• Journal of the Korean Society for Nondestructive Testing
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• v.27 no.1
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• pp.1-7
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• 2007

As fiber reinforced composite materials are widely used in aircraft, space structures and robot arms, the study on non-destructive testing methods has become an important research area for improving their reliability and safety. AE (acoustic emission) can evaluate the defects by detecting the emitting strain energy when elastic waves are generated by the initiation and growth of crack, plastic deformation, fiber breakage, matrix cleavage, or delamination. In the paper, AE signals generated under uniaxial tension were measured and analyzed using the $8{\times}8$ matrix piezo electric sensor. The electronic circuit to control the transmitting distance of AE signals was designed and constructed. The optical data storage system was also designed to store the AE signal of 64channels using LED (light emitting diode) elements. From the tests, it was shown that the source location and propagation path of AE signals in composite materials could be detected effectively by the $8{\times}8$ matrix piezo electric sensor.

• Composites Research
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• v.16 no.3
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• pp.9-17
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• 2003

In order to simulate the crack connection between cords and the interply crack growth in the belt-layer of real tire, 2 ply rubber/cord laminate specimens with exposed edges were tested in 4~11mm displacement control. Measurement of the crack connection is evaluated when crack reaches the half of the length between 45$^{\circ}$ aligned cords, and the amount of the crack growth is measured by the steel probe method. 2 dimensional analytic modeling was performed to simulate the crack connection between cords at the exposed edges. Also, the theoretical life of the specimens was calculated from the crack connection life between cords(critical value) and from the critical value to the final failure by the use of Tearing energy(T); the strain energy release per unit area of one fracture surface of a crack. Then, theoretical life was compared with those of experiments. The life prediction up to the critical value has about 20% error compared to experimental life, and up to the final failure about 65% error. Therefore, total theoretical life has about 45% error compared to the experimental life, which is conceivable in the case of rubber.

• Journal of the Korean Society for Nondestructive Testing
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• v.17 no.1
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• pp.1-10
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• 1997

In this paper, the effects of temperature change (low and high temperature) on the impact damages of CFRP laminates was experimentally studied. Composite laminates used for this experiment are CF/epoxy orthotropic laminated plates, which have two-interfaces $[0^{\circ}\;_6/90^{\circ}\;_6]s$ and $[0^{\circ}\;_4/90^{\circ}\;_4]s$. And CF/PEEK orthotropic laminated plates, which have two-interfaces $[0^{\circ}\;_4/90^{\circ}\;_4]s$. And, this study aims experimentally to present the interrelations between the impact energy vs. impact damages (i.e. delamination area and matrix crack) of CFRP laminates (CF/epoxy, CF/PEEK) subjected to FOD(foreign object damage) under low and high temperatures. A steel ball launched by the air gun collides against CFRP laminates to generate impact damages.

• Fire Science and Engineering
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• v.34 no.4
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• pp.101-106
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• 2020

This study analyzed flame growth characteristics and carbonization patterns when floor materials were burned vertically using a needle flame produced for this study. It was found that PVC flooring was fire retardant and the area under direct flame contracted inward. Vertical combustion causes solidification in the form of a lump at the bottom and also generates soot in a pattern that progresses upwards. This study found that laminated flooring exhibited no fire retarding characteristics and that the laminated layer of its upper surface was destroyed by fire, causing irregular delamination. The carbonization ranges at the left and right sides were determined to be symmetrical. A vertical combustion test of a sample carpet showed that it exhibited no fire-retarding characteristics. It was observed that if heat accumulated in the carpet, the flame formed an ascending air current, and that when flammable materials were present around the flame, they further accelerated the diffusion of the flame. The carbonization pattern at the carpet surface exposed to direct flame revealed that the carpet surface had melted and had flown downwards and that many tiny holes formed on it.

• Journal of Electrochemical Science and Technology
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• v.12 no.2
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• pp.246-256
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• 2021

Mo,Cu-doped CeO₂ (CMCuO) nanopowders were synthesized by the nitrate-fuel combustion method aiming to improve the electrical and electrochemical properties of its Mo-doped CeO₂ (CMO) parent by the addition of copper. An electrical conductivity of ca. 1.22·10^-2 S cm^-1 was measured in air at 800℃ for CMCuO, which is nearly 10 times higher than that reported for CMO. This increase was associated with the inclusion of copper into the crystal lattice of ceria and the presence of Cu and Cu₂O as secondary phases in the CMCuO structure, which also could explain the increase in the charge transfer activities of the CMCuO based anode for the hydrogen and carbon monoxide electro-oxidation processes compared to the CMO based anode. A maximum power density of ca. 120 mW cm^-2 was measured using a CMCuO based anode in a solid oxide fuel cell (SOFC) with YSZ electrolyte and LSM-YSZ cathode operating at 800℃ with humidified syngas as fuel, which is comparable to the power output reported for other SOFCs with anodes containing copper. An increase in the area specific resistance of the SOFC was observed after ca. 10 hours of operation under cycling open circuit voltage and polarization conditions, which was attributed to the anode delamination caused by the reduction of the Cu₂O secondary phase contained in its microstructure. Therefore, the addition of a more electroactive phase for hydrogen oxidation is suggested to confer long-term stability to the CMCuO based anode.

