• Title/Summary/Keyword: curing degree

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Value Engineering Approach for Heat Curing Method Under Cold Weather Condition (한중콘크리트 보온양생 공법에 대한 VE분석)

  • Woo, Dae-Hun;Kim, Tae-Cheong;Kim, Jong;Jeon, Chung-Keun;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2010.05a
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    • pp.21-23
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    • 2010
  • This study was conducted to draw various decisive elements of a reasonable heat curing method and to examine the importance in deciding a construction method when constructing cold weather concrete. As a result, the items proposed as important elements at the time of decision of a heat curing method included economy, workability, maintainability, insulation capability, reduced construction period and usability. As a result of importance by items under AHP technique, it was found the most important element was insulation capability, followed by reduced construction period and workability. As a result of comparison of a heat supplying and a heat insulation method by dual bubble sheet differed 2 times as much as a heat supplying method, especially the evaluation degree by insulation capability and reduced construction period was high.

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Investigation of cure cycle for co-cured metal/composite hybrid structures without fabricating thermal residual stress (동시경화 하이브리드 금속/복합재료 구조물의 제조 잔류 열응력 제거를 위한 경화사이클에 관한 연구)

  • Kim Hak Sung;Park Sang Wook;Lee Dai Gil
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.10a
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    • pp.83-87
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    • 2004
  • In this work, the cure cycle of co-cured metal/composite structure was investigated to decrease fabricating thermal residual stresses between the metal and the composite material. DSC (Differential scanning calorimetry) experiment and static lap shear test of co-cured aluminum/composite double lap joint as well as the curvature experiment of co-cured steel/composite strip were performed to investigate the effect of curing cycle on the thermal residual stress of co-cured hybrid structures. From the experiments, it was found that post curing method after abrupt cooling of co-cured aluminum/composite hybrid structure at certain point of degree of cure during curing process could eliminate fabricating the thermal residual stresses.

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Curing Behavior of Phenolic Resin with Humid Atmosphere on The Porous $ZrO_2$ ceramics

  • Yun, Sang-Hyeon;Kim, Jang-Hun;Kim, Ju-Yeong;Lee, Jun-Tae;Lee, Hui-Su
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.05a
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    • pp.57.1-57.1
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    • 2011
  • The effects of relative humidity on the properties of the porous $ZrO_2$ ceramics were investigated in terms of the curing behavior of phenolic resin as a binder. The $ZrO_2$ powders containing 5wt% of phenolic resin were conditioned in a consistent chamber condition at a temperature of $50^{\circ}C$ and different humidity levels (25, 50, 75, and 95%) for 1 h. The exposure of humid atmosphere caused changes of density and microstructure in the green bodies. The higher level the powders were exposed to the humid atmosphere, the lower green density was obtained and the more irregular microstructure was observed due to aggregation by the curing of phenolic resin. After firing, the porosity of specimens has risen from 35.7% to 38.1% and Young's modulus has declined in response to the variation of green density. These results could be explained by the degree of resin cure which was associated with the area under the exothermic peak enclosed by a baseline of DSC thermogram curve. Also, the curing behavior of phenolic resin according to relative humidity has been confirmed by decrease of ether groups which have interacted with the phenolic-OH group and the hexamine as a curing agent. Consequently, it could be demonstrated that increase the relative humidity during fabrication of porous $ZrO_2$ diminished the compaction and properties of specimens after firing owing to curing of phenolic resin.

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A Field Trial of Norfloxacin on Bovine, Swine and Poultry with Respiratory Diseases and Diarrhea (소, 돼지, 닭의 호흡기병과 설사에 대한 Norfloxacin 주사 및 경구용 제제의 야외치료시험)

