• 패션비즈니스
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• 제15권2호
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• pp.120-130
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• 2011

This study is a fundamental research on the natural Polygoum tinctoria dyeing to quantify scientifically and satisfy the reproducibility of the procedure. By dyeing the silk fabrics, the establishment of accurate dyeing method was sought. At the same time, we tried to modify the traditional dyeing methods, broaden the methods, and apply the dyeing variously. The dyeability and color changes were compared and reviewed according to the changes in the reducing temperature, reducing time, concentration of the reducing agent, dyeing temperature, dyeing time, concentration of NaOH, and the number of repetition of dyeing. The optimum conditions in the dyeing procedure are as follows: Added concentration of the reducing agent is 3g/${\ell}$. Reducing temperature is $60^{\circ}C$. Reducing time is 40minutes. Dyeing temperature is $30^{\circ}C$. Added concentration of NaOH is 1g/${\ell}$. Dyeing time is 30minutes.

• 한국생활과학회지
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• 제23권5호
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• pp.861-871
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• 2014

This study explored applicability of natural dyeing and functional property of base paper using paper yarn and fabrics with green laver extracts. As a result of measuring dyeability and functional property of cotton, silk, and a blended fabric of cotton/mulberry, $60^{\circ}C$ and 40 minutes was the optimal dyeing condition for the cotton fabric under an alkali condition; $50^{\circ}C$ and 60 minutes for the silk fabric; $60^{\circ}C$ and 50 minutes for the blended fabric of cotton/mulberry. As a result of measuring the color fastness after dyeing cotton, silk and the blended fabric of cotton/mulberry, fastness to washing, water, rubbing, dry cleaning and light was superior. In terms of functional property, the silk and the blended fabric of cotton/mulberry were superior concerning antimicrobial properties of the fabric dyed with green laver extracts while the cotton fabric showed 90% or over. Regarding deodorization, the blended fabric of cotton/mulberry was the most superior. All the fabrics were harmless to the human body as they had heavy metal content below the standard. Considering the research results comprehensively, the green laver extracts possibly has enough applicability and functional property as a natural dyes. Moreover, it has potential to be developed new eco-friendly fashion materials.

• 한국의상디자인학회지
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• 제5권3호
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• pp.1-6
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• 2003

The purpose of this study was to investigate the dyeability and color fastness of cotton and silk fabrics dyed with extract of Arrowroot leaf princeps. The experimental items were divided into the mordant treatment, component of fabric and kind of mordants. The experimental study was done by laundering, abrasion(dry/wet), perspiration(acid/alkali), light fastness, color difference by C.C.M system and K/S test. The summerized finding reulted from experiment and investigation are suggested as follows : In the C.C.M and K/S test on mordanting method and kind of fabric, that of silk and cotton was the most effective in the pre mordant treatment. In the C.C.M and K/S analysis on 5 mordants, that of silk and cotton was significantly improved when mordants was treatmented. Especially, that of Fe mordanting treatment was higher than Al, Cu, Cr and none. In color fastness on mordants, laundering, perspiration and abrasion fastness showed 4-5 grade but light fastness showed 1-3 grade.

• 한국가정과학회지
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• 제9권1호
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• pp.43-50
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• 2006

The main colorant of Chelidonium majus extracts is a berberine which shows relatively good dyeability onto silk fabrics in the appropriate dyeing conditions without mordant, But cotton fabrics are difficult to dye with berberine because of the low substantivity the cationic to cellulosic fibers. we treated cotton fabrics using three types of polycarboxylic acid, DL-malic acid, citric acid, 1,2,3,4-butanetetracarboxylic acid(BTCA) to increase dyeability of Chelidonium majus extracts onto cotton fabrics. As a result the cotton fabrics treated with polycarboxylic acid could be dyed with Chelidonium majus extracts and also showed yellow vividly. The dye uptake were increased with increasing the number of carboxy groups. And so dye uptake resulted the largest in the BTCA solutions which have four carboxylic groups in the molecular unit. The optimal dyeing temperature a of Chelidonium majus extracts onto polycarboxylic acid treated cotton fabrics were $60^{\circ}C$. The dye equilibrium was reached 20 minutes after dyeing. Neutral pH of dye solutions showed in higher K/S value than acidic or alkaline conditions. But the colorfastness to washing and light according to polycarboxylic acid treat was not enhance.

