• Title/Summary/Keyword: cure conditions

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Evaluation of mechanical properties of several dual-cure resin cements by curing modes (중합방법에 따른 여러 이중중합 레진 시멘트의 기계적 성질 평가)

  • Kim, Soo-Yeon;Park, Se-Hee;Kim, Jin-Woo;Cho, Kyung-Mo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.31 no.1
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    • pp.1-9
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    • 2015
  • Purpose: The purpose of this study was to evaluate the mechanical properties of several dual-cure cements by different curing modes. Materials and Methods: One resin-modified glass ionomer cement (FujiCEM 2), two conventional dual-cure resin cements (RelyX ARC, Multilink N), and two dual-cure self-adhesive resin cements (RelyX U200, G-CEM LinkAce) were used. To evaluate the influence of the curing methods, each cements divided into four conditions (n = 20); Condition 1: self-curing for 10 minutes, Condition 2: immediate after 20 seconds light-curing, Condition 3: 24 hours after self-curing, Condition 4: 24 hours after light-curing. The compressive strength and diametral tensile strength were measured with a universal testing machine. All data were statistically analyzed using t-test, one-way ANOVA and Scheffe's test. Results: The results showed the compressive strength and diametral tensile strength after 24 hours in all curing modes were higher than immediate except RelyX ARC light-cured and Multilink N light-cured. The FujiCEM 2 showed lowest values (P < 0.05). Conclusion: The outcome was cement-depend, but there is no significant difference about compressive strength and diametral tensile strength between dual-cure self-adhesive resin cements and conventional resin cements. And this result will be used as a base line data selecting resin cement for favorable long-term prognosis.

Fluoride Release and Recharge Properties of Several Fluoride-Containing Restorative Materials (수종의 불소함유 수복재의 불소 유리 및 재충전)

  • Lee, Dongyun;Kim, Jongsoo;Han, Miran;Shin, Jisun
    • Journal of the korean academy of Pediatric Dentistry
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    • v.47 no.2
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    • pp.196-204
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    • 2020
  • The aim of the study is to compare the fluoride release and recharge properties of glass ionomer cements and 'alkasite'. Specimens of two glass ionomer cements (Fuji IX GP and Riva Self Cure), 'alkasite' restorative material (Cention N) and composite resin (Filtek™ Z350XT) were prepared. The fluoride release of each specimen was measured for 28 days. Thereafter, 1.23% acidulated phosphate fluoride (APF) gel was applied to experimental groups. No treatment was performed on control groups. The fluoride release was measured for additional 7 days to evaluate the fluoride recharge properties of each materials. The fluoride release was highest in Riva Self Cure, followed by Fuji IX GP, Cention N (p < 0.05). Fluoride release of Cention N was measured to be approximately 49% of Fuji IX GP's. After the application of 1.23% APF gel, increases in fluoride release were observed in Riva Self Cure, Fuji IX GP and Cention N (p < 0.05). Fluoride recharge was observed in Cention N as well as in glass ionomer cements. Further studies are required to evaluate the anti-cariogenic properties of Cention N at clinical conditions.

Strength Properties of Polymer-Modified Repair Mortars According to Curing Conditions and Repair Methods (양생조건 및 보수방법에 따른 폴리머시멘트모르타르의 강도 성상)

  • Kim, Wan-Ki;Jo, Young-Kug
    • Journal of the Korea Concrete Institute
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    • v.19 no.4
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    • pp.457-465
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    • 2007
  • In this paper, polymer-modified repair materials using polymer dispersions with six repair methods are prepared with various polymer-cement ratios, and tested for compressive and flexural strengths through each curing condition such as dry cure, water cure, and freezing and thawing cyclic action. And, the adhesive interface between the polymer-modified mortar and mortar substrate is observed by a scanning electron microscope. From the test results, the compressive and flexural strengths of cement mortar repaired by polymer-modified mortar are improved with a rise in the polymer-cement ratio regardless of the type of polymer and curing conditions. Such an improvement in the strengths of polymer-modified repair materials to ordinary cement mortar is explained by the high adhesion of polymer-modified mortar. Strength reduction of polymer-modified repair materials after freezing and thawing cyclic actions is recognized, but it is lower than that of unmodified mortar. Especially, cement mortar repaired by polymer-modified mortar with a St/BA emulsion has good strength properties compared with those of SBR latex and PA emulsion. Accordingly, it is judged that polymer-modified mortars with a St/BA emulsion are possible to use as repair materials to ordinary cement mortar and concrete.

