• 제목/요약/키워드: dental resin

검색결과 1,266건 처리시간 0.03초

Benzalkonium Chloride가 NTG-GMA/BPDM계 및 DSDM계 상아질접착제의 접착성능에 미치는 영향 (EFFECT OF BENZALKONIUM CHLORIDE ON DENTIN BONDING WITH NTG-GMA/BPDM AND DSDM SYSTEM)

  • 신일;박진훈
    • Restorative Dentistry and Endodontics
    • /
    • 제20권2호
    • /
    • pp.699-720
    • /
    • 1995
  • 본 연구는 양이온 계면활성효과를 가져 소독제로 사용되고 있는 benzalkonium chloride 수용액을 상아질 표면에 대한 습윤용 처리제로 적용시킬 경우 상아질접착제의 접착성능에 미치는 영향을 관찰하기 위해 시행되었다. 소의 하악전치 80개를 8개군으로 분류하여 순면의 상아질을 노출시켜서 산처리한 후 물로 습윤 상태를 유지시킨 대조군과 0.1%, 0.5% 및 1% 농도의 benzalkonium chloride 수용액으로 습윤시킨 실험군으로 나누어 NTG-GMA/BPDM계 상아질접착제인 All-bond 2와 DSDM 계 상아질접착제인 Aelitebond를 각각 접착시킨 후 접착시험을 시행하였다. 상아질 표면을 10% 인산수용액으로 처리한 후 습윤과정을 거친 시편을 각 접착시스템의 primer와 bonding resin을 도포하고 Aelitefil 복합레진으로 접 착시 킨후 항온조에서 24시간 방치한 뒤 인장접착강도를 측정하고, 상아질표면 및 파단면의 양상을 주사전자 현미경으로 관찰하였으며 FT-IR을 사용하여 전처리 전후의 상아질 표면을 분석하여 다음의 결과를 얻었다. 1. NTG-GMA/BPDM 계 상아질접착제 (All-bond 2)로 접착시킨 경우 물로 습윤시킨 대조군에 비해 0.1 % benzalkonium chloride 수용액으로 습윤시킨 군에서 유의하게 높은 인장접착강도를 보였으나(p<0.05), 0.5% 및 1.0 % benzalkonium chloride 수용액으로 습윤시킨 군에서는 유의한 차이가 나타나지 않았다. 2. DSDM계 상아질접착제 (Aelitebond) 로 접착시킨 경우 물로 습윤시킨 대조군과 0.1 %, 0.5% 및 1.0 % benzalkonium chloride 수용액으로 습융시킨 군 간의 인장접착강도의 유의한 차이는 없었다(p>0.05). 3. Benzalkonium chloride 수용액의 적용과 관계 없이 전체적으로 NTG-GMA/ BPDM계 상아질접착제로 접착시킨 경우가 DSDM계 상아질접착제로 접착시킨 경우보다 인장접착강도가 높았으며, 파단양상의 관찰결과에서도 NTG-GMA /BPDM계 상아질접착제를 사용한 경우는 응집성 및 혼합성 파단양상이, DSDM 계 상아질접착제를 사용한 경우는 부착성 파단양상이 우세하였다. 4. 주사전자 현미경적 관찰상에서 benzalkonium chloride 수용액 적용 유무에 따른 각 상아질 표면의 primer 도포양상의 뚜렷한 차이는 관찰되지 않았으나, 상아질 표면에 대한 benzalkonium chloride 수용액 적용 전후의 FT-IR 분석결과 에서는 0.1 % benzalkonium chloride 수용액으로 습윤 처리 시킨 군이 대조군에 비해 NTG-GMA/ BPDM 및 DSDM primer의 도포효과를 다소 향상시킨 소견이었다.

  • PDF

여러 복합레진에서 수분 흡수에 의한 색변화에 연마가 미치는 영향 (Effect of polishing methods on color change by water absorption in several composite resins)

