• Title/Summary/Keyword: dispersion method

검색결과 1,631건 처리시간 0.035초

실란처리를 통한 안정화된 $TiO_2$졸의 합성 (Synthesis of stabilized $TiO_2$ sol by sillane treatment)

  • 한동희;강동준;김락희;강동필
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
    • /
    • pp.234-235
    • /
    • 2007
  • Transparent nanosized $TiO_2$ sol has been made by sol-gel method, using Titanium(IV) isopropoxide precursor. To promote hydrolysis for titania is needed excess water, Oil bath and temperature about $80^{\circ}C$. $TiO_2$ sol is peptized ranging from pH 1 to 1.5 using hydrochloric acid for the stability of sol during a condensation reaction. The average particle size of $TiO_2$ sol was approximately 20nm. $TiO_2$-sillane sol was synthesized by surface treatment using MTMS to the $TiO_2$ sol. TEM analysis has been used to check the degree of dispersion and FT-IR analysis has been used to see if the sillane has been chemically bonded on the surface of $TiO_2$.

  • PDF

고밀도 폴리에틸렌에 있어서 전계의 세기의 영향 (Pigment Influence in High Density Polyethylene Electrical Strength)

  • 윤주호;최용성;문종대;이경섭
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2007년도 추계학술대회 논문집
    • /
    • pp.331-332
    • /
    • 2007
  • In this work, the TiO2 pigment influence in HDPE dielectric strength was analyzed. Chemical and structural characterizations were made to identify changes during the processing and your influence in the electrical properties, formulations containing 0, 0.5, 1, 2.5, 4 and 6 of titanium dioxide were processed by extrusion and injection molding with stabilization-antioxidants, ultraviolet stabilizers and plasticizers. The electrical strength tests were analyzed by the statistical distribution of Weibull, and the maximum likelihood method. The high concentrations present lower values to electrical strength. The parameter could be using to insulator panicles dispersion. The TiO2 concentration variation shows that these incorporations implicate strength values increase has a maximum (5,35MV/cm). High pigment concentration induces a little falls in property values. Observing the parameter, minimum experiment electric field (Ebmin) and electric strength value, found that the best electric perform formulation was the formulation with 2.5% TiO2 weight.

  • PDF

고밀도 폴리에틸렌의 전계 세기의 영향에 관한 연구 동향 (A Research Trend on High Density Polyethylene Electrical Strength)

  • 윤희광;김찬호;허인호;이정수;황종선;최용성;이경섭
    • 대한전기학회:학술대회논문집
    • /
    • 대한전기학회 2007년도 제38회 하계학술대회
    • /
    • pp.1982-1983
    • /
    • 2007
  • In this work, the $TiO_2$ pigment influence in HDPE dielectric strength was analyzed. Chemical and structural characterizations were made to identify changes during the processing and your influence in the electrical properties. Formulations containing 0, 0.5, 1, 2.5, 4 and 6 of titanium dioxide were processed by extrusion and injection molding with stabilization-antioxidants, ultraviolet stabilizers and plasticizers. The electrical strength tests were analyzed by the statistical distribution of Weibull, and the maximum likelihood method. The high concentrations present lower values to electrical strength. The ${\beta}$ parameter could be using to insulator particles dispersion. The TiO2 concentration variation shows that these incorporations implicate strength values increase has a maximum (5,35MV/cm). High pigment concentration induces a little falls in property values. Observing the ${\beta}$ parameter, minimum experiment electric field (Ebmin) and electric strength value, found that the best electric perform formulation was the formulation with 2.5% TiO2 weight.