• 한국생활과학회지
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• 제21권4호
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• pp.791-803
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• 2012

This study intends to identify applicability of natural dye extracted from Aplysia kurodai, aiming to standardization of Aplysia kurodai natural dyeing through scientific validation by analyzing characteristics of pigment elements to review dyeability, colorfastness and antibacterial activity. Such material as silk fabrics that is animal fiber were used for this purpose, and derived following summarized results. UV/VIS spectrum analysis on the pigment of Aplysia kurodai that was extracted from purple gland showed that maximum absorbtion was near 540 nm. The silk fabric optimal dyeing can be achieved at a temperature of $55^{\circ}C$ with a colorant concentration of 5%. Dyed at $55^{\circ}C$ with interval of 10~90 minutes for identifying dye uptake over time to observed slow increase of dye uptake over time, and equilibrium occurred at 50 minutes. For dye uptake according to pH, while dye uptake was superior in acidity, it decreased rapidly in a base after pH 7. For color changes according to pH variation, it was reddish purple in acidity and was purplish red in a base. For color changes according to mordanting method, more clear color change had been obtained when process with aluminium pre-mordanting than non-mordanting and post-mordanting. The colorfastness to light, perspiration and washing was 1, 4~5, and 3~4 ratings respectively. The silk fabric dyed with Aplysia kurodai demonstrated excellent antimicrobial activity to Staphylococcus aureus and Klebsiella pneumoniae. The Aplysia kurodai can be used as a new colorant for the natural dyeing of silk.

• 한국의류산업학회지
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• 제15권1호
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• pp.138-146
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• 2013

Chemical compositions and biological functions of brown colorants extracted from pine bark(Pinus densiflora) have been studied. Dyeing test using multifiber fabrics with extracted colorants were preliminary carried out. Dyeing conditions and fastness tests of selected fabrics have been also studied. The brown colorants were produced 1.5% concentrations by solvent extraction from milled pine bark using methanol. The colorants were extracted with 80% methanol as best choice by a criteria of solid quantity and dyeability on fabrics. The chemical compositions were identified as mixtures of taxifolin epicatechin and procyanidin by LC/MS analysis. The brown colorants could be dyed not only natural fibers such as cotton, silk and wool but also synthetic fiber as nylon and semi-synthetic fiber as viscose rayon. Maximum K/S values was shown at 400 nm according to different fiber with color appearance of redish brown. Optimum pH and temperature of dyeing conditions was 4 and above $80^{\circ}C$, respectively. The brown colorants had a strong antioxidant activity compared to Butylated hydroxyanisole as standard and weak antimicrobial activity against E. coli. compared to kanamycin. Washing, rubbing, perspiration, dry cleaning and light fastness for cotton, nylon and silk dyed with the brown colorants were carried out by KS K method. Most of color fastness such as washing, rubbing, perspiration, and dry cleaning were represented as 4-5 grade. However, light fastness was reported as 2-3 grade. From this studies, brown colorants produced pine bark have a high potentials for natural dyeing on fabrics with antioxidant activity.

• 패션비즈니스
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• 제20권4호
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• pp.128-140
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• 2016

In this study, dyeability of Urtica Dioica L. extract, which is relatively less studied, was measured. The extract of this plant was used to dye cellulose and protein fiber to check its usage as a natural green dye. Three different methods were used to produce extract. Dried Urtica Dioica L. was extracted with 100% ethanol, 50% ethanol with 50% distilled water and 100% distilled water. Then dyeing solution was obtained by blending with distilled water at 1-to-1 ratio. The maximum dyeability was obtained when 100% ethanol extract of dried Urtica Dioica L. used to dye fabrics at 60 degrees celsius for 60 minutes without mordant treatment. Cotton, rayon, wool and silk were dyed and dyeability for each fiber was measured for color difference value then compared to its control. The results show that dyeability of rayon and dyeability of wool are stronger, and that when color position for each mordant is measured, color difference is most diverse on cotton with pre-mordant treatment. Color fastness to wash, perspiration and rubbing crockmeter were superb, but color fastness to light was low, therefore, additional study on this is needed to improve. Urtica Dioica L. is now expected to be used practically as green color dye as well as medicinally and edible.