  • 김혜진;김미연;송병철;김선호;김정희
    • 구강회복응용과학지
    • /
    • 제35권1호
    • /
    • pp.1-10
    • /
    • 2019
  • 목적: 복합레진의 색조안정성에 있어서 연마가 영향을 주는지 알아보았다. 연구 재료 및 방법: 2 개의 벌크필 레진과 4개의 복합레진을 6 mm 너비, 4 mm 높이로 제작하여 광중합한 후 $34^{\circ}C$ 멸균 증류수에 24 시간 보관하고 분광광도계를 이용하여 CIE $L^*a^*b^*$ 값을 측정하였다. 시편을 연마 방법에 따라 대조군(Mylar strip 그룹), PoGo로 연마한 그룹, Sof-Lex Spiral wheels로 연마한 그룹으로 나누었다(n = 5). 색측정은 4 주 동안 매주 시행하였고 실험 기간 동안 시편은 $34^{\circ}C$ 멸균증류수에 보관하였다. 실험결과는 일반최소자승법으로 통계분석하였다(P < 0.05). 결과: 일반최소자승법 분석에 따르면 Sof-Lex Spiral wheels로 연마한 그룹의 ${\Delta}E$ 값이 PoGo로 연마한 그룹과 대조군의 ${\Delta}E$ 값보다 낮게 나타났다(P < 0.05). 복합레진을 연마한 그룹의 ${\Delta}E$ 값은 연마하지 않은 대조군의 ${\Delta}E$ 값보다 낮게 나타났다(P < 0.05). 복합레진 비교시 Filtek Z250과 Filtek Z350 XT Universal restorative는 모든 기간에서 통계적 차이가 나타나지 않았으며 Tetric N-Ceram Bulk Fill은 1, 2, 3주에서 통계적으로 낮은 ${\Delta}E$ 값을 나타냈다(P < 0.05). 결론: 이번 연구의 한계점을 감안하면 연마 방법은 복합레진의 색조안정성에 영향을 미친다. Sof-Lex Spiral wheels로 연마한 그룹이 PoGo로 연마한 그룹보다 변색에 더 큰 저항을 보여주었다.

지르코니아-전장도재 계면의 전단결합강도에 대한 ZirLiner® 적용과 분사처리의 영향에 관한 연구 (Effect of Application of ZirLiner® and Blasting Treatments on Shear Bond Strength of Zirconia-Veneered Porcelain Interface)

  • 신영호;이유나;이해형;동진근;오상천
    • 구강회복응용과학지
    • /
    • 제24권1호
    • /
    • pp.113-127
    • /
    • 2008
  • 이 연구의 목적은 지르코니아 도재 표면의 전단 결합 강도에서 $ZirLiner^{(R)}$와 블라스팅 처리의 적용 효과를 평가하기 위한 것이다. 60개의 무색의 지르코니아 판과 30개의 색이 있는 지르코니아 판이 규격화되고 연마, 글래스블라스팅, 알루미나블라스팅, 그리고 zirliner 같은 블라스팅 처리를 적용시키는 것에 따라 10개씩 9개의 그룹으로 나누어졌다. 시편을 고정대에 위치하고 만능시험기로 전단력을 측정하였다. 파절된 견본의 파절 표면은 SEM으로 검사되었다. 각 군별 시편을 통계처리하여 그 결과를 비교하였다.

미세입자 분사마모 표면처리가 Fiber-Reinforced Composite 포스트의 굴곡 강도에 미치는 영향 (Influence of airborne-particle abrasion on flexural strength of fiber-reinforced composite post)

  • 심은주;김진우;조경모;박세희
    • 구강회복응용과학지
    • /
    • 제32권1호
    • /
    • pp.24-31
    • /
    • 2016
  • 목적: 미세입자 분사마모 표면처리가 Fiber-Reinforced Composite (FRC) 포스트의 굴곡강도에 미치는 영향을 평가하는 것이다. 연구 재료 및 방법: 두 종류의 FRC 포스트 (DT Light Post, Size 2, Bisco Inc. / RelyX Fiber Post, Size 3, 3M ESPE)를 사용하여 표면처리에 따라 6개의 그룹으로 무작위 분류하였다. 표면처리를 위해 $30{\mu}m$ Rocatec Soft와 $50{\mu}m$ aluminum oxide를 사용하였다. 표면처리 후 편평한 5 mm 부분을 만능시험기로 3점 굽힘시험을 시행하여 FRC 포스트의 굴곡강도와 굴곡계수를 측정하고 통계분석하였다. 결과: FRC포스트의 미세입자 분사마모 표면처리가 FRC포스트의 굴곡강도와 굴곡계수에는 영향을 미치지 않음을 알 수 있었다. 결론: 임상가들이 FRC포스트에 대하여 미세입자 분사마모 표면처리를 하여도 포스트의 굴곡강도와 굴곡계수에는 영향을 미치지 않으면서 접착강도를 높일 수 있을 근거 중의 하나가 될 수 있을 것이다.