  • PDF

음향방출신호에 대한 이산웨이블릿 변환기법의 적용 (Application of Technique Discrete Wavelet Transform for Acoustic Emission Signals)

  • 박재준;김면수;김민수;김진승;백관현;송영철;김성홍;권동진
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
    • /
    • pp.585-591
    • /
    • 2000
  • The wavelet transform is the most recent technique for processing signals with time-varying spectra. In this paper, the wavelet transform is utilized to improved the assessment and multi-resolution analysis of acoustic emission signals generating in partial discharge. This paper especially deals with the assessment of process statistical parameter using the features extracted from the wavelet coefficients of measured acoustic emission signals in case of applied voltage 20[kv]. Since the parameter assessment using all wavelet coefficients will often turn out leads to inefficient or inaccurate results, we selected that level-3 stage of multi decomposition in discrete wavelet transform. We applied FIR(Finite Impulse Response)digital filter algorithm in discrete to suppression for random noise. The white noise be included high frequency component denoised as decomposition of discrete wavelet transform level-3. We make use of the feature extraction parameter namely, maximum value of acoustic emission signal, average value, dispersion, skewness, kurtosis, etc. The effectiveness of this new method has been verified on ability a diagnosis transformer go through feature extraction in stage of acting(the early period, the last period) .

  • PDF

4H 탄화규소 쇼트키 다이오드에서 접합종단기법에 따른 항복전압특성 (Reverse voltage characteristics of 4H SiC Schottky Diode by Edge termination Method)

  • 정희종;방욱;강인호;김상철;한현숙;김남균;이용재
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
    • /
    • pp.191-192
    • /
    • 2005
  • The reverse breakdown voltages of 4H-SiC SBD(schottky barrier diode)s with FP(Field Plate) and/or FLR(Field Limiting Ring) as a edge termination, were investigated. The breakdown voltages of SBDs with FP ware investigated varying the overlap width from $1{\mu}m$ to $30{\mu}m$. The maximum average breakdown voltages was 475V. There is no significant changes for the devices with overlap width of between $5{\mu}m\sim30{\mu}m$. It was confirmed that the dielectric breakdown of the thin thermal oxide is main cause of device failure. However, the breakdown voltage of SBD with FLR was 1400V even though the FLR edge termination structure was not optimized.

  • PDF

Si-N 전구체를 이용한 에폭시/실리카 나노복합재료의 제조 (Novel Preparation of Epoxy/Silica Nanocomposite Using Si-N Precursor)

  • 김이주;윤호규;이상수;김준경
    • 폴리머
    • /
    • 제28권5호
    • /
    • pp.391-396
    • /
    • 2004
  • 기존의 에폭시/실리카 나노복합재료의 제조 방법에서 나타나는 문제점인 경화 반응 중의 휘발성 부산물 생성에 의한 미세기공 형성 및 치수 불안전성 등을 극복하고자 Si-N 전구체를 사용한 새로운 방법을 제안하고자 한다. 실리카 전구체로 부산물이 형성되지 않는 메틸트리페닐실란 (MTPS)을 합성하고 이를 이용하여 솔-젤 반응과 에폭시 경화 반응이 병행되는 동시 복합화 반응을 통하여 무기상의 고른 분산상태를 지닌 에폭시/실리카 나노복합재료를 제조하였으며, 이로부터 뛰어난 투명성뿐 아니라 기계적 물성과 열적특성에서 탁월한 물성의 증가를 얻을 수 있었다.

QUAL II 모형의 금강수계에의 적용 (An Application of the QUAL II Model to the Keum River System)

  • 최흥식;이길성
    • 한국수자원학회:학술대회논문집
    • /
    • 한국수자원학회 1987년도 제29회 수공학연구발표회논문초록집
    • /
    • pp.159-168
    • /
    • 1987
  • 하용에서 수질 시뮬레이숀에 의한 시간적, 공간적 수질예측은 하용 수질관리를 위한 계획수립, 설계 및 모형의 최적화에 필요한 자료를 제공해 준다. 본 연구는 대청댐 하류에서 부여백제대교에 이르는 금강수계에서의 QUAL II 모형의 적용에 관한 것이다. QUAL II모형에서 사용된 물질수지방정식에 근거를 둔 대류-분석모형과 그 수치해석법을 제시하였다. 하용을 따르는 BOD, DO 및 수온의시뮬레이숀괍과 실측값과의 비교분석을 통한 모형의 활용성 제고에 역점을 두었다. 이러한 과정을 통해 금강에서의 하용수질을 평가하고, 탈산소 계수, 재폭기 계수 및 자정계수의 값을 추정하였다. 또한 대청댐 방류량 조절에 의한 목표하는 DO의 유지에 대하여 논의하였다.

