• Title/Summary/Keyword: distillation control

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Antibacterial Activity of Essential Oils from Pinaceae Leaves Against Fish Pathogens (어병 세균에 대한 소나무과 잎 정유의 항세균 효과)

  • HAM, Youngseok;YANG, Jiyoon;CHOI, Won-Sil;AHN, Byoung-Jun;PARK, Mi-Jin
    • Journal of the Korean Wood Science and Technology
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    • v.48 no.4
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    • pp.527-547
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    • 2020
  • Fish pathogens cause not only economic damages to fish farming but also infectious pathogens known as a zoonotic agent. Since the continued use of antibiotics to control fish pathogens entails side effects, materials of natural origin need to be developed. The purpose of this study is to discover coniferous essential oils with excellent antibacterial effects in order to develop antibiotic alternatives. We have extracted essential oils using hydro-distillation from the leaves of Abies holophylla, Pinus thunbergii, Pinus parviflora, Tsuga sieboldii, and Pinus rigitaeda, which are all Pinaceae family. And, we have evaluated antibacterial activity with the extracted essential oils against Edwardsiella tarda, Photobacterium damselae, Streptococcus parauberis, and Lactococcus garvieae, which are fish pathogens. As a result, the essential oils from A. holophylla and P. thunbergii showed the selectively strong antibacterial activity against E. tarda and P. damselae, which are gram-negative bacteria. From GC-MS analysis, it was identified that main component of A. holophylla essential oils are (-)-bornyl acetate (29.45%), D-limonene (20.47%), and camphene (11.73%), and that of P. thunbergii essential oils is α-pinene (59.81%). In addition, we found three compounds: neryl acetate, (-)-borneol, and (-)-carveol, which are oxygenated monoterpenes. These exist in a very small amount but exhibit the same efficacy as essential oil. Therefore, we expect that A. holophylla and P. thunbergii essential oils having excellent growth inhibitory effect against gram-negative fish pathogens can be used as biological products such as feed additives and fishery products.

Volatile Components of Parsley Leaf and Seed (Petroselinum crispum) (파슬리의 잎과 씨의 휘발성 성분)

  • Kim, Young-Hoi;Kim, Kun-Soo;Hong, Chong-Ki
    • Applied Biological Chemistry
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    • v.33 no.1
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    • pp.62-67
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    • 1990
  • The volatile oils of the fresh leaf and seed of parsley(Petroselinum crispum) were isolated by simultaneous steam distillation and extraction procedure. The compositions of the resulting oils were investigated by gas chromatography and gas chromatography-mass spectrometry. The volatile oil contents of leaf and seed were 0.06 % and 3.11 %, respectively. Fifty-eight components including 15 partially characterized components were identified in leaf oil and 23 components in seed oil. Seven of them are suggested as new parsley leaf volatiles. Terpenoids were represented as much as 46.4 % of total leaf volatiles and 49.3 % of total seed volatiles. The leaf volatiles contained a lot of myrcene(3.02%), 4-isopropenyl-1-methyl benzene(4.52%) and p-1,3,8-menthatriene(10. 49 % ), but the seed volatiles were characterized by greater quantities of the isomers, ${\alpha}-pinene$(22.28 %) and ${\beta}-pinene$(16.20 %), although these compounds were contained only trace in leaf volatiles. Of the components identified in both oils, the most abundant component was myristicin, constituting 21.80 % of the leaf volatiles and 47.54 % of the seed volatiles.

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Effects of Hinokitiol Extract of Tunja orientalis on Shelf-life of Bread (측맥의 히노키티올 추출물이 식빵의 Shelf-life에 미치는 영향)

  • 강길진;짐정수
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.29 no.4
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    • pp.624-628
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    • 2000
  • Effects of hinokitiol extract Tunja orientalis [5 g/leaf (0.603 mg as hinokitiol), 50 g/leaf (6.03 mg as hinokitiol) and 10 g/prop distillation extract (1.378 mg as hinokitiol)] on shelf-life of bread were investigated. The contents of hinokitiol of leaf and prop and prop in tunja orientalis were 12.06 mg/100g and 13.78 mg/100 g. Added hinokitiol extract of Tunja orientalis on bread inhibited the growth of bacteria and fungi, and the more hinokitiol extract of Tunja orientalis was add, the higher degree of inhibition of those was observed. Results of sensory evaluation showed that there was no significant differ in each treatment and control (no add hinokitiol extract). These results suggest that the shelf-life of bread was extended by hinokitiol extract of Tunja orientalis.