S-PRG 필러를 포함하는 치면열구전색제의 전단결합강도 및 미세누출 (Shear Bond Strength and Microleakage of a New Self-etch Sealant Containing S-PRG filler)

  • 안진선;이주현;서현우;박호원
    • 대한소아치과학회지
    • /
    • 제43권4호
    • /
    • pp.347-353
    • /
    • 2016
  • 본 연구의 목적은 S-PRG 필러를 포함하는 치면열구전색제(BeautiSealant)의 법랑질 전단결합강도 및 미세누출을 평가함에 있다. 45개의 소구치를 실험대상으로 사용하였으며, 자가부식 프라이머 도포 후 BeautiSealant를 적용한 군(SEPBS), 인산 부식 후 BeautiSealant를 적용한 군(AEBS), 인산 부식 후 $Clinpro^{TM}$ sealant를 적용한 군(AECP)으로 나누어 실험하였다. 전단결합강도 측정을 위해 치면열구전색제 블록을 법랑질 표면에 적용하였고, 미세누출을 평가하기 위해 소구치의 소와열구에 치면열구전색제를 도포하였다. 전단결합강도와 관련하여 SEPBS군은 AEBS, AECP군에 비해 유의하게 낮은 값을 보였으나(p < 0.05), AEBS군과 AECP군 사이에는 통계적으로 유의한 차이가 존재하지 않았다. 미세누출과 관련하여 3군 사이에 통계적으로 유의한 차이가 존재하지 않았다.

하악 절치의 근관계에 관한 연구 (THE CANAL SYSTEM OF MANDIBULAR INCISORS)

  • 임은미;최호영;박상진;최기운
    • Restorative Dentistry and Endodontics
    • /
    • 제27권4호
    • /
    • pp.432-440
    • /
    • 2002
  • The purpose of this study is to identificate root canal system including ideal access placement, root curvature, canal configuration, incidence of isthmus in mandibular incisors for success of endodontic treatment. 200 mandibular incisors were selected. The ideal access placement was determimed as follows. The teeth there radiographed from mesiodistal and buccolingual views using intraoral dental film. The image was divided into coronal, middle and apical third using the proximal film. Straight line access was determined by measuring the faciolingual canal width and placing points at midway point between the buccal and lingual wall at the junction of the middle and apical third and at the juntion of coronal and middle third of the root canal. A line was drawn connecting these two points extending through the crown of the tooth. The point at which the line crossed the external crown surface was recorded as facial, incisal, lingual. Degree of root curvature was determined by Schneider Protractor Method. Both section method and clearing method were used in this study. By section method, 100 mandibular incisors were embedded in clear resin and transeverse serial sectioned at 0.5, 1.0, 2.0, 3.0, 4.0, 5.0mm level from root apex. The resected surfaces were stained by methylene blue and examined under $\times$40 magnification with a stereomicroscope. By clearing method, 100 mandibular incisors were cleared in methysalicylate after decalcification with 10% nitric acid and evaluated under $\times$18 magnification with a stereomicroscope. The results were as follows ; 1. 29% had the center of the plotted straight-line access facial to incisal edge, whereas 71% had straight-line access at the incisal edge. When incisal wear classified as extensive, the straight-line access was plotted on the incisal edge 95.5%. When incisal wear classified as slight/none, the straight-line access was plotted on the facial 65.9%. 2. Degree of curvature of main canal was straight or almost straight, and only 10% in buccolingual direction had a degree of curvature greater than 20 degrees and 5.5% in mesiodistal direction had. 3. In section method, canal configuration analysis showed that 51% of the specimen classified as type I, 27% as type II, 12% as type III, 10% as type IV. For theses setions with two canals, the incidence of an isthmus was 36.7%, 64.3%, 79.2%, 96.3%, 97.4%, 97.6% at each level and highest in 3~5mm sections. 4. In clearing method, canal configuration analysis showed that 74% of the specimen classified as type I, 11% as type II, 6% as type III, 9% as type IV. These results suggested that traditional access from lingual should be moved as far toward the incisal as possible to locate and debride the lingual canal and root canal system should be cleaned, shaped completely and obturated three dimensionally for successful endodontic treatment.

만곡된 레진 모형 근관에서 4종의 엔진 구동형 니켈-티타늄 기구의 근관 중심율 유지 능력 (The instrument-centering ability of four Nickel-Titanium instruments in simulated curved root canals)

