• Title/Summary/Keyword: deposit stress

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The Change in Residual Stress of Electroless Nickel Deposits on Aluminum Substrate (Al 소지상에 무전해 Ni도금시 응력 변화)

  • 권진수;최순돈
    • Journal of the Korean institute of surface engineering
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    • v.29 no.2
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    • pp.100-108
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    • 1996
  • The internal stress of acidic electroless nickel deposits on zincated aluminum was determined by spiral contractometer. Several plating conditions such as inhibitor and complexing agent concentrations and pH affecting the internal stress were studied. The resulting intrinsic stress contribution to the total stress was discussed in terms of phosphorous content of the deposit, solution pH, and surface morphology. However, the most important was found to be thermal stress for the total stress of Al substrate, because of high thermal expansion coefficient of the aluminum substrate.

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The Effects of Additives and Residual Stresses on the Electroless Nickel Plating on Carbon Substrate (첨가제와 잔류응력이 탄소 기지상 무전해 니켈도금에 미치는 영향)

  • Cheon, So-Young;Rhym, Young-Mok;Lee, Jae-Ho
    • Journal of the Microelectronics and Packaging Society
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    • v.18 no.4
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    • pp.43-48
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    • 2011
  • Electroless nickel platings on carbon substrate were investigated for porous MCFC electrode applications. Acidic bath and alkaline bath were used in electroless nickel plating on carbon substrates. The rate of electroless plating in alkaline bath was faster than that in acidic bath. As pH was increased, the deposition rate was increased in both baths and the content of phosphorus in nickel deposit was decreased. The residual stresses of nickel deposit from acidic bath showed the compressive stress and on the other hand those from alkaline bath showed the high tensile stress. High tensile internal stress in nickel deposit caused the cracks over pH 11. Thiourea was added to both acidic and alkaline bath. The deposition rate of nickel was increased upto 0.5 ppm of thiourea and decreased. The maximum concentration of thiourea for the electroless nickel plating on carbon substrate was 1.5 ppm in both acidic and alkaline bath. Succinic acid was added to acidic bath. Addition of succinic acid up to 5 g/L increased the deposition rate of nickel and beyond which the deposition rate was decreased and maintained.

The Principle and Practice of pulse Plating (펄스도금의 원리와 기술)

  • 김종상;송락현;변수일
    • Journal of the Korean institute of surface engineering
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    • v.21 no.1
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    • pp.19-27
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    • 1988
  • The principe and practice of pulse plating, and prospect in the future on pulse plating are reviewed. Some of the advantages of pulse pulse plating are detailed as compared with DC plating. The advantages of pulse plating are summarized as follows: 1)smooth and fine grained deposits 2) reduction in hydrogen embrittlement of deposits 3) reduction of residual stress and microcracks in the deposit 4) improvement of physical properties 5) uniform alloy composition through the deposit thinkness 6) improved thrower and adhesion.

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Alleviating Deformation of MEMS Structure in Surface Micromachining (표면미세가공시 발생하는 MEMS 구조물의 변형 억제)

  • Hong Seok-Kwan;Kweon Soon-Cheol;Jeon Byung-Hee;Shin Hyung-Jae
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.8 s.185
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    • pp.163-170
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    • 2006
  • By removing sacrificial layer through ashing process, movable MEMS structure on substrate can be fabricated in surface micromachining. However, MEMS structure includes, during the ashing process, the warping or buckling effects due to stress gradient along the vertical direction of thin film. In this study, we presented method for counteracting the unwanted deflection of MEMS structure and designed using character of deposit process to overcome limited design conditions. Unit cell patterns were designed with character of deposit shape, and their final shapes were adopted using Finite Element Method. Finally, RF MEMS switch was fabricated by surface micro machining as test vehicles. We checked out that alleviation effect for deformation of switch improved by 35%.

