• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2015.11a
• /
• pp.137-137
• /
• 2015

The purposed of this work was to observe hydroxyapatite precipitation phenomena on micro-pore formed Ti-Nb alloy by PEO technique. The Ti-30Nb and Ti-30Ta alloys were remelted at least ten times in order to avoid inhomogeneity, and then cylindrical specimens (diameter 10 mm, thickness 4 mm) were cut by using laser from cast ingots of the Ti alloys. Heat treatment was carried out at $1050^{\circ}C$ for 2 h for homogenization in argon atmosphere. The morphologic change of the alloys were examined by X-ray diffractometer (XRD) and field emission scanning electron microscopy (FE-SEM).

• Geomechanics and Engineering
• /
• v.3 no.2
• /
• pp.83-108
• /
• 2011

The effect of non-plastic fines (silt) on liquefaction and pore pressure generation characteristics of saturated sands was studied through undrained stress controlled cyclic triaxial tests using cylindrical specimens of size 50 mm diameter and height 100 mm at different cyclic stress ratios and at a frequency of 0.1 Hz. The tests were carried out in the laboratory adopting various measures of sample density through various approaches namely gross void ratio approach, relative density approach, sand skeleton void ratio approach, and interfine void ratio approach. The limiting silt content and the relative density of a specimen were found to influence the undrained cyclic response of sand-silt mixtures to a great extent. Undrained cyclic response was observed to be independent of silt content at very high relative densities. However, the presence of fines significantly influenced this response of loose to medium dense specimens. Combined analyses of cyclic resistance have been done using the entire data collected from all the approaches.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2008.05a
• /
• pp.482-484
• /
• 2008

Anodic aluminum oxide (AAO) which prepared with two-step anodizing method (with dissimilar solutions) was used as a template to fabricate highly ordered, free standing metal nano-rods. AAO nano-template technique can realize self-organized hexagonal pore structure with nanometer dimension size, it's easy to control pore diameter, length and density by varying anodizing conditions. Ni and Ni/Fe/Cu multi-metal layer nanorods were electrochemically deposited into AAO nano-template by AC voltage in simple sulfate solutions.. The properties of samples are tested by X-ray diffraction (XRD), field emission microscopy (FE-SEM).

• Restorative Dentistry and Endodontics
• /
• v.46 no.4
• /
• pp.57.1-57.9
• /
• 2021

Objectives: This study aimed to compare and evaluate the porosity and pore size distribution of high-viscosity glass ionomer cements (HVGICs) and conventional glass ionomer cements (GICs) using micro-computed tomography (micro-CT). Materials and Methods: Forty cylindrical specimens (n = 10) were produced in standardized molds using HVGICs and conventional GICs (Ketac Molar Easymix, Vitro Molar, MaxxionR, and Riva Self-Cure). The specimens were prepared according to ISO 9917-1 standards, scanned in a high-energy micro-CT device, and reconstructed using specific parameters. After reconstruction, segmentation procedures, and image analysis, total porosity and pore size distribution were obtained for specimens in each group. After checking the normality of the data distribution, the Kruskal-Wallis test followed by the Student-Newman-Keuls test was used to detect differences in porosity among the experimental groups with a 5% significance level. Results: Ketac Molar Easymix showed statistically significantly lower total porosity (0.15%) than MaxxionR (0.62%), Riva (0.42%), and Vitro Molar (0.57%). The pore size in all experimental cements was within the small-size range (< 0.01 mm³), but Vitro Molar showed statistically significantly more pores/defects with a larger size (> 0.01 mm³). Conclusions: Major differences in porosity and pore size were identified among the evaluated GICs. Among these, the Ketac Molar Easymix HVGIC showed the lowest porosity and void size.

• Geomechanics and Engineering
• /
• v.25 no.4
• /
• pp.303-315
• /
• 2021

A rigorous and generic similarity solution is developed for assessment of the undrained expansion responses of a cylindrical cavity expansion in K₀-consolidated anisotropic soils. A K₀-consolidated anisotropic modified Cam-clay (K₀-AMCC) model that can represent the initial stress anisotropy and the effects of stress-induced anisotropy is used to model the soil behaviors during cavity expansion. All the seven basic unknowns, the three stress components, the pore water pressure, the particle velocity, the specific volume and the hardening parameter, are reduced to the functions of a dimensionless radial coordinate and are taken as coupled variables to formulate the problem. The governing equations are formulated by making use of the equilibrium equation, the constitutive equation, the consistency condition, the continuity condition and the undrained condition, which are then solved as an initial value problem. The proposed rigorous similarity solution is compared with some well-documented rigorous solutions to validate the solution and to highlight the special expansion responses in anisotropic soils. The results reveal that the present solution can yield more predictions for cavity expansion problems in soils with initial anisotropic stresses.