  • 구재훈;장훈상;장석우;조환희;배지명;민경산
    • Restorative Dentistry and Endodontics
    • /
    • 제31권2호
    • /
    • pp.113-118
    • /
    • 2006
  • 본 연구의 목적은 새로 시판된 NRT 기구의 근관 형태 유지 능력을 기존의 3종의 기구와 비교하는 것이다. 만곡된 레진 모형 근관을 ProFile, K3, ProTaper, NRT 기구를 이용하여 형성하였고 형성 전, 후의 상을 스캔한 후 중첩시켜 이미지 분석 프로그램을 이용하여 근관 만곡도의 변화와 근관 중심축에 대한 근관의 변이 정도를 근관 중심율의 변화로 계산하여 분석하였다. 근관 변이의 유의성 검정을 위해 one-way ANOVA분석을 시행하였으며 각 기구간의 유의성 검정은 Duncan's test로 사후 분석하였다. 근첨에서 1, 2 mm 상방 위치에서의 근관 중심율은 ProFile 군이 다른 군에 비해 우수한 것으로 나타났다. (p < 0.05). NRT기구의 근관 중심율 변화를 측정한 결과 근첨으로부터 5 mm 상방에서는 Profile에 비해서만 큰 것으로 나타났고 6, 7 mm 상방에서는 다른 모든 군들에 비해 큰 것으로 나타났다 (p < 0.05). 비록 NRT기구가 근첨 부위에서는 ProFile을 제외한 다른 기구에 비해 유의차 없는 중심률 유지 능력을 보였으나 근관 입구 및 중간부위의 형성에 사용되는 스테인레스-스틸 파일로 인해 coronal flaring시 다른 기구들에 비해 더 많은 중심률의 변화를 보이는 것으로 사료된다.

카복실레이트계 시멘트의 접착력에 관한 비교 연구 (COMPARATIVE STUDIES OF THE ADHESIVE QUALITIES OF POLYCARBOXYLATE CEMENTS)

  • 이한무
    • 대한치과보철학회지
    • /
    • 제17권1호
    • /
    • pp.23-34
    • /
    • 1979
  • In this study, the adhesive strength of three commercial polycarboxylate cements to ten types of dental casting alloys, such as gold, palladium, silver, indium, copper, nickel, chromium, and human enamel and dentine were measured and compared with that of a conventional zinc phosphate cement. The $8.0mm{\times}3.0mm$ cylindrical alloy specimens were made by casting. The enamel specimens were prepared from the labial surface of human upper incisor, and the dentine specimens were prepared from the occulusal surface of the human molar respectively. Sound extracted human teeth, which had been kept in a fresh condition since, extraction, were mounted in a wax box with a cold-curing acrylic resin to expose the flattened area. The mounted teeth were then placed in a Specimen Cutter (Technicut) and were cut down under a water spray, and then the flat area on the all specimens were ground by hand with 400 and 600 grit wet silicone carbide paper. Two such specimens were then cemented together face-to-face with freshly mixed cement, and moderate finger pressure was applied to squeeze the cement to a thin and uniform film. All cemented specimens were then kept in a thermostatic humidor cabinet regulated at $23{\pm}2^{\circ}C.$ and more than 95 per cent relative humidity and tested after 24 hours and 1 week. Link chain was attached to each alloy specimen to reduce the rigidity of the jig assembly, and then all the specimens were mounted in the grips of the Instron Universal Testing Machine, and a tensile load was delivered to the adhering surface at a cross head speed of 0.20 mm/min. The loads to which the specimens were subjected were recorded on a chart moving at 0.50 mm/min. The adhesive strength was determined by measuring the load when the specimen separated from the cement block and by dividing the load by the area. The test was performed in a room at $23{\pm}2^{\circ}C.$ and $50{\pm}10$ per cent relative humidity. A minimum of five specimens were tested each material and those which deviated more than 15 per cent from the mean were discarded and new specimens prepared. From the experiments, the following results were obtained. 1) It was found that the adhesive strength of the polycarboxylate cement to all alloys tested was considerably greater than that of the zinc phosphate cement. 2) The adhesive strength of the polycarboxylate cements was superior to the non precious alloys, such as the copper, indium, nickel and chromium alloys, but it was inferior to the precious gold, silver and palladium alloys. 3) Surface treatment of the alloy was found to be an important factor in achieving adhesion. It appears that a polycarboxylate cement will adhere better to a smooth surface than to a rough one. This contrasts with zinc phosphate cements, where a rough helps mechanical interlocking. 4) The adhesion of the polycarboxylate cement with enamel was found superior to its adhesion with dentine.