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A Impact Study on Combustion Characteristics of the Engine by Changing the Gasoline Properties (휘발유 물성변화가 엔진의 연소특성에 미치는 영향 연구)

  • Noh, Kyeong-ha;Im, Sang-bin;Lee, Min-ho;Kim, Ki-ho;Ha, Jong-han
    • Journal of Energy Engineering
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    • v.24 no.4
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    • pp.166-174
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    • 2015
  • This study examined combustion characteristics by selecting the fuel which have a different physical properties compared to gasoline in order to examine the effects of vehicle performance and environment depending on the physical properties. The experiment examined the combustion characteristic in the optimum ignition timing according to the physical properties change and the lean burn by performing control about ignition timing and air-fuel ratio for each fuel, and it was also evaluated the exhaust gas according to the experiment. We used a single-cylinder engine for the experiment, and tested for gasoline properties change by selecting a fake fuel that beyond the fuel quality standards in 석대법. As a result, in the case of the selected fuel showed a difference in Octane and distillation characteristics, vapor pressure and it was also found to unstable combustion, and leads to a large amount of harmful exhaust gas.

Analysis of Volatile Compounds and Enantiomeric Separation of Chiral Compounds of Dried Sancho (Zanthoxylum schinifolium Siebold & Zucc)

  • Seo, Hye-Young;Shim, Sung-Lye;Ryu, Keun-Young;Jung, Min-Seok;Hwang, In-Min;Shin, Dong-Bin;Kwon, Joong-Ho;Schreier, Peter;Kim, Kyong-Su
    • Food Science and Biotechnology
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    • v.18 no.1
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    • pp.18-24
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    • 2009
  • The volatile compounds of dried sancho (Zanthoxylum schinifolium), an aromatic plant were extracted by simultaneous distillation and extraction (SDE) method and identified by gas chromatograph-mass spectrometry (GC-MS). Selected chiral constituents of sancho oil were characterized by enantiodifferentiation using multidimensional gas chromatograph (MDGC)-MS. A total of 57 compounds were identified and quantified, and the major compounds were identified estragole, nonanoic acid, octanoic acid, $\beta$-phellandrenene, and limonene. Among them, estragol (63.9%) was found as the predominantly abundant component of sancho. $\alpha$-pinene and nerolidol, and $\beta$-pinene and linalool were determined to be enantiomerically pure (100%) for their (S)-form and (R)-form, respectively. The enantiomeric composition of limonene in sancho revealed 83.9% purity for the (S)-enantiomer, whereas (E)- and (Z)-rose oxides showed mixtures of both enantiomers. The enantiomeric excess (%) for citronellal was 22.6% with the (R)-enantiomer as major enantiomer. The enantiomeric composition of these compounds can be used as parameter for authenticity control of sancho.

The Study on The Method of Manufacturing Herbal Acupuncture (약침액(藥鍼液) 제조법(製造法)에 대한 문헌적(文獻的) 고찰(考察))

  • Lee, Jun-Hee;Lee, Sang-Ryong
    • Korean Journal of Acupuncture
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    • v.22 no.2
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    • pp.127-149
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    • 2005
  • This study is designed to investigate the method of manufacturing herbal acupuncture through literature of oriental medicine. The findings of this study are as follows; 1. The methods of manufacturing herbal acupuncture go through the process of abstraction, purification, mixing, filtration, putting and tight sealing in the container, sterilization, quality control, printing and packing 2. There are many ways to manufacturing herbal acupuncture, for example water-alcohol precipitation, alcohol-water precipitation, liquid-liquid abstract, acid-base abstract, metal base precipitation, distillation, molecular structure, polyamide absorption, dialysis, and ion exchange, etc. And popular method is water-alcohol precipitation. This is through alcohol precipitate extracting the principal ingredients from water abstraction. This is very simple and efficient way using melting characteristics of compounds in herb to water and ethanol. 3. Sterilization of herbal acupuncture is through heating-pressure, boiling, steam flowing, low temperature, filtering, radiation, cooling, and microwaves. Nowadays filtering is commonly used. And sterilization is estimated by an examination of asepsis . 4. Herbal acupuncture must be undergo study and experiment to clinical use. The problems of herbal acupuncture are turbidity, instability, causing hemolysis, pain, and fever. So many provisions (addition, sterilization, and filtration etc.) must be prepared. 5. The theory of manufacturing herbal acupuncture is from oriental medicine, not western. So it must be corresponded to oriental medical theory, for example Gimi(氣味), Guigyung(歸經), Ingyung(引經), Bosa(補瀉), and Match of Herb. It is recommended that further study of many other sided investigations in the future.