A study on adhesion strength of electroless plated deposits on Alumina substrate (Alumina substrate 상의 무전해 도금층의 밀착력에 관한 연구)

  • 조용균;안균영;박용수
    • Journal of the Korean institute of surface engineering
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    • v.24 no.4
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    • pp.187-195
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    • 1991
  • Adhesion strength of electroless-plated Ni, Ni-P and Cu deposites on alumina substrate has been studied. Grain boundary spaces produced on the substrate surface by etching treatment provided anchoring sites for enhancing the adhesion strength. Adhesion strengths of Ni-P and Ni deposit were higher than that of Cu deposit, because of higher initial nucleation rates than the latter. The electroless-plated Ni-P and Ni underlayer improved the adhesion strength of the Cu deposit. In could be attributed to the enhanced adhesion between the substrate and those underlayers as well as the satisfactory adhesion between Cu deposits and those underlayers. Heat treatment was also conducted in order to enhance the adhesion strength of Cu layer. The strength was enhanced by about 19% when the treatment was conducted at $150^{\circ}C$ for 2 hours. The enhancement was attributed to relief of internal stress and release of hydrogen.

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DETECTION OF ODSCC IN SG TUBES DEPENDING ON THE SIZE OF THE CRACK AND ON THE PRESENCE OF SLUDGE DEPOSITS

  • Chung, Hansub;Kim, Hong-Deok;Kang, Yong-Seok;Lee, Jae-Gon;Nam, Minwoo
    • Nuclear Engineering and Technology
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    • v.46 no.6
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    • pp.869-874
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    • 2014
  • It was discovered in a Korean PWR that an extensive number of very short and shallow cracks in the SG tubes were undetectable by eddy current in-service-inspection because of the masking effect of sludge deposits. Axial stress corrosion cracks at the outside diameter of the steam generator tubes near the line contacts with the tube support plates are the major concern among the six identical Korean nuclear power plants having CE-type steam generators with Alloy 600 high temperature mill annealed tubes, HU3&4 and HB3~6. The tubes in HB3&4 have a less susceptible microstructure so that the onset of ODSCC was substantially delayed compared to HU3&4 whose tubes are most susceptible to ODSCC among the six units. The numbers of cracks detected by the eddy current inspection jumped drastically after the steam generators of HB4 were chemically cleaned. The purpose of the chemical cleaning was to mitigate stress corrosion cracking by removing the heavy sludge deposit, since a corrosive environment is formed in the occluded region under the sludge deposit. SGCC also enhances the detection capability of the eddy current inspection at the same time. Measurement of the size of each crack using the motorized rotating pancake coil probe indicated that the cracks in HB4 were shorter and substantially shallower than the cracks in HU3&4. It is believed that the cracks were shorter and shallower because the microstructure of the tubes in HB4 is less susceptible to ODSCC. It was readily understood from the size distribution of the cracks and the quantitative information available on the probability of detection that most cracks in HB4 had been undetected until the steam generators were chemically cleaned.

A Study on a Compression Index for Settlement Analysis of SCP Treated Ground Using Back Analysis (역해석을 이용한 모래다짐말뚝(SCP)으로 개량된 연약점토지반의 압축지수 결정에 관한 연구)

  • Hwang, Sungpil;Im, Jongchul;Kwon, Jeonggeun;Kang, Yeounike;Joo, Ingon
    • Journal of the Korean GEO-environmental Society
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    • v.11 no.7
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    • pp.5-14
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    • 2010
  • The paper processed settlement analysis using Finite Elements Method(FEM). Because Stress Distribution Ratio has to be decreased, for settlement analysis of soft clay deposit improved by sand compaction piles(SCP). Back analysis was processed comparing the measured settlements of laboratory model tests and finite element analysis where the SCP treated area was assumed as mixed ground with clay deposit rather than being a composite ground. The paper proposes a methodology which employs a compression index($C_c$) for settlement analysis of soft clay deposit improved by sand compaction piles from the back analysis. This approach is applied to a field measurement case(A revetment founded on the SCP improved clay deposit with the replacement ratio of 45%).