  • PDF

골내 임플랜트의 종류에 따른 광탄성 응력 분석 (PHOTOELASTIC ANALYSIS OF STRESS INDUCED BY DIFFERENT TYPE ENDOSSEOUS IMPLANTS)

  • 정재헌;장두익
    • 대한치과보철학회지
    • /
    • 제31권4호
    • /
    • pp.661-678
    • /
    • 1993
  • The purpose of this study was to analyze the stress distribution at supporting bone according to the types of endosseous implants. This investigation evaluated the stress patterns in rectangular photoelastic models produced by four different types of dental implants such as $Br\ddot{a}nemark$, screw type of Steri-Oss, blade type of Steri-Oss, IMZ with IMC and resin tooth using the techniques of quasi-three dimensional photoelasticity. All prostheses were casted in the same nonprecious alloy and were cemented or screwed on their respective implants and abutments. 20 kg of vertical load was applied on the central fossa of casted crown and 16 kg of inclined had was applied on the top third of distal surface of casted crown respectively. The results were as follows : 1. Under the vertical load, screw implants of Steri-Oss and $Br\ddot{a}nemark$ showed increasing stress condition between and around the screw threads along the implant lateral surface and cylindrical implant of IMZ showed the less stress condition along the lateral surface with concentration of stress mostly near the root apex. 2. Under the vertical load, the stress of Steri-Oss blade was distributed uniformly at the alveolar bone under the broad blade. 3. Under the inclined load, the stress concentration of Steri-Oss screw and $Br\ddot{a}nemark$ was developed highly around the mesiocervical bone area on the contralateral side to force application. The stress of $Br\ddot{a}nemark$ with flexible gold glod was more concentrated in the cervical bone area than that of Steri-Oss with stiff screw. 4. Under the inclined load, the stress of Steri-Oss blade broadly was distributed around the mesioceivical bone area and the lower and mesial bone area of the blade. 5. Under the Inclined load, IMZ implant showed the gap between c개wn and fixture due ta deformation of the IMC and IMZ was lower in stress concentration developed around the mesiocervical bone area than $Br\ddot{a}nemark$ and Steri-Oss screw. 6. Under the inclined load, the stress magnitude induced in the mesiocervical bone area of implants was in order of $Br\ddot{a}nemark$, Steri-Oss strew, IMZ and Stsri-Oss blade. 7. Tilting forces as compared to axial forces exerted greater magnitude of stress in the cervical bone area of the implant. 8. In respect of stress distribution, Steri-Oss blade was superior than any other implants and in respect of the stability by horizontal lone, IMB and $Br\ddot{a}nemark$ was inferior than any other implants.

  • PDF

수종 임플랜트 시스템에서의 회전력에 관한 연구 (A STUDY ON THE TORQUE VALUES IN THE DIFFERENT IMPLANT SYSTEM)

  • 문익훈;정재헌
    • 대한치과보철학회지
    • /
    • 제33권2호
    • /
    • pp.335-353
    • /
    • 1995
  • The purpose of this study was to the determine the optimal torques values to tighten the retaining screw. 3-different implant system tested were as follows : Branemark implant system$(3.75mmD{\times}100mm)$, Steri-Oss implant system$(3.8mmD{\times}10mm)$. One fixtures of each implant system was mounted into the epoxy resin block and abutment/superstructure complex was constructed. Eighty dental college students(male : 40, female : 40) of Chosun University were selected and were asked to tighten the retaining screws. Abutment/superstructure complex of each implant system was tightened to the maximum torque by use of hand-held screw driver, and then torque value was measured with torque value was measured with torque driver(Tohnichi torque driver, model 20 FTD, Tohnichi MFG, Co., LTD., Tokyo, Japan). Abutment/superstructure complex of each implant system was titghtened to each torque of 10 N-cm, 20 N-cm and 30 N-cm, and then the dynamic load(vertical & diagonal load) was applied to the abutment / superstructure complex. The gap between abutment/superstrure in each implant system was measured with 3-dimensional measuring microscope(model No. 850, Germany). The results were as follow : 1. Torque values according to the individual subjects showed wide range. 2. Torque values according to sex showed statistical significant difference. Those are as follows : in case of male, $9.38{\pm}2.93$ N-cm ; incase of female, $7.80{\pm}2.25$ N-cm. 3. Torque values according t implant systems showed statistical significant difference. Those are as follows : in ase of Branemark implant system, $6.54{\pm}1.54$ N-cm : in ase of Steri-Oss implant system, $10.1{\pm}2.88$ N-cm ; in case of IMZ implant system, $9.18{\pm}2.17$ N-cm. 4. The more torque value of tightening screw was increased, the less the gap was after the vertical and diagonal loading. 5. The gap after the diagonal loading was greater than that after the vertical loading. 6. The magnitude of gap between abutment/superstructure in order of IMZ, Steri-Oss, Branemark implant system after the verical and diagonal loading. 7. The gap under the diagonal loading after applying 30 N-cm torque showed no statistical significant difference in cases of the Branemark system and the Steri-Oss implant system but it showed significant different in case of the IMZ implant system.

  • PDF