Requests for Tumor Marker Tests in Turkey Without Indications and Frequency of Elevation in Benign Conditions

  • Cure, Medine Cumhur;Cure, Erkan;Kirbas, Aynur;Yazici, Tarkan;Yuce, Suleyman
    • Asian Pacific Journal of Cancer Prevention
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    • v.13 no.12
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    • pp.6485-6489
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    • 2012
  • Aims: To investigate the incidence of ordering tests for tumor markers which are used in cancer diagnosis, follow-up treatment and detection of recurrence, the rate of elevation in benign diseases and which clinics order them frequently. Materials and Method: Data for the tumor markers carbohydrate antigen 19-9 (CA 19-9), carcinoembryonic antigen (CEA), cancer antigen 125 (CA 125), cancer antigen 15-3 (CA 15-3) and alpha-fetoprotein (AFP) that were ordered by all the clinics in our Hospital between 2010 and 2011 were screened. When excluding repeated orders the results of 3,416 patients were available. It has been determined that in which benign diseases were the tumor markers frequently ordered and which of these conditions had high levels of them. Results: CA 19-9 was ordered for 1,858 patients 191 (10.3%) were malignant while 1667 (89.7%) were ordered in benign diseases. For CEA the total was 1,710, 226 (13.2%) malignant and 1484 (86.8%) benign, and for CA 125 1267, 111 (8.8%) malignant and 1156 (91.2%) benign. AFP was ordered for 1687 cases, 80 (4.7%) malignant but 1607 (95.3%) benign. CA 15-3 was ordered 1449 times, 174 (12%) for malignant and 1275 (88%) for benign diseases. In all cases, considerable proportions were positive. Conclusions: It was shown that clinicians frequently order tumor markers for benign conditions. The findings of this study has shown that tumor markers are used widely without indications as cancer screening tests.

A Study on the Treeing Phenomenon due to the Post-Cure Conditions of the Thermo-Setting Epoxy Resin (열경화성 EPOXY수능의 2인경화촉진에 따른 Treeing 현상에 관한 연구)

  • 조정수;김종경;백선환;이종호
    • The Transactions of the Korean Institute of Electrical Engineers
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    • v.37 no.6
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    • pp.406-413
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    • 1988
  • This paper is to investigate relationships between tree inception voltage, tree extension or treeing breakdown voltage and physical characteristics changing as parameter of the post-cured conditions of thermo-setting epoxy resin. According to the results in this paper, the optimal tree inception voltage and treeing breakdown voltage of the samples are obtained for the sample post cured for 15 hours at 100 'C. It can be noticed that these results are closely related with the state of interior molecule coupling and three-dimen sional cross-linked of thermo-setting epoxy resin. And tree inception, tree extension and treeing breakdown of the samples are affected significantly on the post-cured conditions and the cooling method after post-cured of thermo-setting epoxy resin. Moreover, the tree extension by ambient temperature are closely related with softening temperature of thermo-setting epoxy resin.

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Studies on the Prevention of Excessive Drying Leaves during Burley Tobacco Curing II. Effect of the Shading Conditions on the Occurrence of Excessive Drying Leaves (버어리종 담배 건조시 급건엽 발생방지에 관한 연구 II. 차광의 영향)

  • 배성국;임해건;김경태
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.32 no.1
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    • pp.10-15
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    • 1987
  • The experiment was designed to determine the proper shading rate and shading materials to decrease the excessive dried leaves during cure of burley tobacco. Five shading rates and seaven shading materials were applied on the pipe vinyl house from initial stage or yellow stage of cure. Temperature was lower and weight-loss of leaves delayed with shading from initial stage to browning stage of cure. Excessive dried leave were largely decreased as shading rate was increased to 70%. However, at shading rate more than 70%, its decreasing extent was fewer. Price per kg and physical properties improved considerably at shading rate of 50%. Shading materials alone could not completely prevent excessive dried leaves but it could decrease them. Orange, white and purple color vinyl among shading materials had so effects of shading as the black shading cloth during curing. However, white color vinyl didn't endure more than a few months due to sunshine. A difference of light quality in visible light was no significance on air curing.

