• Title/Summary/Keyword: dropping

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N-Alkylation of Primary Aromatic Amines Using Alkylhalide and Triethylamine (알킬할라이드와 Triethylamine을 이용한 일급 아로미틱 아민의 N-알킬레이션)

  • Kim, Ju-Hee;Park, Myung-Sook
    • YAKHAK HOEJI
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    • v.49 no.2
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    • pp.162-167
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    • 2005
  • Synthetic method for the selective N-monoalkylation of anilines using alkyl halides and triethylamine under room temperature was described. The corresponding N-alkyl anilines were obtained in good yields with minor quantities of dialkylated products. Anilines 2a-m and 3a-m were identified using NMR and IR. A series of 2a-m and 3a-m has been synthesized from aniline, toluidines, ethylanilines, aminoacetophenones, phenetidines. Formation of anilines was undertaken with dropping of alkylhalides at room temperature in methanol (or ethanol) for 3 hours~5 days. Selectivity on the monoalkylation was relatively high. Synthetic ratio of monoalkylated and dialkylated product was 94 : 6 in case of maximum monoalkylation.

Effect of High Voltage Pulsed Current on Edema Reduction (고전압 전기 자극의 부종 감소 효과)

  • Kim, Youn-Jung;Kim, Choel-Yong;Hong, Ju-Wan;Ahn, Duk-Hyun
    • Physical Therapy Korea
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    • v.1 no.1
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    • pp.61-66
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    • 1994
  • The purpose of this study was to investigate the effect of a single treatment o voltage pulsed current (HVPC) on edema reduction. Hind limbs of 23 anesthetized were injured by dropping a 400 g weight onto the plantar aspects of the feet. On limb of each frog was randomly selected to receive 30 minutes of continuous, 12 cathodal HVPC at voltages 10 % less than motor threshold levels. Limb volumes measured by water displacement before trauma and at predetermined intervals hours posttrauma. Sources of significant differences were determined by t-test HVPC significantly (p<0.05) reduced edema formation. We hypothesize that HVP also be effective in controlling edema formation after impact injuries in humans.

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Analysis and Design of Nuclear Spent Fuel Dry Storage System under Irregular Operation (사용후 핵연료 건식저장장치의 비정상 운영조건의 해석과 설계)

  • Song, Hyung-Soo;Min, Chang-Shik;Yoon, Dong-Yong
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.11a
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    • pp.381-384
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    • 2004
  • Delaying and objection for the construction of storage spent-fuel disposal has prompted to consider expanding on-site storage of spent reactor fuel since it can eliminate the need for costly and difficult shipping and control of the spent fuel completely under the direction of the owner-utility. The dry storage unit developed in Canada can accommodate Korea heavy water reactor fuel elements and become a candidate for the Korean market. In this paper, finite element analyses were carried out in order to investigate the structural behavior of the nuclear spent fuel dry storage system, which is subjected to impact loads such as collision of a truck load and dropping of flask under the irregular operation.

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A Method for the Performance Ehancement of PRMA Protocol for Mobile Voice/Data Integration (음성/데이터 통합형 PRMA 프로토콜의 성능 개선 기법)

  • 송재섭;김연수
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.25 no.3B
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    • pp.423-430
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    • 2000
  • Future microcellular systems will require distributed network control. A packet-switched network is suitable for this requirement. The packet reservation multiple access(PRMA) is a Reservation-ALOHA like protocol for wireless terminals to transmit packet speech to a base station. It allows spatially distributed users in cellular systems to transmit packeted voice and data to a common base station using a shared channel. In the existing PRMA, the problem is that the voice packets may collide with the data packets due to simultaneous channel access. the problem may be a major performance degradation factor to a voice and data mixed system. We propose a new PRMA method that integrates voice and data traffic efficiently by resolving the collision problem between data and voice packets. The proposed PRMA method gives a performance improvement than the existing PRAMA method in terms of voice packet dropping probability and data delay characteristic. From analytic results, we can confirm that the proposed PRMA method show a performance improvement than the existing PRMA protocol.

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The Effects on the Crystal Structure of LDPE thin film exposed Radiation (방사선이 LDPE박막의 결정구조에 미치는 영향)

  • 강전홍;김한준;유광민;박강식;김종석;한상옥
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.181-184
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    • 2000
  • LDPE pelet is distilled to make 0.5 Wt% solutions and fabricated as LDPE thin film by dropping the solution onto glass substrate, and then annealed the film to be crystalline. The structure is observed as crystalline regions and non-crystalline regions. The crystalline region is exposed at radiation and as the result, there appeared degradation at the total region of the crystal structure. It is considered therefore that radiation exposure at the crystal structure is badly effected on insulation property and lifetime of materials.

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Transient Responses of an Airplane Taking off from and Landing on a Very Large Floating Structure in Regular Waves (규칙파중 항공기 이.착륙시 초대형 부유식 해양구조물의 천이 응답 해석)

  • 신현경;이호영;임춘규;강점문;윤명철
    • Journal of Ocean Engineering and Technology
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    • v.15 no.1
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    • pp.26-30
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    • 2001
  • Up to now, Most studies of hydroelasticity are about frequency domain analysis. Those aren't suited for analysis of the landing take-off, and dropping of aircraft on a structure. So, the concern of this paper is the transient behavior of a VLFS subjected to dynamic load, induced by airplane landing and take-off. To predict the added mass, damping coefficient, and wave exciting force, the source-dipole distribution method was used in the frequency domain. The responses are accomplished by using the FEM scheme. A time domain analysis method is based on the Newmark β method to pursue the time step procedure, taking advantage of memory effect function for hydrodynamic effects.