Chinese buffer material for high-level radiawaste disposal --Basic features of GMZ-l

  • WEN Zhijian
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2005.11b
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    • pp.236-244
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    • 2005
  • Radioactive wastes arising from a wide range of human activities are in many different physical and chemical forms, contaminated with varying radioactivity. Their common feature is the potential hazard associated with their radioactivity and the need to manage them in such a way as to protect the human environment. The geological disposal is regarded as the most reasonable and effective way to safely disposal high-level radioactive wastes in the world. The conceptual model of geological disposal in China is based on a multi-barrier system that combines an isolating geological environment with an engineered barrier system. The buffer is one of the main engineered barriers for HLW repository. The buffer material is expected to maintain its low water permeability, self-sealing property, radio nuclides adsorption and retardation property, thermal conductivity, chemical buffering property, overpack supporting property, stress buffering property over a long period of time. Benotite is selected as the main content of buffer material that can satisfy above. GMZ deposit is selected as the candidate supplier for Chinese buffer material of High Level Radioactive waste repository. This paper presents geological features of GMZ deposit and basic property of GMZ Na bentonite. GMZ bentonite deposit is a super large scale deposits with high content of Montmorillonite (about $75\%$) and GMZ-l, which is Na-bentonite produced from GMZ deposit is selected as reference material for Chinese buffer material study.

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An experimental procedure for evaluating the consolidation state of marine clay deposits using shear wave velocity

  • Chang, Ilhan;Kwon, Tae-Hyuk;Cho, Gye-Chun
    • Smart Structures and Systems
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    • v.7 no.4
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    • pp.289-302
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    • 2011
  • In marine clay deposits, naturally formed or artificially reclaimed, the evaluation and monitoring of the consolidation process has been a critical issue in civil engineering practices due to the time frame required for completing the consolidation process, which range from several days to several years. While complementing the conventional iconographic method suggested by Casagrande and recently developed in-situ techniques that measure the shear wave, this study suggests an alternative experimental procedure that can be used to evaluate the consolidation state of marine clay deposits using the shear wave velocity. A laboratory consolidation testing apparatus was implemented with bimorph-type piezoelectric bender elements to determine the effective stress-shear wave velocity (${\sigma}^{\prime}-V_s$) relationship with the marine clays of interest. The in-situ consolidation state was then evaluated by comparing the in-situ shear wave velocity data with the effective stress-shear wave velocity relationships obtained from laboratory experiments. The suggested methodology was applied and verified at three different sites in South Korea, i.e., a foreshore site in Incheon, a submarine deposit in Busan, and an estuary delta deposit in Busan. It is found that the shear wave-based experimental procedure presented in this paper can be effectively and reliably used to evaluate the consolidation state of marine clay deposits.

Bearing Capacity Evaluation of Marine Clay Dredged Deposit Including Desiccated Crust Layer (건조 고결층이 형성된 준설 매립 지반의 지지력 산정에 대한 연구)

  • Park, Hyun-Ku;Byeon, Wi-Yong;Jee, Sung-Hyun;Lee, Seung-Rae
    • Journal of the Korean Geotechnical Society
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    • v.23 no.5
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    • pp.89-100
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    • 2007
  • In this study, various field and laboratory tests were performed to investigate the characteristics of shear strength and bearing behavior to be considered in the estimation of stability and trafficability in early stage of stabilization process in marine clay dredged deposit. Site characterization was carried out to grasp the basic properties of the deposit. Field vane test, unconfined compression test and direct shear test were conducted to evaluate the shear strength distribution for varied depths, and the characteristics of shear strength and stress-strain behavior of the crust layer. Plate load tests were also performed to estimate the bearing capacity and to assess load-settlement behavior and failure pattern of the deposit. The bearing capacity was also estimated using previously proposed methods for double-layered clay deposit. The estimated bearing capacity was compared with the results of the plate load tests and then, the applicability of the estimation method was discussed.