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A Reforming Consideration about Social and Educational Conditions in Conformity with the Meaning of Design (디자인에 의한 교육과 사회의 개혁개념 연구)

  • 명승수
    • Archives of design research
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    • v.14 no.2
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    • pp.253-266
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    • 2001
  • In this study was groped a plan for an idea and method of design as the alternative of cure of cocial defect. Ailo, it was referred how an idea and method of design could be used for a cure of social defect and it was considered that an educational form that to actualize the idea and method of design is the basic structure of a cure or improvement of social defect. This educational form actualities exactly the 'media'which the idea and method of design pursue. In the end, an effect of media could probably make social change be practical.

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Study on Cure Behavior of Low Temperature and Fast Cure Epoxy with Mercaptan Hardener (Mercaptan 경화제에 의한 저온속경화 에폭시의 경화거동에 관한 연구)

  • Eom, Se Yeon;Seo, Sang Bum;Lee, Kee Yoon
    • Polymer(Korea)
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    • v.37 no.2
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    • pp.240-248
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    • 2013
  • The curing behaviors of diglycidyl ether of bisphenol A (DGEBA) with mercaptan hardener were studied by the comparison with amine-adduct type hardener. Curing behaviors were evaluated by DSC at dynamic and isothermal conditions. In the DSC, the dynamic experiments were based on the method of Kissinger's equation, and the isothermal experiments were fitted to the Kamal's kinetic model. Activation energy of epoxy/amine-adduct type hardener was ca. 40 kcal/mol. As the functional group of mercaptan hardener, -SH increased, on epoxy/mercaptan hardeners, the activation energies decreased from 28 to 19 kcal/mol. Epoxy/amine-adduct type hardener was initiated at $90^{\circ}C$ or higher. However, epoxy/mercaptan hardeners reduced the initiation temperatures below $80^{\circ}C$ and shortened the durations of curing reaction within 10 min. We found out that the reaction kinetics of epoxy with mercaptan hardener followed the autocatalytic reaction models, and the maximum reaction rates were shown at the conversions of 20~40%.

Thermal Stability of Glass Powder and Rubber-Filled Phenolic Resins and Dynamic Mechanical Properties of Glass Braid/Phenolic Composites (유리분말 및 고무 충진 페놀수지의 열안정성 및 Glass Braid/페놀수지 복합재료의 동역학적 열특성)

  • Yoon, Sung Bong;Cho, Donghwan;Lee, Geon-Woong
    • Journal of Adhesion and Interface
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    • v.8 no.4
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    • pp.14-22
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    • 2007
  • In the present study, the effect of milled glass powder and liquid-type nitrile rubber (NBR) on the thermal stability of phenolic resin and the dynamic mechanical properties of glass braid/phenolic composites has been investigated by means of thermogravimetric analysis and dynamical mechanical analysis. It was found that both milled glass power and NBR filled in the waterborne phenolic resin significantly influenced the thermal stability of phenolic resins and the storage modulus and tan delta of the composites. The presence of glass powder increased the thermal stability of the phenolic resin, whereas the presence of NBR resulted in the weight loss in the specific temperature range. The thermal stability of the phenolic resins without and with the fillers was dependent not only on the cure temperature but also on the cure time. The variation of the storage modulus and tan ${\delta}$ of strip-type glass braid/phenolic composites was also influenced with the introduction of glass powder and NBR to the phenolic matrix as well as by the cure conditions given.

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Analysis of Thermo-Viscoelastic Residual Stresses and Thermal Buckling of Composite Cylinders (복합재 원통구조물의 열-점탄성적 잔류음력 및 열좌굴 해석)

  • Kim, Cheol;Kim, Yeong-Kook;Choi, Woong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.8
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    • pp.1653-1665
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    • 2002
  • One of the most significant problems in the processing of composite materials is residual stresses. The residual stresses may be high enough to cause cracking in the matrix even before external loads are applied and can degrade the integrity of composite structures. In this study, thermo-viscoelastic residual stresses occurred in the polymeric composite cylinder are investigated. This type of structure is used for the launch vehicle fuselage. The time and degree of cure dependent thermo-viscoelastic constitutive equations are developed and coupled with a thermo-chemical process model. These equations are solved with the finite element method to predict the residual stresses in the composite structures during cure. A launch vehicle experiences high thermal loads during flight and re-entry due to aerodynamic heating or propulsion heat, and the thermal loads may cause thermal buckling on the structure. In this study the thermal buckling analysis of composite cylinders are performed. Two boundary conditions such as all clamped and all simply supported are used for the analysis. The effects of laminates stacking sequences, shapes and residual stresses on the critical buckling temperatures of composite cylinders are investigated. The thermal buckling analysis is performed using ABAQUS.