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A Study on the Flow Behavior of the Viscoelastic Fluids in the Falling Ball Viscometer (낙구식 점도계를 이용한 점탄성유체의 유동에 관한 연구)

  • 전찬열
    • Journal of the Korean Society of Safety
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    • v.3 no.1
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    • pp.15-19
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    • 1988
  • The falling ball viscometer has been widely used for measuring the viscosity of the Newtonian fluids because of its simple theory and low cost. The use of the falling ball viscometer for measuring the non-Newtonian viscosity has been of interest to rheologists for some years. The analysis of the experimental results in a falling ball viscometer rest on Stokes law which yields the terminal velocity for a sphere moving through an infinite medium of fluids. An attempt to use the falling ball viscometer to measure the non-Newtonian viscosity in the intermediate shear rate ranEe was sucessfully accomplished by combining the direct experimental obserbations with a simple analytical model for the average shear-stress and shear rate at, the surface of a sphere. In the experiments with highly viscoelastic polyacrylamide solutions the terminal velocity was observed to be dependent on the time interval between the dropping of successive balls. The time-dependent phenomenon was used to determine characteristic diffusion times of the concentrated solutions of polyacrylamide.

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A Hand-off Algorithm for Performance Improvement in the Reuse Partitioning Systems (재사용 분할 시스템에서 성능 개선을 위한 핸드오프 알고리즘)

  • Lee, Young-Chul;Kim, Min-Hong;Lim, Jae-Sung;Kimn, Ha-Jine
    • The Transactions of the Korea Information Processing Society
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    • v.7 no.2
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    • pp.437-445
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    • 2000
  • The reuse partitioning system in microcellular networks are dropped performance of system because of increase hand-off of high-speed terminal. In this paper, we propose hand-off algorithm to improve the performance of reuse partitioning system using microcell according to the ratio of traffic distribution between innercell and outercell from resource management of high-speed and slowspeed terminal. Also, we compare to RPS and evaluate the teletraffic performance analysis of high-speed and slow-speed terminal through computer simulations that we derive the hand-off probability, call dropping probability.

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The Experimental Study on Anti-bacterial Potency of Soyum Herbal-acupuncture, Hwangryunhaedoktang & Coptidis rhizoma on Staphylococcus aureus (소염 약침액, 황련해독탕, 황련이 Staphylococcus aureus에 미치는 항균효과에 대한 실험적 연구)

  • Seo, Hyung-Sik
    • Journal of Pharmacopuncture
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    • v.9 no.2
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    • pp.87-92
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    • 2006
  • Objective : This experimental study was performed to investigate the effect of Soyum Herbal-acupuncture, Hwangryunhaedoktang & Coptidis rhizoma on Staphylococcus aureus that induce keratitis. Methods : MIC was measured by dropping to $50\;{\mu}l$ according to density Soyum Herbal-acupuncture, Hwangryunhaedoktang & Coptidis rhizoma(100%, 10%, 1%, 0.1%). Anti-bacterial potency was measured by the size of inhibition zone with change of volume. Results : 1. MIC on Staphylococcus aureus in Soyum Herbal-acupuncture disappear all sample. 2. MIC on Staphylococcus aureus in Hwangryunhaedoktang disappear all sample. 3. MIC on Staphylococcus aureus in Coptidis rhizoma was 100%, $50\;{\mu}l$ and anti-bacterial potency increase compare with quantity. Conclusions : The present author think that Soyum Herbal-acupuncture must be extracted a new method for anti-bacterial potency and Coptidis rhizoma was made Herbal-acupuncture for eye drops.

The Experimental Study on Anti-bacterial Potency of Hwangryunhaedoktang Herbal-acupuncture & extract on Staphylococcus aureus & Staphylococcus epidermidis (황련해독탕 약침액과 전탕액이 Staphylococcus aureus와 Staphylococcus epidermidis에 미치는 항균효과에 대한 실험적 연구)

  • Seo, Hyung-Sik
    • Journal of Pharmacopuncture
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    • v.9 no.2
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    • pp.99-103
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    • 2006
  • Objective : This experimental study was performed to investigate the effect of Hwangryunhaedoktang Herbal-acupuncture & extract on Staphylococcus aureus and Staphylococcus epidermidis that induce keratitis. Methods : MIC was measured by dropping to $50{\beta}^{\circ}$ according to density Hwangryunhaedoktang Herbal-acupuncture & extract(100%, 10%, 1%, 0.1%). Anti-bacterial potency was measured by the size of inhibition zone With change of volume. Results : 1. MIC on Staphylococcus aureus in Hwangryunhaedoktang Herbal-acupuncture & extract were not disappear all sample. 2. MIC on Staphylococcus epidermidis in Hwangryunhaedoktang Herbal-acupuncture & extract were not disappear all sample. Conclusions : The present author think that Hwangryunhaedoktang Herbal-acupuncture must be extract a new method for anti-bacterial potency.