• Composites Research
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• v.35 no.6
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• pp.469-476
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• 2022

In this paper, the microwave absorbing characteristics after the impact of the radar-absorbing structure (RAS) consisting of periodic pattern sheet (PPS) and glass fiber-reinforced plastic (GFRP) were experimentally investigated. The fabricated RAS effectively absorbed the microwave in the X-band (8.2-12.4 GHz). In order to induce the damage to the RAS, a low-velocity impact test with various impact energy of 15, 40, and 60 J was conducted. Afterward, the impact damage was observed by using visual inspection, non-destructive test, and image processing method. Moreover, the absorbing performance of intact and damaged RAS was measured by the free-space measurement system. The experiment results revealed that the delamination damage from the impact energy of 15 J did not considerably affect the microwave absorbing performance of the RAS. However, fiber breakage and penetration damage with a relatively large damaged area were occuured when the impact energy was increased up to 40 J and 60 J, and these failures significantly degraded the microwave absorbing characteristics of the RAS.

• Journal of the Korean Society for Nondestructive Testing
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• v.27 no.5
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• pp.426-431
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• 2007

When a high-energy ultrasound propagates through a solid body that contains a crack or a delamination, the two faces of the defect do not ordinarily vibrate in unison, and dissipative phenomena such as friction, rubbing and clapping between the faces will convert some of the vibrational energy to heat. By combining this heating effect with infrared imaging, one can detect a subsurface defect in material in real time. In this paper a realtime detection of the brazing defect of thin Inconel plates using the UIR (ultrasonic infrared imaging) technology is described. A low frequency (23 kHz) ultrasonic transducer was used to infuse the welded Inconel plates with a short pulse of sound for 280 ms. The ultrasonic source has a maximum power of 2 kW. The surface temperature of the area under inspection is imaged by an infrared camera that is coupled to a fast frame grabber in a computer. The hot spots, which are a small area around the bound between the two faces of the Inconel plates near the defective brazing point and heated up highly, are observed. And the weak thermal signal is observed at the defect position of brazed plate also. Using the image processing technology such as background subtraction average and image enhancement using histogram equalization, the position of defective brazing regions in the thin Inconel plates can be located certainly.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.27 no.3
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• pp.199-206
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• 2014

In this paper, a scheme to evaluate the response variability for functionally graded material (FGM) beam with varying sectional area is presented. The randomness is assumed to appear in a spatial domain along the beam axis in the elastic modulus. The functionally graded material categorized as composite materials, however without the drawbacks of delamination and occurrence of cracks due to abrupt change in material properties between layers in the conventional composite materials. The functionally graded material is produced by the gradual solidification through thickness direction, which endows continuous variation of material properties, which makes this material performs in a smooth way. However, due to difficulties in tailoring the gradients, to have uncertainty in material properties is unavoidable. The elastic modulus at the center section is assumed to be random in the spatial domain along the beam axis. Introducing random variables, defined in terms of stochastic integration, the first and second moments of responses are evaluated. The proposed scheme is verified by using the Monte Carlo simulation based on the random samples generated employing the spectral representation scheme. The response variability as a function of correlation distance, the effects of material and geometrical parameters on the response variability are investigated in detail. The efficiency of the proposed scheme is also addressed by comparing the analysis time of the proposed scheme and MCS.

• Journal of the Korean Electrochemical Society
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• v.21 no.3
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• pp.47-54
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• 2018

To maximize the areal capacity($mAh\;cm^{-2}$) of $LiNi_{0.5}Co_{0.2}Mn_{0.3}O_2$(NCM523) electrode with the same loading level of $15mg\;cm^{-2}$, three NCM523 electrodes with 4, 2, and 1 wt% poly(vinylidene fluoride)(PVdF) binder content are fabricated. Due to the delamination issue of electrode composite at the edge during punching process, the 1 wt% electrode is excluded for further evaluation. When the PVdF binder content decreases from 4 to 2 wt%, both adhesion strength and shear stress decrease from 0.4846 to $0.2627kN\;m^{-1}$ by -46% and from 3.847 to 2.013 MPa by -48%, respectively. Regardless of these substantial decline of mechanical properties, their initial electrochemical properties such as initial coulombic efficiency and voltage profile are almost the same. However, owing to high loading level, the 2 wt% electrode not only exhibits worse cycle performance than the 4 wt% electrode, but also cannot maintain its mechanical integrity only after 80 cycles. Therefore, if the binder content is reduced to increase the area capacity, the mechanical properties as well as the cycle performance must be carefully evaluated.

• Composites Research
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• v.30 no.6
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• pp.356-364
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• 2017

Composite lattice structures are tried to be used in various fields because of its benefit in physical properties. With increase of demand of the composite lattice structure, nondestructive testing technology is also required to certificate the quality of the manufactured structures. Recently, research on the development of the composite lattice structure in Republic of Korea was started and accordingly, fast and accurate non-destructive evaluation technology was needed to finalize the manufacturing process. This paper studied non-destructive testing methods for composite lattice structure using laser ultrasonic propagation imaging systems. Pulse-echo ultrasonic propagation imaging system was able to inspect a rib structure wrapped with a skin structure. To reduce the time of inspection, a band divider, which can get signal in different frequency bands at once, was developed. Its performance was proved in an aluminum sandwich panel. In addition, to increase a quality of results, curvature compensating algorithm was developed. On the other hand, guided wave ultrasonic propagation imaging system was applied to inspect delamination in a rib structure. To increase an area of inspection, multi-source ultrasonic wave propagation image was applied, and defects were successfully highlighted with variable time window amplitude mapping algorithm. These imply that ultrasonic propagation imaging systems provides fast and accurate non-destructive testing results for composite lattice structure in a stage of the manufacturing process.