  • 손봉환;황현순;김정훈;한태호;배도권
    • Korean Journal of Veterinary Service
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    • v.14 no.2
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    • pp.159-174
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    • 1991
  • A field trial of norfloxacin on bovine 206, swine 222 and poultry 205 with respiratory diseases and diarrhea was conducted from Sept 1, 1990 to Jan 30, 1991 in Inchon and Kyonggi-do. The results are as follows. 1. Guinea pigs and rabbits were dosages 10 and 20 times normal. Ten days of observation saw no side effect. 2. Oral treatment on bovine, swine and poultry showed a curing rate of 82.00∼89.06%(Mean 86.00%), compared with 87.27∼96.36%(Mean 92.24%) by Injection. 3. The curing rate was 81.92% by the fourth treatment. 4. The curing rate with and without the use of adjuvant was 80.00∼100% and 83.60∼93. 10%, respectively, for swine, and 81.82∼100% and 82.00∼97.14% for bovine. 5. The curing rate was more dependent on seriousness of illness, environment and time than age. 6. The main disease causing bacteria of bovine respiratory diseases: Haemolytic Sta 27.62%, Haemolytic Str 33.33%, sum of this bacteria is 60.95%, diarrhea: Haemolytic coliform 80.20%, swine respiratory diseases; Haemophilus Spp 20.95%, Haemolytic Sta 72%, Haemolytic Str 21.90%, Sum of these bacteria is 68.57%, diarrhea; Haemolytic coliform 57.26%, poultry respiratory diseases; mycoplasma Spp 29.52%, Haemolytic Sta 13.33%, Sum of this bacteria is 42.85%, diarrhea; Haemolytic coliform 53.00%. 7. The curing rate of norfloxacin by species of strain, the unidentified bacteria on bovine respiratory diseases was the lowest with 77.78%, the others ranged from 84.21% to 100% with most of them over 90%. 8. The loss of clinical sign on bovine and swine was the highest when after 2∼4 application. 9. In terms of antibiotic sensitivity test, norfloxacin was the highest with 84.62∼100% (mean 90.09%) among eight bacterias, only 5 of 15 antibiotics had a sensitivity of over 56.25%, showing a high degree of tolerance.

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Plasmid Profiling and Curing of Lactobacillus Strains Isolated from the Gastrointestinal Tract of Chicken

  • Chin Sieo Chin;Abdullah Norhani;Siang Tan Wen;Wan Ho Yin
    • Journal of Microbiology
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    • v.43 no.3
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    • pp.251-256
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    • 2005
  • In this study, we assessed the susceptibility of 12 Lactobacillus strains, all of which had been isolated from the gastrointestinal tracts of chicken, to three antibiotics (chloramphenicol, erythromycin and tetracycline) used commonly as selective markers in transformation studies of lactic acid bacteria. Among these strains, $17\%,\;58\%,\;and\;25\%$ were found to exhibit a high degree of resistance to $200\;{\mu}g/ml$ of tetracycline, erythromycin, and chloramphenicol, respectively. Seven of the 12 Lactobacillus strains exhibiting resistance to at least $50\;{\mu}g/ml$ of chloramphenicol or erythromycin, and five strains exhibiting resistance to at least $50\;{\mu}g/ml$ of tetracycline, were subsequently subjected to plasmid curing with chemical curing agents, such as novobiocin, acriflavin, SDS, and ethidium bromide. In no cases did the antibiotic resistance of these strains prove to be curable, with the exception of the erythromycin resistance exhibited by five Lactobacillus strains (L. acidophilus I16 and I26, L. fermentum I24 and C17, and L. brevis C10). Analysis of the plasmid profiles of these five cured derivatives revealed that all of the derivatives, except for L. acidophilus I16, possessed profiles similar to those of wild-type strains. The curing of L. acidophilus I16 was accompanied by the loss of 4.4 kb, 6.1 kb, and 11.5 kb plasmids.

Comparing volumetric and biological aspects of 3D-printed interim restorations under various post-curing modes

  • Song, Gun;Son, Ji-Won;Jang, Ji-Hyun;Choi, Sung-Hyeon;Jang, Woo-Hyung;Lee, Bin-Na;Park, Chan
    • The Journal of Advanced Prosthodontics
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    • v.13 no.2
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    • pp.71-78
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    • 2021
  • Purpose. This study aims to compare the volumetric change, degree of conversion (DOC), and cytotoxicity of 3D-printed restorations post-cured under three different conditions. Materials and Methods. 3D-printed interim restorations were post-cured under three different conditions and systems: 5 min, 30 min, and 24 h. Three-unit and six-unit fixed dental prostheses (n = 30 for each case) were printed; ten specimens from each group were post-cured and then scanned to compare their volumetric changes. Root-mean-squared (RMS) values of the data were acquired by superimposing the scanned files with original files. Thirty disk-shaped specimens were printed to evaluate the DOC ratio. Fourier transform infrared spectroscopy was used to compare the DOCs of 10 specimens from each group. Human gingival fibroblasts were used to measure the cell viability of every specimen (n = 7). The data from this experiment were employed for one-way analysis of variance and Tukey's post-hoc comparisons. Results. Differences between the three-unit restorations were statistically insignificant, regardless of the post-curing conditions. However, for the six-unit restorations, a high RMS value was acquired when the post-curing duration was 30 min. The average DOC was approximately 56 - 62%; the difference between each group was statistically insignificant. All the groups exhibited cell viability greater than 70%, rendering them clinically acceptable. Conclusion. The post-curing conditions influenced the volume when the length of the restoration was increased. However, this deviation was found to be clinically acceptable. Additionally, post-curing did not significantly influence the DOC and cytotoxicity of the restorations.