• Journal of Environmental Science International
• /
• v.30 no.12
• /
• pp.1081-1092
• /
• 2021

In this study, the effect on the stability of Aerobic Granular Sludge (AGS) caused by an AGS separator was investigated. The AGS separator was a hydrocyclone. The main factors of the AGS separator were filter pore size (0.125~0.600 mm), conical-to-cylindrical ratio (1.5~3.0), and operating time (1~20 min). The AGS/mixed liquor suspended solid (MLSS) ratio gradually increased to 0.500 mm (AGS/MLSS: 84.3±3.0%). AGS was best separated at the conical-to-cylindrical ratio of 2.5 (AGS/MLSS: 84.7±3.3%). As the operating time increased, the AGS separation performance also tended to increase. The shortest AGS separator run time, but the highest AGS separation performance was 10 min (87.0±2.5%). AGS stability was evaluated by operating the selected AGS separator and sequencing batch reactor. The average removal efficiencies of TOC, TCOD_Cr, SS, TN, and TP were 95.7%, 96.9%, 93.0%, 89.0%, and 96.2%, respectively, which met the effluent standards in Korea. In addition, the AGS/MLSS ratio tended to remain constant, and the sludge volume index demonstrated a tendency to decrease from 140 mL/g to 70 mL/g. During the operation, the particles of AGS in optical microscope observations gradually increased.

• Proceedings of the Materials Research Society of Korea Conference
• /
• 2011.05a
• /
• pp.7.1-7.1
• /
• 2011

Nanoporous templates have been widely used for the development of new functional nanostructured materials suitable for electronics, optics, magnetism, and energy storage materials. We have prepared nanoporous templates by using thin films of mixtures of polystyrene-block-poly (methyl methacrylate) (PS-b-PMMA) and PMMA homopolymers. These templates have cylindrical nanoholes spanning the entire thickness of the film. Some applications of nanoporous templates are introduced: a) anti-reflective coating, b) the preparation of conducting polymer nanowires of poly (pyrrole), poly (3,4-ethylenedioxy-thiopene) onto a glass coated with indium-tin-oxide, and c) the separation membranes for biomaterials. We found that when the pore fraction of nanoholes in the film was ~0.68, almost zero reflectance at a specific wavelength, which can be changed with film thickness, was achieved at visible wavelengths Furthermore, ultra high density array of conducting nanowires was successfully prepared onto various substrates including flexible polymer. Due to highly alignment of polymer chain along the nanowire direction, the conductivity was much increased. Furthermore, these nanoporous films were found to be very effective for the separation of human Rhinovirus type 14 (HRV 14), major pathogen of a common cold in humans, from the buffer solution. We also found that when the pore size was effectively controlled down to 6 nm, a single file diffusion was observed.

• Proceedings of the Polymer Society of Korea Conference
• /
• 2006.10a
• /
• pp.313-313
• /
• 2006

In this study, we describe a new double layered nanoporous membrane suitable for virus filtration. One layer is an 80 nm thick film having cylindrical pores with diameters of 15 nm and a narrow pore size distribution. This layer is prepared by using a thin film of the mixture of a block copolymer and a homopolymer, and mainly acts to separate viruses. The support layer (${\sim}150\;microns\;thick$) is a conventional micro-filtration membrane with a broad pore size distribution. This asymmetric membrane showed very high selectivity and flux for the separation of human rhinovirus type 14 (HRV 14) which has a diameter of ${\sim}30\;nm$ and is a major pathogen of the common cold in humans.

• Proceedings of the Korean Vacuum Society Conference
• /
• 2010.08a
• /
• pp.195-195
• /
• 2010

In recent years, Anodic aluminum oxide(AAO) has become popular and attractive materials. It can be easily fabricated and self-organized pore structures. It has been widely used as a biosensor membrane, photonic crystal for optical circuit and template for nanotube growth etc. In previous papers, the theory was developed that AAO shows anisotropic optical properties, since it has anisotropic structure with numerous cylindrical pores. It gives rise to the anisotropy of the refractive index called as birefringence. It can be used as conventional polarizing elements with high efficiency and low cost. Therefore, we would like to compare the theory and experimental results in this study. One method which can measure effective refractive index of thin film is the prism coupling technique. It can give accurate results fast and simply. Furthermore, we can also measure separately the refractive index with different polarization using polarization of the laser (TE mode and TM mode). We calculated the effective refractive index with effective medium approximations (EMAs) by pore size in the SEM image. EMAs are physical models that describe the macroscopic system as the homogeneous and typical method of all mean field theories.

• Journal of the Korean GEO-environmental Society
• /
• v.11 no.12
• /
• pp.57-62
• /
• 2010

In this study, the effect of different silt contents on the shear characteristics of silty sands was evaluated. Two series of triaxial compression tests were performed on the cylindrical specimens of compacted Nakdong river sand with 10% and 30% silt contents under unconsolidated undrained condition. All identical specimens were prepared to compact with same initial water content for five layers and saturated using control panel and then sheared under initial effective confining pressure, 100 to 400kPa. All specimens exhibited a strain softening tendency after failure in stress-strain curves and deviator stresses of specimens with 10% silt content were greater than those of specimens with 30% silt content. Pore water pressures of specimens with 10% silt content were observed negative(i.e. swelling) due to increasing void ratio after failure but those of specimens with 30% silt content were shown only positive. The behavior of compacted cylindrical specimens with low silt content was more dilative than that of high silt content. Peak deviator stresses decreased as increasing silt content and peak pore water pressures increased as increasing silt content.