. The activation energy$(E_a)$ were calculated to be 1.399~2.595kcal/mol in condition of 6~1%(o.w.f) dyebath. Wool fabrics were dyed reddish blue by iron sulfate, copper sulfate, aluminum acetate and tannic acid, and red by tin chloride, respectively. Lightfastness of wool fabrics dyed by cochineal colors were increased by mordant treatment, especially copper sulfate and iron sulfate treatment.

• Fibers and Polymers
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• v.7 no.3
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• pp.255-261
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• 2006

There is increasing interest in the many beneficial aspects of green tea to human such as anti-carcinogenic, anti-aggregant, anti-allergic, anti-bacterial, anti-mutagenic, and anti-oxidant activities. Besides these beneficial aspects, it has been reported that green tea ingredients, especially polyphenolic families (i.e., catechin), have some UV protection property both in vivo and in topical applications. In this study, green tea extract was used as a dyeing stock for cotton and the UV protection property of the dyed cotton fabric was examined. To increase the affinity of cotton fiber to the polyphenolic components in the green tea extract, a natural biopolymer, chitosan, was used as mordanting agent. The effects of chitosan concentration in mordanting on the dyeing characteristics and the UV protection property were examined. Chitosan mordanted green tea dyed cotton showed better dyeing characteristic and higher UV protection property compared with the unmordanted green tea dyed cotton. As the chitosan concentration in mordanting increased, the dyeing efficiency and the UV protection property also increased. Therefore, adapting chitosan mordanting in green tea dyeing can increase the UV protection property of cotton fabrics to some extent.

• Journal of the Korean Society of Clothing and Textiles
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• v.34 no.3
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• pp.508-517
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• 2010

One-step reduction/dyeing method was optimized for wool dyeing with natural indigo dye in this study. The effects of reduction/dyeing conditions including dye temperature and time, the pH of bath, concentration of dye, and reducing agent on dye uptake and color were investigated. The dye uptake was higher with no addition of alkali. Dyeing was carried out through the use of only sodium hydrosulfite in the bath. The maximum dye uptake was obtained at $60^{\circ}C$ for 30min and the dyed fabrics appeared in the PB Munsell color range. Dye uptake improved with the increase of a natural indigo dye concentration with the same sodium hydrosulfite concentration. At a higher dye uptake, the fabric color became more purplish and the maximum absorption shifted from 660nm to 620nm. Color reproducibility was reliable with a color difference in the range of 0.41~1.43. Regardless of color strength, washing and dry cleaning fastnesses were good with a 4/5 rating, and fastnesses to rubbing and light were acceptable with a 3/4~4 rating.

• Textile Coloration and Finishing
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• v.32 no.4
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• pp.217-225
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• 2020

In this study, the dyeing characteristics of nylon fabric which is dyed with supercritical fluid were investigated. There were two dyes used in the dyeing experiment: C.I. Disperse Red 167 and C.I. Disperse Violet 93. Dyeing temperature, pressure, and leveling time were fixed at 110℃, 250bar, 60minutes, and the experiment was conducted with dyeing concentration of 0.1, 0.3, 0.5, and 0.85% o.w.f. The analysis of the experimental results was found out through the measurement of washing fastness and color coordinate. In addition, the calibration curve of each dye was drawn up and the amount of remaining dye was checked by measuring the absorbance of the residual dye. As a result of color difference measurement, as the concentration increased, the L⁎ value decreased and the K/S value increased. However, the increase in K/S value compared to the amount of input decreased as the concentration increased. The comparative experiment on the amount of residual dye(C.I. Disperse Red 167) in the pot showed that 99.14% of the amount was dyed at the concentration of 0.1% o.w.f, while it rapidly decreased to 77% at 0.85% o.w.f. C.I. Disperse Violet 93 dye also decreased from 0.5% o.w.f to 93.91%. In the washing fastness experiment of both dyes, the level of washing fastness began to decrease from samples dyed at 0.5% o.w.f. It may be because the simply absorbed dye was produced instead of completely being fixed in the amorphous region of the nylon fiber.

• Fashion & Textile Research Journal
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• v.13 no.2
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• pp.263-268
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• 2011

One-step reduction/dyeing method was applied for ramie dyeing with natural indigo powder. The effect of reduction/dyeing conditions including the pH of bath, dye temperature and time, and concentration of indigo powder and reduction agent on dye uptake and color properties were investigated. Regardless of addition of alkali, the dyed fabrics appeared in the PB Munsell color range(${\lambda}_{max}$: 660 nm) and the dye uptake was much higher with no addition of sodium hydroxide. Dyeing was carried out through the use of only sodium hydrosulfite in the bath. The maximum dye uptake was obtained at 60 for 30min. Saturated dye uptake was obtained at 2 g/L of sodium hydrosulfite concentration up to 2 g/ L of indigo powder. Whereas, at higher indigo powder concentration (4 g/L), more than 3 g/L of reducing agent concentration was required for obtaining the saturated dye uptake. Color reproducibility was reliable with color difference in the range of 0.03~0.16. Regardless of color strength, fastness to rubbing was acceptable with a 3/4~4/5. Fastness to washing, dry cleaning, and light of samples with low color strength were poor. Whereas, fastness to washing, dry cleaning, and light of samples with high color strength were very good.

• Textile Coloration and Finishing
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• v.3 no.3
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• pp.34-43
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• 1991

The dyeing property of milling type acid dyes with various chemical constitution were studied in one bath dyeing of Wool/Nylon blended fabrics and the proper dyeing condition to get solid color by using reserving agent was also examined. The result of the experiments can be summarized as follows; 1) Although the effect of pH on dyeing of wool with a highly hydrophiilic dye is great in the dyeing of wool and nylon, the proper pH of dyeing bath is weakly acidic 5, in which levelling dye can be obtained by increasing the solubility product. 2) Under a constant pH, the dye with fewer numbers of sulfonic acid groups increases the dyeing amount of nylon as the concentration of the dye is increased. Thus the appropriate dye for light color is the one with many numbers of sulfonic acid groups and the proper dye for medium and deep color is of fewer sulfonic acid groups for one-bath dyeing. 3) When the dye concentration is greater than the critical depth, the K/S value of wool and nylon was almost not effected or slightly increased.