Effect of Zirconia Particle Addition on Curing Behavior of Phenolic Resins (Zirconia 입자의 첨가가 페놀 수지의 경화거동에 미치는 영향)

  • Yun, Jaeho;Kim, Hanjun;Lee, Jae Min;Kim, Jong Hee;Lee, Seung Goo
    • Composites Research
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    • v.35 no.4
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    • pp.288-297
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    • 2022
  • This study investigated the effect of addition of zirconia(zirconium oxide) powder on the curing behavior of phenolic resins. The heating rate controlled curing and isothermal curing behaviors of the phenol resin according to the content of the zirconia powder were analyzed. The viscosity and thermal decomposition characteristics of the phenolic resin with the zirconia content were also examind. From the DSC analysis, the degree of cure and the rate of cure were obtained. Finally, the activation energy for the cure reaction were calculated from the DSC data of the zirconia added phenolic resin. As a found, the higher the zirconia content, the longer the curing was delayed and the greater the activation energy required for curing. Additionally, the TGA result that as the content of zirconia increased, less weight loss was observed. The surface tackiness of the Carbon/Phenol prepreg was partially changed according to the zirconia content, but had no significant effect.

A STUDY ON THE CHANGES IN DEGREE OF CONVERSION OF DUAL-CURE RESTORATIVE MATERIALS WITH TIME-ELAPSE (이중중합 수복재의 시간경과에 따른 중합도 변화)

  • Yang, Chul-Ho;Kim, Shin;Jeong, Tae-Sung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.26 no.3
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    • pp.554-563
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    • 1999
  • For the purpose of elucidating the polymerization modes of dual-cure restorative materials and comparing them with single-cure restorative materials, a study was performed on the light-cured composite resin, dual-cure composite resin, dual-cure glass ionomer cement and chemical-cure glass ionomer cement. By measuring the microhardness of each material at 0mm, 1mm and 3mm depth during initial 24 hours with predetermined interval, the state of polymerization and degree of conversion was indirectly evaluated for each material, and obtained results are as follows : 1. All of four materials tested showed significant increase in microhardness after 24hrs compared with just after curing starts. 2. In all materials except Ketac-fil, there showed a significant difference in microhardness between each depth at each time interval. 3. In the test of lap time till final curing for each material, the polymerization process was revealed to last longer in the dual-cure type materials than in single-cure type materials at 3mm depth. Based on the results above, it was demonstrated with materials of dual-cure mode that the degree of conversion increases by successive curing reactions even in the deeper layers where sufficient curing light is impermeable.

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Dielectric Cure Monitoring for Glass/Polyester Prepreg Composites (유리섬유/폴리에스터 복합재료를 위한 유전 경화 모니터링)

  • Kim, Hyoung-Geun;Kim, Jin-Kook;Lee, Dai-Gil
    • Proceedings of the KSME Conference
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    • 2001.11a
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    • pp.797-803
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    • 2001
  • The on-line cure monitoring of fiber reinforced thermosetting resin matrix composite material was performed for the better quality and productivity during manufacturing. Since the dissipation factor measured by dielectrometry method is dependent on the degree of cure and temperature of resin, in this study, a new method to obtain the degree of cure during on-line cure monitoring for glass/polyester composites was developed by employing a combination function of the temperature and the dissipation factor. Two sensor signals from a K-type thermocouple and an interdigitated dielectric sensor were processed during curing process under various cure cycles. The DSC (Differential Scanning Calorimetry) data was also used for the reference of degree of cure.

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Cure Monitoring for Prototyping of Reaction Injection Molding (RIM 시작공정을 위한 경화 모니터링)

  • 권재욱;이대길
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2001.04a
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    • pp.32-36
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    • 2001
  • Recently, reaction injection molding has been used broadly for rapid prototyping, because of its convenience and versatility. Since the properties of molded products are dependent on the process variables and the production is very short(less than 2minutes), the control of process variables is important. Generally, the two significant process variables are degree of cure and temperature of the reactants. In this paper, the relation between the degree of cure and the temperature of reactants was investigated to find the optimal curing condition of reaction injection molding for rapid prototyping. The degree of cure during reaction injection molding was measured by the Lacomtech sensor and dielectrometry equipment employing Wheatstone bridge type circuit.

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