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Utilization of Essential Oil Free Needles for Compost and Roughage (침엽정유추출잔사의 퇴비화 및 조사료 이용)

  • 최인규;강하영
    • Journal of Korea Foresty Energy
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    • v.21 no.1
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    • pp.7-15
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    • 2002
  • The essential oil free needles, which were left after distillation of essential oil from various coniferous needles, were fermented with food waste organics in order to use as compost and roughage. Microorganisms for the fermentation were selected from domestic sources such as swine compost, bark compost, and kimchi, etc, and consisted of aerothermophilic bacteria and actinomycetes. The weight reduction ratio of food waste organics treated with the microorganisms was 90% after 30 days treatment, and the fermentation temperature was kept at approximately $45^{\circ}C$. The compost process was really slow due to chemical compounds derived from needles, and it finally took 60 days for complete compost. When 10% of needle compost was mixed with soil for radish growth, the growth indicators such as leaf length and root weight were increased compared with control, while root weight, root width, and root length were inhibited on the addition of 20% needle compost. The nutrient value and digestibility ratio of various essential oil free needles as roughage for ruminant animals were evaluated. The ratio of crude protein for essential oil free needles from Korean pine(Pinus koraiensis) was 10.02%, which was higher than those of rice straw(5.48%) and corn(9.00%). The digestibility ratios of essential oil free needles from Sawara cypress(Chamaecwaris pislfera), Korean pine(Pinus koraiensis), and Japanese Red Pine(Pinus densiflora) was 53%, 34%, 34%, respectively, indicating that those essential oil free needles were considered as excellent roughage.

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A Study on the Frequency Control on the Induction Heating System Using Two Step Resonant Inverter (공진형 인버터를 이용한 2단 유도가열 시스템의 주파수제어에 관한 연구)

  • Yoo, Jae-Hoon;Shin, Dae-Cheul
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.22 no.1
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    • pp.95-103
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    • 2008
  • Proposed induction-heated system is innovative system which applied special high-frequency power circuit technique for thermal converse technique and IH(Induction-Heating) magnetic induction heating generated from induction-heated metallic package that is for distillation unit. In this occurs not burning, so that the working environment can be improved. This electromagnetic induction heating technique is used high frequency inverter. By using high frequency inverter high frequency alternative current (HFAC) in the range of [kHz] can be made with conventional alternative current. In this contribution IGBT module is used for high frequency inverter. In this paper are discussed action analysis and characteristics analysis of 1.5[kW]-Class half-bridge resonant inverter system and resonant metallic package. In addition, by using this system, how two step heating superheated steam generator is developed and application of system are also discussed.

Corrosion and Materials Selection for Bitumen with Heavy Naphthenic Acid in Canadian Oil Sands

  • Eun, Thomas Jung-Chul
    • Corrosion Science and Technology
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    • v.7 no.6
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    • pp.350-361
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    • 2008
  • Canada's oil sands contain one of the largest reserves of oil in the world. According to recent estimates, there are nearly 180 billion barrels of oil in the Canadian oil sands trapped in a complex mixture of sand, water and clay. More than 40 companies have been currently operating or developing oil sands facilities since the first production in 1967. The process of oil sands upgrading is similar with down stream refinery, but the corrosion environment in upgrading refinery is often more severe than in the refinery because of high chlorides, mineral contents, carbonic acid, heavy viscosity and fouling, higher naphthenic acid [$NA-R(CH_{2})nCOOH$], and greater sulfur contents. Naphthenic acid corrosion (NAC) which is one of the most critical corrosion issues in up & downstream refinery plants was observed for the first time in 1920's in refinery distillation processes of Rumania, Azerbaizan (Baku), Venezuela, and California. As a first API report, the 11th annual meeting stated sources and mechanism of NAC in early 1930's. API has been developing the risk base standards, such as API RP580, 571, and Publication 581 which are based on the worst NAC damage in the world since 2000. Nevertheless not only the NAC phenomena and control in Canadian sands oil process are not much widely known but also there are still no engineering guidances for the Canadian sands oil in API standards. This paper will give NAC phenomina and materials selection guidance against NA environment in Canadian oil sands upgrading processes.

Effects of Aromatics and T90 Temperature of Low Cetane Number Fuels on Exhaust Emissions in Low-Temperature Diesel Combustion (저온디젤연소에서 저세탄가 연료의 방향족 및 T90 온도가 배기가스에 미치는 영향)

  • Han, Man-Bae
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.34 no.12
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    • pp.1121-1126
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    • 2010
  • This study is to investigate the effects of aromatics and T90 for low cetane number (CN) fuels on combustion and exhaust emissions in low-temperature diesel combustion. We use a 1.9-L common rail direct injection diesel engine at 1500 rpm and 2.6 bar BMEP. Low temperature diesel combustion was achieved via a high external EGR rate and strategic injection control. The tested fuels four sets: the aromatic content was 20% (A20) or 45% (A45) and the T90 temperature was $270^{\circ}C$ (T270) or $340^{\circ}C$ (T340) with CN 30. Given the engine operating conditions, the T90 was the stronger factor on the ignition delay time, resulting in a longer ignition delay time for higher T90 fuels. All the fuels produced nearly zero PM because of the extension of the ignition delay time induced by the low cetane number. The aromatic content was the main factor that affected the NOx and the NOx increased with the aromatic content.