  • PDF

Analysis of Statistical Methods Currently used in Toxicology Journals

  • Na, Jihye;Yang, Hyeri;Bae, SeungJin;Lim, Kyung-Min
    • Toxicological Research
    • /
    • 제30권3호
    • /
    • pp.185-191
    • /
    • 2014
  • Statistical methods are frequently used in toxicology, yet it is not clear whether the methods employed by the studies are used consistently and conducted based on sound statistical grounds. The purpose of this paper is to describe statistical methods used in top toxicology journals. More specifically, we sampled 30 papers published in 2014 from Toxicology and Applied Pharmacology, Archives of Toxicology, and Toxicological Science and described methodologies used to provide descriptive and inferential statistics. One hundred thirteen endpoints were observed in those 30 papers, and most studies had sample size less than 10, with the median and the mode being 6 and 3 & 6, respectively. Mean (105/113, 93%) was dominantly used to measure central tendency, and standard error of the mean (64/113, 57%) and standard deviation (39/113, 34%) were used to measure dispersion, while few studies provide justifications regarding why the methods being selected. Inferential statistics were frequently conducted (93/113, 82%), with one-way ANOVA being most popular (52/93, 56%), yet few studies conducted either normality or equal variance test. These results suggest that more consistent and appropriate use of statistical method is necessary which may enhance the role of toxicology in public health.

Computations of Droplet Impingement on Airfoils in Two-Phase Flow

  • Kim, Sang-Dug;Song, Dong-Joo
    • Journal of Mechanical Science and Technology
    • /
    • 제19권12호
    • /
    • pp.2312-2320
    • /
    • 2005
  • The aerodynamic effects of leading-edge accretion can raise important safety concerns since the formulation of ice causes severe degradation in aerodynamic performance as compared with the clean airfoil. The objective of this study is to develop a numerical simulation strategy for predicting the particle trajectory around an MS-0317 airfoil in the test section of the NASA Glenn Icing Research Tunnel and to investigate the impingement characteristics of droplets on the airfoil surface. In particular, predictions of the mean velocity and turbulence diffusion using turbulent flow solver and Continuous Random Walk method were desired throughout this flow domain in order to investigate droplet dispersion. The collection efficiency distributions over the airfoil surface in simulations with different numbers of droplets, various integration time-steps and particle sizes were compared with experimental data. The large droplet impingement data indicated the trends in impingement characteristics with respect to particle size ; the maximum collection efficiency located at the upper surface near the leading edge, and the maximum value and total collection efficiency were increased as the particle size was increased. The extent of the area impinged on by particles also increased with the increment of the particle size, which is similar as compared with experimental data.

Cpk Index Estimation under Tw (the weakest t-norm)-based Fuzzy Arithmetic Operations

  • Hong, Dug-Hun
    • International Journal of Fuzzy Logic and Intelligent Systems
    • /
    • 제8권3호
    • /
    • pp.170-174
    • /
    • 2008
  • The measurement of performance of a process considering both the location and the dispersion of information about the process is referred to as the process capacity indices (PCIs) of interest, $C_{pk}$. This information is presented by the mean and standard deviation of the producing process. Linguistic variables are used to express the evaluation of the quality of a product. Consequently, $C_{pk}$ is defined with fuzzy numbers. Lee [Eur. J. Oper. Res. 129(2001) 683-688] constructed the definition of the $C_{pk}$ index estimation presented by fuzzy numbers and approximated its membership function using the "min" - norm based Zadeh's extension principle of fuzzy sets. However, Lee's result was shown to be invalid by Hong [Eur. J. Oper. Res. 158(2004) 529-532]. It is well known that $T_w$ (the weakest t-norm)-based addition and multiplication preserve the shape of L-R fuzzy numbers. In this paper, we allow that the fuzzy numbers are of L-R type. The object of the present study is to propose a new method to calculate the $C_{pk}$ index under $T_w-based$ fuzzy arithmetic operations.