• 패션비즈니스
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• 제11권2호
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• pp.92-101
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• 2007

This research was carried out following the preceding research on natural cellulose fabrics dyed with extract of fresh african marigold petals. Dyeability on fabrics was tested by dyeing with wool and silk which are natural protein fibers. Dyeing tests were carried out under different pH of the dye solution and mordants, examining the changes in the surface color, K/S value, and maximum absorption wavelength. The probability of improving dyeability was investigated by pre-mordanting with pre-treated chitosan. Wool fabrics showed color tone of medium or less saturation and brightness, in dark yellow color series. An orange color of high saturation was only obtained by tin mordanting. Wool showed higher K/S value than cellulose fibers. In summary, marigold dye has more affinity for protein fibers. It showed better dye effect in wool than silk. The chitosan pre-treatment and pre-mordanting lowered the K/S value of wool, which showed that chitosan pre-treatment does not improve dye uptake. However, different from the dyeing carried out by pre-mordanting without pre-treatment with chitosan, more diversified colors could be obtained by mordants. Therefore, for the dyeing natural protein fibers with marigold extract, post-mordanting does not require chitosan pre-treatment. However, pre-mordanting with chitosan pre-treatment could implement diverse colors. Considering its dyeing behaviors which are similar in both natural cellulose and protein fibers, african marigold extracts can be evaluated as a stable and highly practical dye.

• 한국염색가공학회:학술대회논문집
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• 한국염색가공학회 2011년도 제45차 학술발표회
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• pp.33-33
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• 2011

Artificial silk that called "Ponggi (Gyeongsangbukdo, Korea) In-Gyeun" in Korea is entirely viscose rayon of which made main component refined larches and cotton linter. It also is natural fabrics with light weight, cool texture, free from the body and well ventilation property, so, feel good touch during the wearing. In addition, it often used as summer cloth and bedding because it has good absorbancy to perspiration and antistatic. The "Hanji", made of paper mulberry, is known as useful material for human. In this research focused on dyeability of Artificial silk/paper mulberry mixed fabrics using Dendropanax morbifera Lev.(called as "Hwangchil") Especially, the results were in comparison to the dyeing properties of Hwangchil with liquid/solid fermentation or not. As the results, The ${\Delta}E$ difference was dominated when the fabric dyed with fermentation by solid state at $60^{\circ}C$. And it was confirmed that the pH of fermented dye had an important influence in the coloration.

• 한국의류산업학회지
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• 제11권5호
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• pp.818-826
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• 2009

Dyeability of microbial violacein produced from Chromobacterum violaceum CV107 on to multifiber fabrics has been studied. The bluish-purple colourants were produced by cultivation of Chromobacterum violaceum using LB liquid medium for 2 days. The colourant was extracted with 80% acetone and identified as violacein by LC/MS analysis. The violacein could be dyed on not only natural fibers such as Cotton, Silk and Wool but also synthetic fibers such as Diacetate, Triacetate, Creslan 61 and Nylon 66. Maximum K/S values were shown at 540-580 nm according to different fiber with color appearance of purple or blue. An optimum pH and temperature under dyeing condition were 10 and $70^{\circ}C$, respectively. Any mordants were not improved colour density and quality on various fabrics. From this studies, pigments produced microbe have a high potentials for natural dyeing on fabrics. Finally, development of new colourants from microbe has made a possible change for new dyeing field in respects of eco-friend and repeatability of natural dyeing for apparels.